WO2020151597A1 - 烟支加热组件及电加热吸烟装置 - Google Patents

烟支加热组件及电加热吸烟装置 Download PDF

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Publication number
WO2020151597A1
WO2020151597A1 PCT/CN2020/072817 CN2020072817W WO2020151597A1 WO 2020151597 A1 WO2020151597 A1 WO 2020151597A1 CN 2020072817 W CN2020072817 W CN 2020072817W WO 2020151597 A1 WO2020151597 A1 WO 2020151597A1
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WO
WIPO (PCT)
Prior art keywords
heating
cigarette
resistance
substrate layer
track
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PCT/CN2020/072817
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English (en)
French (fr)
Inventor
雷宝灵
袁军
李郑发
徐中立
李永海
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深圳市合元科技有限公司
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Application filed by 深圳市合元科技有限公司 filed Critical 深圳市合元科技有限公司
Priority to KR1020217026884A priority Critical patent/KR20210116638A/ko
Priority to JP2021542566A priority patent/JP2022523485A/ja
Priority to EP20744467.0A priority patent/EP3915410A4/en
Priority to US17/425,946 priority patent/US20220248758A1/en
Publication of WO2020151597A1 publication Critical patent/WO2020151597A1/zh

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    • HELECTRICITY
    • H05ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
    • H05BELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
    • H05B3/00Ohmic-resistance heating
    • H05B3/40Heating elements having the shape of rods or tubes
    • H05B3/42Heating elements having the shape of rods or tubes non-flexible
    • H05B3/46Heating elements having the shape of rods or tubes non-flexible heating conductor mounted on insulating base
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24FSMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F40/00Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
    • A24F40/40Constructional details, e.g. connection of cartridges and battery parts
    • A24F40/46Shape or structure of electric heating means
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24FSMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F40/00Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
    • A24F40/20Devices using solid inhalable precursors
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24FSMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F40/00Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
    • A24F40/50Control or monitoring
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24FSMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F40/00Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
    • A24F40/50Control or monitoring
    • A24F40/51Arrangement of sensors
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24FSMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F40/00Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
    • A24F40/50Control or monitoring
    • A24F40/57Temperature control
    • HELECTRICITY
    • H05ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
    • H05BELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
    • H05B1/00Details of electric heating devices
    • H05B1/02Automatic switching arrangements specially adapted to apparatus ; Control of heating devices
    • H05B1/0202Switches
    • HELECTRICITY
    • H05ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
    • H05BELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
    • H05B3/00Ohmic-resistance heating
    • H05B3/0019Circuit arrangements
    • HELECTRICITY
    • H05ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
    • H05BELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
    • H05B3/00Ohmic-resistance heating
    • H05B3/40Heating elements having the shape of rods or tubes
    • H05B3/42Heating elements having the shape of rods or tubes non-flexible
    • H05B3/48Heating elements having the shape of rods or tubes non-flexible heating conductor embedded in insulating material
    • HELECTRICITY
    • H05ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
    • H05BELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
    • H05B3/00Ohmic-resistance heating
    • H05B3/40Heating elements having the shape of rods or tubes
    • H05B3/54Heating elements having the shape of rods or tubes flexible
    • H05B3/58Heating hoses; Heating collars
    • HELECTRICITY
    • H05ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
    • H05BELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
    • H05B2203/00Aspects relating to Ohmic resistive heating covered by group H05B3/00
    • H05B2203/013Heaters using resistive films or coatings

Definitions

  • the embodiments of the application relate to the field of electronic cigarettes, and in particular to a cigarette heating assembly and an electrically heated smoking device.
  • the heating non-combustion cigarette electronic cigarettes one is to heat the cigarettes with tubular heating components heated around; this type of tubular heating components are usually prepared by printing heating circuits on ceramic or stainless steel substrates . among them,
  • the heating component of the ceramic substrate adopts a heating circuit printed on a flat ceramic green body, and then is wound into a circular tubular shape and sintered to obtain a ceramic heating tube that can contain and heat cigarettes.
  • the heating element of the stainless steel base material is obtained by sintering after printing a heating circuit on the stainless steel tube after the surface insulation treatment.
  • the circuit printing of the ceramic substrate heating component is carried out on the flat ceramic green embryo, and the thickness consistency and resistance stability of the printed circuit obtained are good; but the thermal conductivity of the ceramic is relatively lacking, and the temperature rise during the heating process of the cigarette The speed is slow, and due to the slow heat conduction, the heat is mainly concentrated near the track of the printed circuit, and the cigarettes contained in the ceramic tube cannot be uniformly heated.
  • the stainless steel substrate heating element has high thermal conductivity and thinner wall thickness, so its heating speed is fast, and the overall heating of the cigarette contained in the tube is more uniform; but because the heating circuit is printed on the tube during preparation, the printing The lack of uniformity and consistency of the circuit thickness makes the resistance stability poor, which is not conducive to the heating temperature control of the product.
  • the embodiments of the present application provide a cigarette heating assembly with both resistance stability and thermal conductivity.
