WO2017204255A1 - Dispositif de traitement de liquide - Google Patents

Dispositif de traitement de liquide Download PDF

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Publication number
WO2017204255A1
WO2017204255A1 PCT/JP2017/019394 JP2017019394W WO2017204255A1 WO 2017204255 A1 WO2017204255 A1 WO 2017204255A1 JP 2017019394 W JP2017019394 W JP 2017019394W WO 2017204255 A1 WO2017204255 A1 WO 2017204255A1
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Prior art keywords
liquid
treated
ultrasonic generator
water
processed
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PCT/JP2017/019394
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English (en)
Japanese (ja)
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年明 恒松
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年明 恒松
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Publication of WO2017204255A1 publication Critical patent/WO2017204255A1/fr

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    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/30—Treatment of water, waste water, or sewage by irradiation
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/34—Treatment of water, waste water, or sewage with mechanical oscillations
    • C02F1/36—Treatment of water, waste water, or sewage with mechanical oscillations ultrasonic vibrations
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/68—Treatment of water, waste water, or sewage by addition of specified substances, e.g. trace elements, for ameliorating potable water
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
    • C04B35/46—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on titanium oxides or titanates

Definitions

  • the present invention relates to a liquid processing apparatus, and more particularly, to a liquid processing apparatus for processing water or a liquid obtained by mixing water with another substance.
  • Ordinary water is in a state called a cluster in which a plurality of water molecules are linked together.
  • the physical and chemical properties of water are changed by breaking down the clusters and making them smaller, or by separating them into independent single water molecules, and by separating the water molecules into hydrogen ions and hydroxide ions.
  • a phenomenon different from the previous one appears, for example, the permeability and solubility are improved, and the oxidation-reduction potential is inclined toward the reduction side, resulting in an alkaline water quality.
  • a ceramic containing SiO 2 , Al 2 O 3 , or Fe 2 O 3 is immersed in water in order to modify the water by reducing the water cluster.
  • a method for discharging electrodes for 12 hours or more has been proposed, but the conventionally developed method for miniaturizing a water cluster requires a long time for cluster miniaturization and further has a processing capability. Compared to the power consumption, the power consumption is large, and many of the devices are large.
  • the present invention reduces the redox potential when water is treated by miniaturizing water clusters and decomposing water into hydrogen ions and hydroxide ions, thereby obtaining alkaline water quality. It is possible to provide a liquid processing apparatus capable of generating an emulsion fuel that does not separate for a long time when a mixed liquid of water and fuel oil, particularly water and heavy oil, is processed. According to the apparatus, it is possible to eliminate the disadvantages of the conventional method.
  • the liquid treatment apparatus according to the present invention is effective not only for treating water or a mixed liquid of water and fuel oil, but also for treating various liquids in which other substances are mixed with water, and reforms each into a useful liquid. It is possible.
  • the liquid processing apparatus as described in claim 1 is an apparatus for processing water or a liquid obtained by mixing water with another substance as a processing target liquid, provided the filling of the ceramic containing ore to SiO 2, Al 2 O 3 which emits electromagnetic waves successive having a main vibration range to the frequency 0.3 ⁇ 3TH Z zone in the flow path of the treatment target liquid as a main component And an ultrasonic generator for irradiating ultrasonic waves toward the ceramic filling portion is provided so that the liquid to be processed passes through the ceramic filling portion. But it is characterized by being processed.
  • the ceramic filling unit and the ultrasonic generator are disposed in a container that forms a flow path of the liquid to be processed. Introduced into the container from the ceramic filling section side, the treated liquid is treated by passing through the ceramic filling section, and treated with ultrasonic waves emitted from the ultrasonic generator, and the treated liquid. Is configured to be discharged out of the container from the ultrasonic generator side.
  • the ceramic filling unit and the ultrasonic generator are disposed in a container that forms a flow path of the liquid to be processed.
  • the introduced processing target liquid is processed by the ultrasonic wave irradiated from the ultrasonic generator, flows into the ceramic filler, and passes through the ceramic filler. Further, the liquid is further processed and the processed liquid is discharged from the ceramic filling portion side to the outside of the container.
  • a flow path for fluid for cooling the ultrasonic generator is provided inside or outside the ultrasonic generator, and the flow path
  • the liquid to be processed or the processed liquid is circulated, and when the flow path is outside the ultrasonic generator, a fluid having excellent electrical insulation properties such as air is circulated.
  • the ceramic containing ore mainly composed of SiO 2 and Al 2 O 3 has the following components (component value is mass%) , The same shall apply hereinafter) or a gravel-like sintered body.
  • Al 2 O 3 3.4 to 3.8%
  • TiO 2 33.3 to 36.9%
  • ZrO 2 11.3 to 12.7%
  • Bentonite 24.7 to 27.3%, the balance being other oxides.
