WO2019049207A1 - Matériau à base de tabac - Google Patents

Matériau à base de tabac Download PDF

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Publication number
WO2019049207A1
WO2019049207A1 PCT/JP2017/031947 JP2017031947W WO2019049207A1 WO 2019049207 A1 WO2019049207 A1 WO 2019049207A1 JP 2017031947 W JP2017031947 W JP 2017031947W WO 2019049207 A1 WO2019049207 A1 WO 2019049207A1
Authority
WO
WIPO (PCT)
Prior art keywords
tobacco
tobacco material
particles
dispersion medium
material according
Prior art date
Application number
PCT/JP2017/031947
Other languages
English (en)
Japanese (ja)
Inventor
亮祐 長瀬
敬一 塙
Original Assignee
日本たばこ産業株式会社
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 日本たばこ産業株式会社 filed Critical 日本たばこ産業株式会社
Priority to RU2020112537A priority Critical patent/RU2745863C1/ru
Priority to KR1020207009086A priority patent/KR102425798B1/ko
Priority to CA3074591A priority patent/CA3074591C/fr
Priority to JP2019540157A priority patent/JP6945635B2/ja
Priority to PCT/JP2017/031947 priority patent/WO2019049207A1/fr
Priority to CN201780094636.9A priority patent/CN111050572A/zh
Priority to EP17924586.5A priority patent/EP3662765B1/fr
Publication of WO2019049207A1 publication Critical patent/WO2019049207A1/fr
Priority to US16/809,322 priority patent/US20200196657A1/en

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Classifications

    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18—Treatment of tobacco products or tobacco substitutes
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18—Treatment of tobacco products or tobacco substitutes
    • A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18—Treatment of tobacco products or tobacco substitutes
    • A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
    • A24B15/32—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by acyclic compounds
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00—Preparing tobacco in the factory
    • A24B3/12—Steaming, curing, or flavouring tobacco