  • the cigarette heating assembly of the present application includes an elongated heat conducting tube, a substrate layer and a resistance heating track formed on the substrate layer; the heat conducting tube has radially opposed inner and outer surfaces; wherein, the The substrate layer is cured on the outer surface of the heat pipe, and the resistance heating track is located between the substrate layer and the heat pipe and extends along the longitudinal direction of the heat pipe; the thermal conductivity of the heat pipe material Greater than the thermal conductivity of the substrate layer material;
  • the inner surface forms a heating cavity for containing cigarettes.
  • the substrate layer includes a ceramic substrate layer, and the thickness of the ceramic substrate layer is 0.05 to 0.2 mm.
  • the ceramic substrate layer is wound by a bendable flat ceramic sheet and sintered and solidified on the outer surface of the heat pipe, and the resistance heating track is printed on at least one plane of the flat ceramic sheet The metal heating circuit.
  • the heat conducting pipe includes a metal pipe, and the thickness of the metal pipe is 0.1-0.2 mm.
  • an insulating layer is provided on the outer surface of the metal tube to insulate the metal tube from the resistance heating track.
  • the resistance heating track includes one or more heating circuits distributed at intervals; the heating circuit has a specific temperature coefficient of resistance, so that it can be used as a resistance heater and as a sensor for sensing the temperature of the cigarette heating assembly. Temperature Sensor.
  • the resistance heating track includes at least a heating circuit and a temperature measurement circuit, and the heating circuit and the temperature measurement circuit have different resistance temperature coefficients; wherein,
  • the temperature coefficient of resistance of the heating circuit satisfies it to be used as a resistance heater, and the temperature coefficient of resistance of the temperature measurement circuit satisfies to be used as a temperature sensor for sensing the temperature of the cigarette heating assembly.
  • the resistance heating trajectory includes at least a first heating trajectory and a second heating trajectory, and the first heating trajectory and the second heating trajectory are spaced apart along the longitudinal direction of the heat conduction pipe so as to pass through the heat pipe radially Conducting heat heats different areas of the heating cavity in the longitudinal direction.
  • both the first heating track and the second heating track are differentially connected to electrode pins connected to the circuit so that they can be individually controlled to generate heat.
  • This application also proposes an electrically heated smoking device, which includes a cigarette heater and a power supply for supplying power to the cigarette heater; the cigarette heater adopts the above-mentioned cigarette heating assembly.
  • This application also proposes a method for preparing the above cigarette heating assembly, which includes the following steps:
  • the heating element drive body is baked and solidified at a temperature of 70-100° C., it is then sintered at a temperature of 800-1200° C. to obtain a cigarette heating assembly.
  • the step of obtaining the ceramic germ layer includes:
  • the ceramic powder and the sintering aid are uniformly mixed, they are then pressed to form the ceramic green layer; wherein, the sintering aid includes 75% to 80% of solvent, 10% to 15% of binder, and dispersant. 2.5 ⁇ 3.5%, plasticizer 5 ⁇ 10%.
  • the binder is at least one of polyvinyl alcohol, cellulose or polyacrylic acid.
  • the dispersant is at least one of sodium polyacrylate, sodium polyphosphate or sodium citrate;
  • the plasticizer is at least one of dibutyl phthalate, glycerol or polyethylene glycol .
  • the resistance heating track has a double substrate substrate, wherein the substrate layer is used as the printing substrate in the preparation process, and the heat pipe is used as the bonding substrate for sintering and bonding after printing, and the heat conduction and heating process Disperse the base material; on the one hand, it can maintain stable resistance value of the resistance heating track and excellent heat conduction properties of the heating component during the preparation and use, and on the other hand, the heat pipe and the substrate layer can respectively form the two surfaces of the resistance heating track during use Protection to avoid the resistance change caused by the deformation of the resistance heating track due to high temperature use, and the physical friction of the cigarette plugging and so on, which causes the resistance heating track to wear.
  • Fig. 1 is a schematic diagram of a cigarette heating assembly provided by an embodiment of the present application
  • Figure 2 is a schematic cross-sectional view of the cigarette heating assembly in Figure 1 in the radial direction;
  • FIG. 3 is a schematic diagram of the ceramic substrate layer and resistance heating track of the cigarette heating assembly in FIG. 1 after being expanded along the circumferential direction of the heat pipe;
  • Fig. 4 is a graph showing the temperature rise test results of the cigarette heating assembly of the embodiment and the conventional ceramic heating tube.
  • the embodiment of the present application proposes a method for preparing a cigarette heating assembly with resistance stability and thermal conductivity, and the cigarette heating assembly is prepared on the basis of the structure shown in FIGS. 1 to 3; including a heat conduction tube 10, and The resistance heating track 20 and the ceramic substrate layer 30 are sequentially stacked outward along the radial direction of the heat pipe 10.
  • the ceramic substrate layer 30 is solidified on the outer surface of the heat pipe 10; the resistance heating track 20 is located between the heat pipe 10 and the ceramic substrate layer 30 and extends along the longitudinal direction of the heat pipe 10.
  • the ceramic substrate layer 30 may be alumina-based ceramics, zirconia-based ceramics, or diatomaceous earth-based ceramics.