  • a liquid to be processed that is, a liquid to be processed, is introduced into a container in which a ceramic filling unit and an ultrasonic generator are disposed, and the liquid to be processed is passed through the ceramic filling unit and the ultrasonic generator. Since the liquid can be processed, the processing does not take a long time without requiring a large-scale apparatus.
  • the water cluster becomes finer as described above, and the water molecule contains hydrogen ions and water.
  • the water molecule contains hydrogen ions and water.
  • the liquid processing apparatus of the present invention is effective in the field of manufacturing soft drinks, chemicals, liquid seasonings, liquor, lotions, etc., and has water permeability and solubility by modifying the water itself.
  • characteristics and applications such as drinking, cooking, bathing, animal and plant growth, fish and shellfish preservation, etc. Can be used.
  • the liquid processing apparatus of the present invention uses water or a liquid obtained by mixing other substances in water as a processing target liquid, and is used for processing the processing target liquid.
  • Water includes tap water, natural water, well water, etc., and water mixed with other substances means water and non-hydrophilic oil, especially mixed liquid of water and heavy oil or waste oil, water and hydrophilic Liquids such as ethanol and the like, and liquids in which water is one of the main ingredients (for example, alcoholic beverages and soy sauce).
  • ores containing SiO 2 and Al 2 O 3 as main components that emit continuous electromagnetic waves having a main vibration region in the frequency 0.3 to 3 TH Z band in the flow path of the liquid to be processed ores containing SiO 2 and Al 2 O 3 as main components that emit continuous electromagnetic waves having a main vibration region in the frequency 0.3 to 3 TH Z band in the flow path of the liquid to be processed.
  • Ceramic comprising ore of SiO 2, Al 2 O 3 which emits electromagnetic waves continuous with the main vibration range to the frequency 0.3 ⁇ 3TH Z (wavelength 100 [mu] m ⁇ 1 mm) as a main component, SiO 2, Al 2 O 3 Is a sintered body composed of ore containing other oxides and ZrO 2 , TiO 2, etc., and is used as a spherical or gravel of an appropriate size, or a mixture of these .
  • Preferred components of the ceramic comprising ore to the SiO 2, Al 2 O 3 as a main component, SiO 2,: 16.6 ⁇ 18.6 %, Al 2 O 3: 3.4 ⁇ 3.8%, TiO 2 : 33.3 to 36.9%, ZrO 2 : 11.3 to 12.7%, bentonite: 24.7 to 27.3%, the balance is other oxides, and the most preferable component values are SiO 2,: 17.6%, Al 2 O 3: 3.6%, TiO 2: 35.1%, ZrO 2: 12.0%, bentonite: is 26.0%.
  • the configuration of the liquid processing apparatus of the present invention includes, for example, a ceramic filling unit and an ultrasonic generator for irradiating ultrasonic waves toward the ceramic filling unit in a container in which a flow path of a liquid to be processed is formed.
  • the liquid to be processed is processed by passing through the ceramic filling portion, and is further processed by ultrasonic waves.
  • the ceramic filling unit and the ultrasonic generator do not necessarily need to be arranged in series, as long as the liquid to be treated can be continuously passed through the ceramic filling unit and the ultrasonic generator in the container. Good.
  • the ultrasonic wave is not only directly irradiated to the ceramic filling part, but also the ultrasonic wave emitted from the ultrasonic generator is indirectly applied to the ceramic filling part using a reflector such as a reflector. It is also possible to adopt a method of irradiating automatically.
  • the ultrasonic generator is disposed outside the container and only the vibrator of the ultrasonic generator that generates ultrasonic waves is disposed. You may make it insert in a container and may irradiate an ultrasonic wave toward the ceramic filling part.
  • a cooling fluid is circulated inside or outside the ultrasonic generator to cool the ultrasonic generator and suppress temperature rise so that it can withstand continuous oscillation. Is preferable.
  • a preferred embodiment of the liquid processing apparatus of the present invention is provided with a ceramic filler 3 and an ultrasonic generator 8 in a container 1 that forms a flow path of a liquid to be processed.
  • the treatment target liquid is introduced into the container 1 from the ceramic filling unit 3 side, and the introduced treatment target liquid is processed by passing through the ceramic filling unit 3, and the supersonic wave irradiated from the ultrasonic generator 8.
  • the liquid is processed with sound waves, and the processed liquid is discharged from the ultrasonic generator 8 side to the outside of the container.
  • Reference numeral 2 denotes an inlet for the liquid to be processed
  • 9 denotes an outlet for the liquid to be processed
  • 5 denotes a partition plate having a large number of holes through which the liquid to be processed passes
  • 6 denotes a vibrator of the ultrasonic generator 8.