Definitions

  • the present invention relates to tobacco materials and tobacco products comprising the same.
  • Patent Document 1 discloses a method of dispersing leaf tobacco particles in a dispersion medium and adding a dispersion to cut tobacco.
  • Patent Document 2 discloses a method of heating a suspension of tobacco particles to improve flavor by utilizing a Maillard reaction or the like (Patent Document 2, paragraph 0013).
  • the tobacco particles are less than 40 mesh (Patent Document 2, paragraph 0024), ie, less than 400 ⁇ m.
  • Patent Document 3 discloses a tobacco particle suspension of 60 to 400 mesh at 80 to 180 ° F. (26.7 to 82. Heating to 2 ° C. is disclosed (Patent Document 3, paragraph 0056).
  • the particle size of the tobacco particles is 38 to 250 ⁇ m.
  • Patent Document 1 is a useful technique in that it can impart flavor evenly to tobacco cutting and the like.
  • viscosity of the dispersion increases due to interaction between water-soluble component derived from tobacco raw material and water, etc.
  • the said subject is a subject peculiar to using the microparticles
  • the inventors of the present invention have solved the above problems by setting the amount of hemicellulose to a certain amount or less in a tobacco material containing an aqueous dispersion medium and tobacco particles having an average particle diameter of 30 ⁇ m or less dispersed in the dispersion medium. That is, the said subject is solved by the following this invention.
  • a tobacco material comprising an aqueous dispersion medium and tobacco particles having an average particle size of 30 ⁇ m or less dispersed in the dispersion medium, A tobacco material, wherein the hemicellulose content in the tobacco material is 0.8 wt% or less based on bone dry tobacco particles.
  • the tobacco material as described in (1) whose pH is 4.8 or less.
  • the aqueous organic compound is selected from the group consisting of monohydric alcohols, polyhydric alcohols, sugar alcohols, saccharides, polyhydric alcohol esters, and combinations thereof.
  • a tobacco product comprising the tobacco material according to any one of the above (1) to (8).
  • the present invention can provide a low viscosity tobacco material in which tobacco particles are dispersed in an aqueous dispersion medium.
  • X to Y includes X and Y which are final values.
  • the tobacco material of the present invention comprises an aqueous dispersion medium and tobacco particles having an average particle size of 30 ⁇ m or less dispersed in the dispersion medium.
  • the tobacco particles may be derived from tobacco raw materials, fermented tobacco raw materials, or heat-treated tobacco raw materials.
  • a tobacco raw material is the whole tobacco or the site
  • the type of tobacco is not particularly limited, and examples thereof include yellow species, burley species, native species, and orient leaves.
  • the state of the tobacco material to be used may be a fresh leaf which has not been subjected to drying immediately after harvest, etc., or it may be dried after harvest, or these may be used in combination.
  • the tobacco particles can be prepared by any method, but it is preferable to subject the tobacco raw material to a usual drying treatment and then to coarsely grind it with a usual coarse crusher and then to finely grind it. Drying treatment and coarse grinding may be performed as known, and the average particle size of the coarsely crushed tobacco particles is preferably in the range of several hundred ⁇ m to several mm.
  • the method of pulverization is also not limited, and any method of wet pulverization or dry pulverization may be used.
  • the wet pulverization can be carried out by adding a liquid dispersion medium to coarsely pulverized tobacco particles and mixing them, and treating the mixture with a wet pulverizer (for example, MIC-2: manufactured by Nara Machinery Co., Ltd.).
  • the rotation speed of the pulverizer is preferably 1100 to 1300 rpm, and the pulverizing time is preferably about 5 to 100 minutes.
  • the dry pulverization can be carried out by treating the roughly pulverized tobacco particles with a dry pulverizer such as a jet mill.
  • the average particle size of the tobacco particles thus obtained is 30 ⁇ m or less, preferably 20 ⁇ m or less.
  • the lower limit of the average particle diameter of the tobacco particles is 5 ⁇ m or more, and in another embodiment 8 ⁇ m or more.
  • the average particle size of the tobacco particles can be adjusted under the pulverizing conditions, and for example, the average particle size can be increased by shortening the pulverizing time, lowering the viscosity of the dispersion medium, or the like.
  • the average particle size in the present invention is determined by laser diffraction scattering method. Specifically, the average particle diameter in the present invention is measured with a refractive index of 1.60 to 0.101 using a laser diffraction particle size distribution measuring apparatus (for example, Shimadzu nanoparticle size distribution measuring apparatus SALD-2100). Ru.
  • a laser diffraction particle size distribution measuring apparatus for example, Shimadzu nanoparticle size distribution measuring apparatus SALD-2100.
  • the aqueous dispersion medium is a liquid medium containing water.
  • the aqueous dispersion medium may be water alone or may contain a specific organic compound.
  • the organic compound is preferably water soluble, and the aqueous organic compound is preferably selected from the group consisting of monohydric alcohols, polyhydric alcohols, sugar alcohols, saccharides, polyhydric alcohol esters, and combinations thereof. .
  • an amphiphilic organic compound such as methanol.
  • Examples of the monohydric alcohol include methanol, ethanol, 1-propanol, 2-propanol, 1-butanol, 2-butanol, 2-methyl-1-propanol, 2,2-dimethylethanol, cyclohexanol and the like monovalent C1- Examples thereof include C6 aliphatic alcohols, monohydric alcohols having an aromatic substituent such as benzyl alcohol, monohydric alcohols containing one or more halogen elements, and monohydric alcohols having one or more ether bonds.
  • Polyhydric alcohol is a generic term for compounds having two or more hydroxyl groups in one molecule, and includes, but is not limited to, glycerin and propylene glycol.
  • sugar alcohols include sorbitol, maltitol, xylitol, erythritol, lactitol, sorbitan, xylose, arabinose, mannose, trehalose and the like.
  • sugars include lactose, sugar, coupling sugar, glucose, enzyme starch syrup, acid saccharified starch syrup, maltose starch syrup, malt sugar, isomerized sugar, fructose, reduced maltose, reduced starch starch syrup, honey and the like.
  • polyhydric alcohol esters include fatty acid polyhydric alcohol esters such as fatty acid triglyceride.
  • the mixing ratio of water and the organic compound is not limited.
  • the mixing ratio may be arbitrary.
  • the content of water in the aqueous dispersion medium is preferably more than 50% by weight, more preferably 80% by weight or more, and still more preferably 90% by weight or more. .
  • the ratio of additives may be optional, when the additive is contained, the total amount of tobacco particles and dispersion medium in the tobacco material of the present invention is preferably 90% by weight or more in the total amount of the tobacco material, 95% by weight It is more preferable that it is more than.
  • Example 2 The tobacco material of the present invention was manufactured and evaluated in the same manner as in Example 1 except that the content of tobacco particles (absolute drying) was changed to 14.3% by weight, and the high-temperature and high-pressure treatment was changed to D described above.
  • Example 3 The tobacco material of the present invention was produced and evaluated in the same manner as in Example 1 except that the content of tobacco particles (absolute drying) was changed to 20.0% by weight, and the high-temperature and high-pressure treatment was changed to D described above.
  • Comparative Example 1 A comparative tobacco material was produced and evaluated in the same manner as in Example 1 except that the high temperature and high pressure treatment was changed to the following. X: not implemented Y: 150-5 minutes Z: 150 ° C-15 minutes
  • Comparative Example 1Y and the like As shown in FIG. 1, the comparative tobacco material treated with the conditions Y and Z in Comparative Example 1 (hereinafter referred to as “Comparative Example 1Y and the like”) showed a tendency to be thickened. This is presumed to be because the interaction with water was increased because the polysaccharide was not extracted in large amounts into the aqueous medium and was not decomposed by the high temperature and high pressure treatment under the conditions.
  • the tobacco material of the present invention such as Example 1A, it is considered that viscosity reduction is achieved by decomposing polysaccharides containing hemicellulose after being extracted in large amounts in the aqueous medium. From the above, it is clear that the tobacco material of the present invention having a hemicellulose content equal to or less than a predetermined value has a low viscosity.
  • Example 4 For the tobacco material of the present invention (cigarette particle (absolute dry) content: 16.7% by weight) treated under high temperature and high pressure conditions A and C in Example 1, the treated product is in a slurry using a pH meter manufactured by METTLER TOLEDO Hydrogen ion concentration was measured.
  • the tobacco material was divided into 50 ml vials and subjected to storage tests. The storage test was performed by storing the vials in a constant temperature room at 35 ° C. Immediately after the start of the storage test, sampling was performed for 72 hours and 120 hours, and the number of viable bacteria was measured. The measurement of the general viable count was carried out as follows according to the method described in Japan Food Research Laboratories HP.
  • the sample was diluted with sterile water to prepare a 10-fold serial dilution.
  • the samples diluted to each concentration were seeded on a standard agar medium, cultured at 35 ° C. for 2 days, and the number of colonies was counted after culture.
  • the initial viable count of the sample was calculated based on the difference in the number of colonies appeared for each dilution ratio.