  • the heat pipe 10 is made of materials with good thermal conductivity, which can include metal or alloy materials, as well as non-metallic materials, such as stainless steel, aluminum alloy, zinc alloy, copper alloy, etc.; or metal oxides, nitrides, carbides with high thermal conductivity Material, such as aluminum oxide, magnesium oxide, nickel oxide, aluminum nitride, silicon nitride, boron nitride, silicon carbide, etc.
  • the heat pipe 10 is used for heat transfer.
  • the thermal conductivity of the heat pipe 10 is made greater than the thermal conductivity of the ceramic substrate layer 30, so that the heat is used for heating.
  • the resistance heating track 20 has a dual substrate substrate, wherein the ceramic substrate layer 30 is used as a printing substrate in the preparation process, and the heat pipe 10 is used as a thermal conductive substrate combined after printing; During the preparation and use, the resistance value of the cigarette heating component is stable and the heat conduction is excellent.
  • the heat pipe 10 and the ceramic substrate layer 30 can respectively protect the two surfaces of the resistance heating track 20 to avoid high temperature use.
  • the resistance heating track 20 is deformed to cause resistance value changes, and physical friction such as cigarette sticking causes the resistance heating track 20 to wear.
  • the ceramic substrate layer 30 is composed of an unsintered flat ceramic sheet printed on the resistance heating track 20, then wound on the outer surface of the heat pipe 10 and sintered and solidified.
  • the ceramic sheet is flexible before being wound on the outer surface of the heat pipe 10, and it can be formed by mixing ceramic powder and a sintering aid into a slurry and then coating, or it can use existing commercially available flexible ceramic paper.
  • the inner diameter of the heat pipe 10 is adapted to the diameter of the usual cigarettes, and 5-6mm is suitable, which can ensure the smooth insertion of the cigarettes and make the cigarettes Close contact to improve heating efficiency during heating.
  • the resistance heating track 20 is preferably prepared by screen printing and sintering, and the material is usually pure nickel, nickel-chromium alloy, nickel-iron alloy, iron-chromium alloy, iron-chromium aluminum alloy, tungsten, platinum, and titanium alloy. Or powders such as stainless steel are mixed with the slurry and printed according to the designed pattern.
  • the thickness of the ceramic substrate layer 30 serving as the substrate and the protective layer is preferably 0.05 to 0.2 mm; and the thickness of the heat pipe 10 is preferably 0.1 to 0.2 mm.
  • the resistance heating track 20 includes a first heating track 21 and a second heating track 21 that are spaced apart along the longitudinal direction of the heat pipe 10.
  • Heating trajectory 22; the first heating trajectory 21 and the second heating trajectory 22 respectively heat different areas of the heating chamber 11 in the longitudinal direction, and can realize segmented heating at the same time, so as to meet the requirements of different smoking stages for cigarettes Separate heating to ensure uniform and stable overall smoke output.
  • the first heating trajectory 21 and the second heating trajectory 22 are set to have different heating temperatures to meet the requirements of more differentiated control.
  • the first heating track 21 and the second heating track 22 above can be differentiated and respectively provided with electrode pins for connecting with the circuit, so that the two can be individually controlled to generate heat.
  • the pins used in the embodiment in the figure include a first pin 121, a second pin 122 and a third pin 123, one of which is configured as a common
  • the other two pins are respectively configured for the corresponding connection of the first heating track 21 and the second heating track 22; for example, in one embodiment, the first pin 121 is used as a negative common pin to connect to the negative electrode of the power supply device,
  • the second pin 122 is connected to the positive pole of the power supply device as the positive pin of the first heating trace 21, and the third pin 123 is connected to the positive pole of the power supply device as the positive pin of the second heating trace 22;
  • the welding position of the pin 121 and the resistance heating track 20 is the intersection of the first heating track 21 and the second heating track 22, so that the two can share the first pin
  • the resistance heating track 20 includes one or more heating circuits distributed at intervals, and the resistance material of the heating circuit can be selected from a metal or alloy material with a specific temperature coefficient of resistance, such as a positive temperature coefficient or a negative temperature coefficient.
  • the heating circuit can be used not only as a resistance heater, but also as a temperature sensor for sensing the real-time working temperature of the heating component.
  • the resistance heating track 20 includes at least a first heating circuit and a second heating circuit. The first heating circuit and the second heating circuit have different resistance temperature coefficients; wherein the resistance temperature coefficient of the first heating circuit satisfies Used for heating cigarettes, the temperature coefficient of the second heating circuit is sufficient for sensing the temperature of the heating component.
  • the heat pipe 10 when the heat pipe 10 is made of metal or alloy, it needs to be insulated on the outer surface opposite to the resistance heating track 20, such as surface oxidation, anodization, insulating layer plating or glazing, etc. , Thereby insulating from the resistance heating track 20.
  • the method for preparing the cigarette heating assembly with the above structure of the present application adopts the following steps:
  • step S20 winding the ceramic heating drive body obtained in step S10 on the outer surface of a heat conducting tube 10a to form a heating component drive body;
  • the heating element layer 20a is printed on the surface of the ceramic green layer 30a, and then wound on the heat conducting tube 10a for sintering to prepare a heating assembly.