  • the ceramic filling portion 3 may contain ceramic spheres or gravel as a group of layers, but in order to prevent unevenness of the flow path of the liquid to be treated, a large number of openings are formed in a honeycomb shape between the ceramic layers.
  • the ceramic plate 4 which has can also be inserted.
  • the ceramic constituting the ceramic filling portion 3 disposed in the front stage of the container 1 is SiO that emits a continuous electromagnetic wave having a main vibration range at a frequency of 0.3 to 3 TH Z (wavelength 100 ⁇ m to 1 mm). 2 , ores containing Al 2 O 3 as main components, as described above, SiO 2 , Al 2 O 3 as main components, ores containing other oxides, ZrO 2 , TiO 2, etc. It is blended and sintered and used as a sphere or gravel of an appropriate size.
  • Ultrasonic waves are continuously irradiated from the transducer 6 of the ultrasonic generator 8 disposed at the rear stage of the container 1 toward the partition plate 5 disposed at a distance of several centimeters from the tip of the transducer 6. Is done.
  • the ultrasonic waves are preferably irradiated directly toward the partition plate 5, but depending on the arrangement form of the ceramic filler 3 and the ultrasonic generator 8, the generated ultrasonic waves may be reflected using a reflector such as a reflector.
  • a method of indirectly irradiating the ceramic filling portion may be employed, and direct irradiation and indirect irradiation may be used in combination.
  • FIG. 1 illustrates an example in which four ultrasonic generators are installed in parallel
  • the number of ultrasonic generators installed can be appropriately selected according to the size of the container 1, desired processing capability, and the like.
  • the distance between the vibrator 6 and the partition plate 5 of the ultrasonic generator 8 is appropriately selected and determined according to the propagation state of the ultrasonic wave in the liquid to be treated.
  • the processing target liquid is introduced from the inlet 2 of the processing target liquid in the container 1, and this processing target liquid is processed by passing through the ceramic filling unit 3 and is irradiated from the vibrator 6 of the ultrasonic generator 8. Treated with ultrasound. Specifically, the liquid to be treated passes through the ceramic filling unit 3 and is treated, and then travels toward the ultrasonic generator 8. The ultrasonic waves continue from the vibrator 6 of the ultrasonic generator 8 toward the partition plate 5. As a result, the treatment with ultrasonic waves proceeds, so that the processed liquid is almost completed when passing through the ultrasonic generator 8.
  • a flow path for circulating the processed liquid is provided inside the ultrasonic generator 8, and the processed liquid is passed through the flow hole 7 into the flow path. It is preferable that the ultrasonic generator 8 is cooled by the treated liquid to suppress temperature rise and endure continuous oscillation. The treated liquid that has been treated is finally discharged out of the container from the outlet 9 of the treated liquid.
  • a fluid flow path for cooling the ultrasonic generator is provided outside the ultrasonic generator, A fluid having excellent electrical insulation such as air can be circulated through the path.
  • the liquid processing apparatus of the present invention shown in FIG. 1, it is basically provided with a container 1 in which a ceramic filling portion 3 is disposed at the front stage and an ultrasonic generator 8 is disposed at the rear stage.
  • the ceramic filling unit 3 and the ultrasonic generator 8 may be arranged in parallel as a pair, or the pair may be arranged in series, or may be arranged in series and parallel.
  • a liquid processing related apparatus can be arranged in the subsequent stage of the ultrasonic generator 8 or in front of the ceramic filler 3.
  • the liquid processing related apparatus may be provided inside the container or outside the container.
  • the ultrasonic generator 8 and its vibrator 6 are integrated, so that the central axes of the ceramic filling portion 3 and the ultrasonic generator 8 and the vibrator 6 are aligned with each other.
  • the ceramic filling part is arranged in the front stage and the vibration part of the ultrasonic generator is arranged in the rear stage, the expected function can be exhibited, and the central axes of both do not necessarily match. It does not have to be.
  • a ceramic filling unit and an ultrasonic generator are disposed in a container that forms a flow path of the liquid to be processed, and the liquid to be processed is on the ultrasonic generator side. Is introduced into the container, and the introduced processing target liquid is processed by the ultrasonic wave irradiated from the ultrasonic generator and flows into the ceramic filler, and further processed by passing through the ceramic filler. The finished solution is configured to be discharged out of the container from the ceramic filling portion side.
  • the structure of the ceramic filling portion and the ultrasonic generator is the same as that in the above-described preferred embodiment, and the cooling of the ultrasonic generator 8 is preferably the same as described above.
  • the liquid to be processed enters from the outlet 9 of the processed liquid positioned on the ultrasonic generator 8 side and is discharged from the inlet 2 of the liquid to be processed positioned on the ceramic filling unit 3 side. It is. Even in this embodiment, the processing efficiency is slightly reduced, but it can be practically used.