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Manufacture Of Tobacco Products (AREA)

Abstract

L'invention concerne un matériau à base de tabac comprenant : un milieu de dispersion aqueux ; et des particules de tabac dispersées dans le milieu de dispersion et ayant une taille moyenne de particule de 30 µm ou moins, ledit matériau à base de tabac ayant une teneur en hémicellulose de 0,8 % en poids ou moins sur la base de particules de tabac anhydre. Le matériau à base de tabac est caractérisé en ce qu'il présente une faible viscosité.
PCT/JP2017/031947 2017-09-05 2017-09-05 Matériau à base de tabac WO2019049207A1 (fr)

Priority Applications (8)

Application Number Priority Date Filing Date Title
RU2020112537A RU2745863C1 (ru) 2017-09-05 2017-09-05 Табачный материал, способ производства табачного материала, табачный продукт и способ его производства
KR1020207009086A KR102425798B1 (ko) 2017-09-05 2017-09-05 담배 재료
CA3074591A CA3074591C (fr) 2017-09-05 2017-09-05 Materiau a base de tabac
JP2019540157A JP6945635B2 (ja) 2017-09-05 2017-09-05 たばこ材料
PCT/JP2017/031947 WO2019049207A1 (fr) 2017-09-05 2017-09-05 Matériau à base de tabac
CN201780094636.9A CN111050572A (zh) 2017-09-05 2017-09-05 烟草材料
EP17924586.5A EP3662765B1 (fr) 2017-09-05 2017-09-05 Matériau à base de tabac
US16/809,322 US20200196657A1 (en) 2017-09-05 2020-03-04 Tobacco material

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/JP2017/031947 WO2019049207A1 (fr) 2017-09-05 2017-09-05 Matériau à base de tabac

Related Child Applications (1)

Application Number Title Priority Date Filing Date
US16/809,322 Continuation US20200196657A1 (en) 2017-09-05 2020-03-04 Tobacco material

Publications (1)

Publication Number Publication Date
WO2019049207A1 true WO2019049207A1 (fr) 2019-03-14

Family

ID=65634894

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/JP2017/031947 WO2019049207A1 (fr) 2017-09-05 2017-09-05 Matériau à base de tabac

Country Status (8)

Country Link
US (1) US20200196657A1 (fr)
EP (1) EP3662765B1 (fr)
JP (1) JP6945635B2 (fr)
KR (1) KR102425798B1 (fr)
CN (1) CN111050572A (fr)
CA (1) CA3074591C (fr)
RU (1) RU2745863C1 (fr)
WO (1) WO2019049207A1 (fr)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2022137903A1 (fr) * 2020-12-24 2022-06-30 日本たばこ産業株式会社 Procédé de fabrication de matériau à base de tabac
WO2022259702A1 (fr) * 2021-06-11 2022-12-15 日本たばこ産業株式会社 Formulation de tabac