  • the printing process of the heating drive body layer 20a is performed on the flat surface of the ceramic green embryo to ensure the thickness consistency of the formed heating drive body layer 20a and the bonding tightness with the ceramic layer; and before sintering, it is wound and combined with the heat conducting tube 10a,
  • the sintering under the maintenance of the base material of the heat pipe 10a helps to suppress the ablation deformation, which is beneficial to maintain the resistance stability and heat conduction heating efficiency.
  • the ceramic green layer 30a in the implementation of step S10 is obtained by uniformly mixing the raw materials of the ceramic powder and a certain sintering aid and then pressing.
  • the ceramic powder can be modified or doped with alumina ceramic powder based on the quality requirements of flatness and compactness in the implementation and the effect of the outermost heat insulation substrate. It is preferably made of 45%-50% alumina and dioxide Silicon 35%-40%, calcium oxide 5%-10%, magnesium oxide 7%-9%.
  • the sintering aids include solvents, binders, dispersants and plasticizers, according to 75% to 80% of solvent, 10% to 15% of binder, 2.5% to 3.5% of dispersant, and 5 to 10% of plasticizer.
  • the solvent can be water;
  • the binder is polyvinyl alcohol (PVA), cellulose (MC) or polyacrylic acid (PAA), etc.;
  • the dispersant is sodium polyacrylate, polyacrylic acid (PAA), etc.
  • plasticizers are dibutyl phthalate (DBP), glycerol (glycerin), polyethylene glycol (PEG), etc.
  • DBP dibutyl phthalate
  • glycerol glycerin
  • PEG polyethylene glycol
  • the material used for the heating drive body layer 20a can be pure nickel, nickel-chromium alloy, nickel-iron alloy, iron-chromium alloy, iron-chromium aluminum alloy, titanium alloy or stainless steel, etc.
  • the drive body powder of these materials and the sintering aid are uniform during preparation Mix into a slurry, and then print on the surface of the ceramic green layer 30a according to the desired shape.
  • step S20 the ceramic heating element printed in step S10 is wound and combined on the outer surface of the heat pipe 10a.
  • the final step S30 is to bake and solidify the heating component driver body combined with the winding and low-temperature sintering.
  • the ceramic green embryo and the printed circuit are cured by baking to ensure stable circuit resistance; after curing, the ceramic layer is co-fired at low temperature.
  • the printed resistor heating track and the heat pipe are sintered together to form a heating component.
  • S00 Prepare ceramic powder with weight percentages of aluminum oxide 48%, silicon dioxide 36%, calcium oxide 8%, and magnesium oxide 8%; and the weight ratio of the ceramic powder and the sintering aid is 2:1 to be mixed and pressed into a thickness of 0.15mm ceramic germ layer 30a; among them, the sintering aid contains 80% water, 12% polyvinyl alcohol as a binder, 2.5% sodium citrate as a dispersant, and 5.5% glycerin as a plasticizer;
  • the heating drive body layer 20a is formed by printing on the surface of the ceramic green layer 30a of step S00 by means of screen printing to obtain a ceramic heating drive body;
  • step S20 winding and attaching the ceramic heating drive body of step S10 to the stainless steel tube after surface oxidation treatment to form a heating component drive body; wherein the wall thickness of the stainless steel tube is 0.1 mm;
  • the resistance heating track 20 is prepared by a nickel heating circuit with a resistance of 0.8 ohm.
  • the temperature rise test is compared with a conventional ceramic heating tube of the same resistance specification. The result is shown in Fig. 3; wherein, S1 in Fig. 3 is The temperature rise curve on the inner wall of the cigarette heating assembly prepared in the embodiment, S2 is the temperature rise curve of the inner wall of the conventional ceramic heating tube. It can be seen from the figure that the heating time of the ceramic heating tube is also 54s when the temperature is raised to 200 degrees, and the heating time of the cigarette heating assembly of the embodiment is 10s.
  • the common holding structure formed by flat printing on the ceramic green sheet and then winding it on the heat conducting tube and sintering makes the resistance heating track more flat and stable, and has better resistance. Value stability and longevity.
  • the application further proposes an electrically heated smoking device.
  • the electrically heated smoking device includes a cigarette heater and a power supply for supplying power to the cigarette heater; the cigarette heater uses the above-described cigarette heating assembly; The two ends of the resistance heating track in the heating assembly are respectively connected with the positive and negative poles of the power supply by pins to work.

Abstract

一种烟支加热组件,包括纵长形的导热管(10)、衬底层(30)和形成在衬底层(30)上的电阻发热轨迹(20);该导热管(10)具有径向方向相对的内表面和外表面;其中,衬底层(30)固化在导热管(10)的外表面,且电阻发热轨迹(20)位于衬底层(30)与导热管(10)之间并沿该导热管(10)的纵长方向延伸;导热管(10)材料的热导率大于衬底层(30)材料的热导率;内表面形成用于容纳烟支的加热腔(11)。该烟支加热组件,电阻发热轨迹(20)具有双衬底基材,衬底层(30)作为制备过程中的印刷衬底,而导热管(10)作为印刷之后烧结结合的结合衬底以及热量传导和分散基材;一方面维持电阻发热轨迹(20)阻值稳定和加热组件导热优良的性质,另一方面,对电阻发热轨迹(20)的两个表面形成保护,避免因高温使用、以及物理摩擦导致磨损。

Description

烟支加热组件及电加热吸烟装置 技术领域
本申请实施例涉及电子烟领域,尤其涉及一种烟支加热组件及电加热吸烟装置。
背景技术
目前加热不燃烧烟电子烟中,一种是采用四周加热的管状加热组件对烟支进行加热;这一类管状加热组件通常采用在陶瓷或者不锈钢这两种基材上印刷发热线路的方式制备获得。其中,
陶瓷基材的加热组件采用先在平面陶瓷生坯上印刷发热电路后,再卷绕成圆管状形状烧结,获得能容纳并加热烟支的陶瓷发热管。不锈钢基材的加热组件采用在表面绝缘处理后的不锈钢管上印刷发热线路后烧结获得。
陶瓷基材加热组件的线路印刷是在平面陶瓷生胚上进行,获得的印刷线路的厚度一致性、阻值稳定性较好;但是陶瓷的导热性相对欠缺,对烟支加热过程中的温升速度较慢,并且由于导热慢热量主要集中在印刷线路的轨迹附近,无法对容纳在陶瓷管内的烟支进行均匀的加热。而不锈钢基材加热组件的导热系数高、壁厚更薄,因此其升温速度快,且对容纳在管内烟支的整体加热比较均匀;但是由于是制备时发热线路是在圆管上印刷,印刷的线路厚度均匀性和一致性不足,使得阻值稳定性较差,不利于产品的发热温度控制。
发明内容
为了解决现有技术中的烟支加热组件的不同制备类型在各自阻值稳定性和导热性方面的问题,本申请实施例提供一种同时具备阻值稳定性和导热性的烟支加热组件。
本申请的烟支加热组件,包括纵长形的导热管、衬底层和形成在所述衬底层上的电阻发热轨迹;该导热管具有径向方向相对的内表面和外 表面;其中,所述衬底层固化在所述导热管的外表面,且所述电阻发热轨迹位于所述衬底层与所述导热管之间并沿该导热管的纵长方向延伸;所述导热管材料的热导率大于所述衬底层材料的热导率;
所述内表面形成用于容纳烟支的加热腔。
可选的,所述衬底层包括陶瓷衬底层,所述陶瓷衬底层的厚度为0.05~0.2mm。
可选的,所述陶瓷衬底层是由一可弯曲的平板状陶瓷片卷绕并烧结固化于所述导热管的外表面,所述电阻发热轨迹为印刷在该平板状陶瓷片至少一个平面上的金属发热线路。
可选的,所述导热管包括金属管,所述金属管的厚度0.1~0.2mm。
可选的,在所述金属管的外表面上具有用于使金属管与电阻发热轨迹绝缘的绝缘层。
可选的,所述电阻发热轨迹包括有一个或多个间隔分布的发热线路;该发热线路具有特定电阻温度系数,使其既作为电阻发热器,又作为用于感测烟支加热组件温度的温度传感器。
可选的,所述电阻发热轨迹至少包括有发热线路和测温线路,且所述发热线路和测温线路具有不同的电阻温度系数;其中,
所述发热线路的电阻温度系数满足用作为电阻加热器,所述测温线路的电阻温度系数满足用作为感测烟支加热组件温度的温度传感器。
可选的,所述电阻发热轨迹至少包括第一发热轨迹和第二发热轨迹,该第一发热轨迹和第二发热轨迹沿所述导热管的纵长方向间隔分布,以通过该导热管径向传导热量加热所述加热腔在纵长方向上的不同区域。
可选的,所述第一发热轨迹和第二发热轨迹均区别性地连接有接入电路的电极引脚以使得二者被单独控制发热。
本申请还提出一种电加热吸烟装置,包括烟支加热器、以及用于为烟支加热器供电的电源;所述烟支加热器采用以上所述的烟支加热组件。
本申请还提出以上烟支加热组件的制备方法,包括如下步骤:
获取陶瓷生胚层,并在陶瓷生胚层表面上形成发热驱体层,得到陶瓷发热驱体;
将所述陶瓷发热驱体卷绕在一导热管的外表面,形成发热组件驱体;
将所述发热组件驱体于70~100℃温度下烘烤固化后,再置于800~1200℃温度下烧结,即获得烟支加热组件。
可选的,获取所述陶瓷生胚层的步骤包括:
按照各质量分数为氧化铝45%~50%、二氧化硅35%~40%、氧化钙5%~10%、氧化镁7%~9%配置陶瓷粉末;