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6218157B2 (fr) * 1984-09-11 1987-04-21 Nippon Tabako Sangyo Kk
JPH0646817A (ja) 1992-04-09 1994-02-22 Philip Morris Prod Inc 再構成タバコシート及びその製造法及び使用法
JPH1066559A (ja) 1996-08-01 1998-03-10 R J Reynolds Tobacco Co 風味・芳香化合物を提供する方法
JP2013215187A (ja) * 2012-03-15 2013-10-24 Kao Corp 糖の製造方法
WO2014185103A1 (fr) 2013-05-13 2014-11-20 日本たばこ産業株式会社 Matière à base de tabac, produit à base de tabac auquel est ajouté de la matière à base de tabac, et procédé pour produire une matière à base de tabac
JP2015200056A (ja) * 2014-03-31 2015-11-12 日本製紙株式会社 溶解クラフトパルプを連続製造する方法
US20170064993A1 (en) * 2015-09-08 2017-03-09 R.J. Reynolds Tobacco Company High-pressure cold pasteurization of tobacco material

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CN101273796B (zh) * 2008-05-07 2010-06-02 广东省金叶烟草薄片技术开发有限公司 一种复合造纸法再造烟叶及其生产方法
US9167847B2 (en) * 2009-03-16 2015-10-27 Philip Morris Usa Inc. Production of coated tobacco particles suitable for usage in a smokeless tobacoo product
CN102429319B (zh) * 2011-08-26 2013-11-27 重庆恒远晋通科技有限公司 烟草连续提取的方法
JP2014185103A (ja) 2013-03-22 2014-10-02 L'oreal Sa 縮合剤を用いる毛髪の持続的着色
EP2783585A1 (fr) * 2013-03-28 2014-10-01 Philip Morris Products S.A. Boîtier à base de tabac
JP6847845B2 (ja) * 2015-04-01 2021-03-24 フィリップ・モーリス・プロダクツ・ソシエテ・アノニム 均質化したたばこ材料、および均質化したたばこ材料を製造する方法
RU2713492C2 (ru) * 2015-07-21 2020-02-05 Филип Моррис Продактс С.А. Способ изготовления табачных продуктов

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6218157B2 (fr) * 1984-09-11 1987-04-21 Nippon Tabako Sangyo Kk
JPH0646817A (ja) 1992-04-09 1994-02-22 Philip Morris Prod Inc 再構成タバコシート及びその製造法及び使用法
JPH1066559A (ja) 1996-08-01 1998-03-10 R J Reynolds Tobacco Co 風味・芳香化合物を提供する方法
JP2013215187A (ja) * 2012-03-15 2013-10-24 Kao Corp 糖の製造方法
WO2014185103A1 (fr) 2013-05-13 2014-11-20 日本たばこ産業株式会社 Matière à base de tabac, produit à base de tabac auquel est ajouté de la matière à base de tabac, et procédé pour produire une matière à base de tabac
JP2015200056A (ja) * 2014-03-31 2015-11-12 日本製紙株式会社 溶解クラフトパルプを連続製造する方法
US20170064993A1 (en) * 2015-09-08 2017-03-09 R.J. Reynolds Tobacco Company High-pressure cold pasteurization of tobacco material

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Title
See also references of EP3662765A4

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2022137903A1 (fr) * 2020-12-24 2022-06-30 日本たばこ産業株式会社 Procédé de fabrication de matériau à base de tabac
WO2022137904A1 (fr) * 2020-12-24 2022-06-30 日本たばこ産業株式会社 Procédé de fabrication de matériau à base de tabac
WO2022259702A1 (fr) * 2021-06-11 2022-12-15 日本たばこ産業株式会社 Formulation de tabac

Also Published As

Publication number Publication date
KR102425798B1 (ko) 2022-07-28
EP3662765B1 (fr) 2022-08-17
RU2745863C1 (ru) 2021-04-02
JP6945635B2 (ja) 2021-10-06
US20200196657A1 (en) 2020-06-25
EP3662765A1 (fr) 2020-06-10
CA3074591C (fr) 2022-07-12
EP3662765A4 (fr) 2021-04-07
CN111050572A (zh) 2020-04-21
JPWO2019049207A1 (ja) 2020-10-01
KR20200044925A (ko) 2020-04-29
CA3074591A1 (fr) 2019-03-14

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