将所述陶瓷粉末与烧结助剂均匀混合后,再进行压制成型,即为所述陶瓷生胚层;其中,所述烧结助剂包括溶剂75~80%、粘结剂10~15%、分散剂2.5~3.5%、增塑剂5~10%。
可选的,所述粘结剂为聚乙烯醇、纤维素或聚丙烯酸中的至少一种。所述分散剂为聚丙烯酸钠、多聚磷酸钠或柠檬酸钠中的至少一种;所述增塑剂为邻苯二甲酸二丁酯、丙三醇或聚乙二醇中的至少一种。
本申请的以上烟支加热组件,电阻发热轨迹具有双衬底基材,其中衬底层作为制备过程中的印刷衬底,而导热管作为印刷之后烧结结合的结合衬底以及加热过程的热量传导和分散基材;一方面可以在制备和使用中维持电阻发热轨迹阻值稳定和加热组件导热优良的性质,同时另一方面,使用时导热管和衬底层可以分别对电阻发热轨迹的两个表面形成保护,避免因高温使用导致电阻发热轨迹产生形变引起阻值变化、以及烟支抽插等物理摩擦导致电阻发热轨迹磨损。
附图说明
一个或多个实施例通过与之对应的附图中的图片进行示例性说明,这些示例性说明并不构成对实施例的限定,附图中具有相同参考数字标号的元件表示为类似的元件,除非有特别申明,附图中的图不构成比例限制。
图1是本申请一实施例提供的烟支加热组件的示意图;
图2是图1中烟支加热组件径向方向的截面示意图;
图3是图1中烟支加热组件的陶瓷衬底层和电阻发热轨迹沿导热管的圆周方向展开后的示意图;
图4是实施例的烟支加热组件与常规陶瓷加热管的升温测试结果图。
具体实施方式
为了便于理解本申请,下面结合附图和具体实施方式,对本申请进行更详细的说明。
本申请实施例提出一种具备阻值稳定性和导热性的烟支加热组件的制备方法,而其中烟支加热组件以图1至图3所示的结构基础进行制备;包括导热管10,以及沿导热管10的径向方向向外依次层叠设置的电阻发热轨迹20和陶瓷衬底层30。并且,陶瓷衬底层30固化在导热管10外表面上;电阻发热轨迹20位于导热管10和陶瓷衬底层30之间,并沿导热管10的纵长方向延伸。
其中,陶瓷衬底层30可以采用氧化铝系陶瓷、氧化锆系陶瓷或硅藻土系陶瓷等等。导热管10采用导热性质好的材质制备,可以包括金属或合金材质、以及非金属材质,如不锈钢、铝合金、锌合金、铜合金等;或高导热性的金属氧化物、氮化物、碳化物材质,如氧化铝、氧化镁、氧化镍、氮化铝、氮化硅、氮化硼、碳化硅等。在功能上导热管10用于作为热量传递,为了防止热量被陶瓷衬底层30向外传递,因此使导热管10的热导率大于陶瓷衬底层30的热导率,使热量用于加热。
以上结构的烟支加热组件,电阻发热轨迹20具有双衬底基材,其中陶瓷衬底层30作为制备过程中的印刷衬底,而导热管10作为印刷之后结合的导热基材;一方面可以在制备和使用中维持烟支加热组件阻值稳定和导热优良的性质,同时另一方面,导热管10和陶瓷衬底层30可以分别对电阻发热轨迹20的两个表面形成保护,避免因高温使用导致电阻发热轨迹20产生形变引起阻值变化、以及烟支抽插等物理摩擦导致电阻发热轨迹20磨损。
因此基于以上,陶瓷衬底层30是由一未烧结的平板状的陶瓷片在印刷上电阻发热轨迹20后,卷绕在导热管10外表面上并烧结固化。陶瓷片卷绕于导热管10外表面之前为柔性性质,可以采用陶瓷粉料与烧结助剂混合成浆料之后涂覆形成,或者可以采用现有的可以购买获得的柔性陶瓷纸。
基于导热管10内用于容纳并加热烟支的功能设定,将其内径与通常烟支的直径适配,采用5~6mm为适,既能保证烟支的顺畅插入,又能使烟支紧密接触,提升加热时的受热效率。
在这一种结构中,电阻发热轨迹20优选采用丝网印刷烧结的方式制备,材料采用通常的纯镍、镍铬合金、镍铁合金、铁铬合金、铁铬铝合金、钨、铂、钛合金或不锈钢等粉末与浆料混合后按照设计的图案印刷即可。作为衬底和保护层的陶瓷衬底层30厚度优选采用0.05~0.2mm;而导热管10优选采用厚度0.1~0.2mm。
进一步可以参见图3将电阻发热轨迹20和陶瓷衬底层沿导热管10的圆周方向展开之后的示意图;电阻发热轨迹20包括沿导热管10的纵长方向间隔分布的第一发热轨迹21和第二发热轨迹22;第一发热轨迹21和第二发热轨迹22分别对加热腔11在纵长方向上的不同区域进行分别加热,同时可以实现分段加热,满足对烟支在不同的出烟阶段进行分别加热,保证整体出烟量的均匀稳定。或者,在另一种实施方式中,第一发热轨迹21和第二发热轨迹22被设定为具有不同的发热温度,满足更多差异化控制的要求。
根据单独控制的需要,以上第一发热轨迹21和第二发热轨迹22可以区别性地分别设置用于与电路连接的电极引脚,以使这两者可以单独被控制发热。进一步参见图1所示,从图中可以看出,图中实施例中采用的引脚包括有第一引脚121、第二引脚122和第三引脚123,其中有一个被配置为公共引脚,其余两个分别配置为用于第一发热轨迹21和第二发热轨迹22对应连接;比如在一个实施方式中,将第一引脚121作为负极公共引脚连接至电源装置的负极,第二引脚122作为第一发热轨迹21的正极引脚连接至电源装置的正极,第三引脚123作为第二发 热轨迹22的正极引脚连接至电源装置的正极;则在实施中第一引脚121与电阻发热轨迹20的焊接位点为第一发热轨迹21和第二发热轨迹22交接部位,使这两者能共用该第一引脚121。
进一步在另一实施方式中,电阻发热轨迹20包括有一个或多个间隔分布的发热线路,发热线路的电阻材料可以选取具有特定电阻温度系数的金属或合金材料,例如正温度系数或负温度系数,这样发热线路既可以用来作为电阻发热器,又可以作为用来感测加热组件实时工作温度的温度传感器。作为另一实施例,电阻发热轨迹20至少包括有第一发热线路和第二发热线路,第一发热线路和第二发热线路具有不同的电阻温度系数;其中,第一发热线路的电阻温度系数满足用来加热烟支,第二发热线路的温度系数满足用来感测加热组件的温度。
同时基于防止短路的导电要求,当导热管10采用金属或合金材质时,那么需要对其与电阻发热轨迹20相对的外表面上进行绝缘处理,比如表面氧化、阳极氧化、镀绝缘层或者上釉等,从而与电阻发热轨迹20绝缘。
本申请以上结构的烟支加热组件的制备方法,采用如下步骤进行:
S10,在陶瓷生胚层30a的表面上通过丝网印刷的方式形成发热驱体层20a,得到陶瓷发热驱体;
S20,将步骤S10获得的陶瓷发热驱体卷绕在一导热管10a的外表面,形成发热组件驱体;
S30,将发热组件驱体于70~100℃温度下烘烤固化后,再置于800~1200℃温度下烧结,即获得烟支加热组件。
以上制备方法采用将发热驱体层20a在陶瓷生胚层30a的表面印刷后,再卷绕于导热管10a上一次烧结制备加热组件。发热驱体层20a的印刷过程是在陶瓷生胚的平整表面进行,保证形成的发热驱体层20a的厚度一致性和与陶瓷层的结合紧密性;并且烧结之前与导热管10a卷绕结合,在导热管10a的基材保持下烧结,有助于抑制烧蚀形变利于保持阻值稳定性和导热升温效率。
其中,步骤S10实施中陶瓷生胚层30a是采用将陶瓷粉料的原料与 一定的烧结助剂混合均匀后压制获得。其中陶瓷粉料基于实施中平整致密性的品质要求,以及作为最外层隔热的基材效果,可以采用改性或者掺杂氧化铝陶瓷粉,优选可由氧化铝45%~50%、二氧化硅35%~40%、氧化钙5%~10%、氧化镁7%~9%进行配置。
另,烧结助剂包括有溶剂、粘结剂、分散剂及增塑剂,按照溶剂75~80%、粘结剂10~15%、分散剂2.5~3.5%、增塑剂5~10%的重量比混合配制。在本申请的陶瓷衬底的生胚制备中,溶剂可以采用水;粘结剂为聚乙烯醇(PVA)、纤维素(MC)或聚丙烯酸(PAA)等;分散剂为聚丙烯酸钠、多聚磷酸钠或柠檬酸钠等;增塑剂为邻苯二甲酸二丁酯(DBP)、丙三醇(甘油)、聚乙二醇(PEG)等。混合成生胚料时,陶瓷粉末与烧结助剂按照质量比1~2.5:1进行混合。
发热驱体层20a所采用的材质可以是纯镍、镍铬合金、镍铁合金、铁铬合金、铁铬铝合金、钛合金或不锈钢等,制备中将这些材质的驱体粉末与烧结助剂均匀混合成浆料,然后按照所需的形状在陶瓷生胚层30a表面进行印刷即可。
步骤S20将步骤S10印刷完成的陶瓷发热驱体在导热管10a外表面上进行卷绕结合。最终步骤S30对卷绕结合的发热组件驱体进行烘烤固化和低温烧结,先通过烘烤使陶瓷生胚和印刷线路固化,确保线路阻值稳定;固化后再低温共烧的方式将陶瓷层、印刷电阻发热轨迹、以及导热管烧结在一起形成发热组件。
在以上方式和结构的基础上,为了进一步体现制备获得的发热组件的升温速率和阻值稳定性,以下以具体的实施例为例进行说明。
S00,以重量百分数氧化铝48%、二氧化硅36%、氧化钙8%、氧化镁8%配置陶瓷粉末;并按照陶瓷粉末与烧结助剂的重量比为2:1混合后压制成厚度为0.15mm的陶瓷生胚层30a;其中,烧结助剂中含水80%、粘结剂聚乙烯醇12%、分散剂柠檬酸钠2.5%、增塑剂甘油5.5%;
S10,然后将纯镍金属粉与购买的印刷烧结助剂(90%左右为松油醇、5%左右为乙基纤维素,其余为厂家自行补充添加的功能助剂)混合成混 合浆料;通过丝网印刷的方式在步骤S00的陶瓷生胚层30a表面印刷形成发热驱体层20a,获得陶瓷发热驱体;
S20,将步骤S10的陶瓷发热驱体于表面氧化处理后的不锈钢管上卷绕贴附,形成发热组件驱体;其中,不锈钢管的管壁厚度0.1mm;
S30,将发热组件驱体于100度℃下保温5min固化,再于真空炉中烧结;烧结过程中10℃/min的速率升温至1000℃后,保温1小时后,取出即为实施例制备的烟支加热组件。
以上实施例中电阻发热轨迹20采用按照0.8欧姆阻值的镍发热线路制备,与同样阻值规格的常规陶瓷发热管进行升温测试对比,其结果如图3所示;其中,图3中S1为实施例制备的烟支加热组件的内壁上升温曲线,S2为常规陶瓷发热管内壁的升温曲线。从图中可以看出,同样升温到200度陶瓷发热管的升温时间为54s,实施例的烟支加热组件的升温时间为10s。
进一步检测各自通电循环使用50次后的电阻阻值变化,对比结果如下表:
  样品数 烧结后的电阻值 循环50次后的电阻值
实施例 3 0.80±0.01欧 0.86~0.91欧
常规陶瓷发热管 1 0.82欧 1.08欧
从以上测试的结果可以看出,本实施例中在陶瓷生胚上平整印刷后卷绕在导热管上后烧结形成的共同保持结构,使得电阻发热轨迹更加平整和稳固,具有更好的电阻阻值稳定性和寿命。
本申请进一步还提出一种电加热吸烟装置,电加热吸烟装置包括烟支加热器、以及为烟支加热器供电的电源;烟支加热器采用以上所描述的烟支加热组件;装配时使烟支加热组件中电阻发热轨迹的两端分别用引脚与电源的正负极连通即可工作。
需要说明的是,本申请的说明书及其附图中给出了本申请的较佳的 实施例,但并不限于本说明书所描述的实施例,进一步地,对本领域普通技术人员来说,可以根据上述说明加以改进或变换,而所有这些改进和变换都应属于本申请所附权利要求的保护范围。

Claims (10)

  1. 一种烟支加热组件,其特征在于,包括纵长形的导热管、衬底层和形成在所述衬底层上的电阻发热轨迹;该导热管具有径向方向相对的内表面和外表面;其中,所述衬底层固化在所述导热管的外表面,且所述电阻发热轨迹位于所述衬底层与所述导热管之间并沿该导热管的纵长方向延伸;所述导热管材料的热导率大于所述衬底层材料的热导率;
    所述内表面形成用于容纳烟支的加热腔。
  2. 如权利要求1所述的烟支加热组件,其特征在于,所述衬底层包括陶瓷衬底层,所述陶瓷衬底层的厚度为0.05~0.2mm。
  3. 如权利要求2所述的烟支加热组件,其特征在于,所述陶瓷衬底层是由一可弯曲的平板状陶瓷片卷绕并烧结固化于所述导热管的外表面,所述电阻发热轨迹为印刷在该平板状陶瓷片至少一个平面上的金属发热线路。
  4. 如权利要求1或2所述的烟支加热组件,其特征在于,所述导热管包括金属管,所述金属管的厚度0.1~0.2mm。
  5. 如权利要求4所述的烟支加热组件,其特征在于,在所述金属管的外表面上具有用于使金属管与电阻发热轨迹绝缘的绝缘层。
  6. 如权利要求1或2所述的烟支加热组件,其特征在于,所述电阻发热轨迹包括有一个或多个间隔分布的发热线路;该发热线路具有特定电阻温度系数,使其既作为电阻发热器,又作为用于感测烟支加热组件温度的温度传感器。
  7. 如权利要求1或2所述的烟支加热组件,其特征在于,所述电阻发热轨迹至少包括有发热线路和测温线路,且所述发热线路和测温线路具有不同的电阻温度系数;其中,
    所述发热线路的电阻温度系数满足用作为电阻加热器,所述测温线路的电阻温度系数满足用作为感测烟支加热组件温度的温度传感器。
  8. 如权利要求1所述的烟支加热组件,其特征在于,所述电阻发热轨迹至少包括第一发热轨迹和第二发热轨迹,该第一发热轨迹和第二发 热轨迹沿所述导热管的纵长方向间隔分布,以通过该导热管径向传导热量加热所述加热腔在纵长方向上的不同区域。
  9. 如权利要求8所述的烟支加热组件,其特征在于,所述第一发热轨迹和第二发热轨迹均区别性地连接有接入电路的电极引脚以使得二者被单独控制发热。
  10. 一种电加热吸烟装置,包括烟支加热器、以及用于为烟支加热器供电的电源;其特征在于,所述烟支加热器为权利要求1至9任一项所述的烟支加热组件。
PCT/CN2020/072817 2019-01-26 2020-01-17 烟支加热组件及电加热吸烟装置 WO2020151597A1 (zh)

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