  • the main reason is that, in the vicinity of the partition plate 5, coupled with the fact that the decomposition of the water cluster in the ceramic filling portion 3 is maximized in the vicinity of the partition plate 5 that receives the most vibrational energy transmission and reception. This is because it is the central part of the process for the liquid to be processed, and from which direction the liquid to be processed comes is because it does not greatly affect the efficiency of the process.
  • a processing target liquid composed of water or a liquid obtained by mixing water with another substance is introduced into the container 1 from the inlet 2 of the processing target liquid provided in the container 1, and the ceramic layer filled in the ceramic filler 3. To the downstream partition plate 5.
  • a ceramic sphere or gravel is a sintered body containing an ore having the ability to emit continuous electromagnetic waves having a main vibration range in the terahertz band (0.3 to 3 THz (wavelength 100 ⁇ m to 1 mm)).
  • the water molecules in the treatment liquid are subjected to vibration with a wavelength of 100 ⁇ m to 1 mm by the electromagnetic waves radiated from the gravel.
  • Water molecules form a cluster such as (H 2 O) n in which many water molecules gather due to hydrogen bonding, but the value of n is considered to be relatively easy and change in a short time. From the behavior, liquid water molecules can be regarded as a compound having an apparently large molecular weight.
  • the generated frequency can decompose a cluster of mixed sizes, and the cluster decomposed by receiving electromagnetic waves becomes a small cluster having a smaller n value than before, or changes into an independent water molecule.
  • part of hydrogen atoms constituting water is separated by applying ultrasonic vibrations or shocks to the refined or single water molecules, and part of the water consists of hydrogen ions and hydroxides. Decomposes into ions. As the separation and decomposition progresses, some of them become hydrogen molecules and oxygen molecules that dissolve in water, and some are released into the atmosphere. Therefore, hydroxide ions are left in the water, and the oxidation-reduction potential is lowered and the pH value is increased to become alkaline water quality.
  • An ultrasonic generator 8 that generates an ultrasonic wave of about 20 KHz is installed on the downstream side of the partition plate 5 and is continuously irradiated from the vibrator 6 in the direction of the partition plate 5 with an interval of several centimeters. .
  • This ultrasonic wave causes the ceramic spheres and gravel to obtain more vibration energy and radiate stronger electromagnetic waves.
  • the cavitation generated in the liquid to be processed by the ultrasonic waves destroys the liquid to be processed, and the liquid to be processed is also subjected to actions such as generation of shock waves, partial high temperature and pressure, and stirring and dispersion.
  • the ultrasonic generator disposed in the subsequent stage acts to further enhance the function of the ceramic filling section disposed in the previous stage, and the function of the ultrasonic generator is also added. Thus, more effective liquid treatment can be performed.
  • the monomolecularized water molecules are small particles, so they are easy to disperse in the oil component, and ultrasonic waves can cause partial destruction of the oil.
  • recombination proceeds, and in the process hydrogen ions, hydroxide ions or water molecules present in the surrounding are incorporated by covalent bonds or hydrogen bonds, and further hydrogen molecules and oxygen
  • the molecule is dissolved and incorporated, and a normal W / O emulsion is also formed to have a structure different from that of the original oil component.
  • a major feature is that it is not used at all.
  • the fuel oil which is a treated liquid, has an increased calorific value and improved combustibility by restructuring the oil composition and becoming an oxygen-containing fuel containing oxygen inside. Is possible.
  • Example 1 As shown in FIG. 1, the ceramic (SiO 2 , Al 2 O 3 ) that emits a continuous electromagnetic wave (terahertz wave) having a main vibration range at a frequency of 0.3 to 3 TH Z (wavelength 100 ⁇ m to 1 mm) A ceramic ball or gravel with a diameter of 8 to 15 mm formed by sintering ore or the like to be sintered is disposed in the front stage, and an ultrasonic generator 8 that generates ultrasonic waves of 20 KHz is provided in the rear stage. The tap water was treated using the containers 1 installed in parallel.
  • a continuous electromagnetic wave terahertz wave
  • the distance between the tip of the transducer 6 of the ultrasonic generator 8 and the partition plate 5 is about 5 cm, and a flow path 7 through which the treated liquid flows to the ultrasonic generator 8 is provided in each of the ultrasonic generators 8.
  • the ultrasonic generator 8 can be cooled with the treated liquid.
  • the redox potential and pH value of tap water before treatment and tap water after treatment are as shown in Table 1.
  • the redox potential decreases and the pH value rises. It was confirmed that the water quality was alkaline.
  • Example 2 Using the same liquid processing apparatus as in Example 1, a liquid in which tap water was mixed with fuel oil (heavy oil) was processed. The mixed solution was sufficiently mixed and then introduced into the liquid processing apparatus. About the emulsion fuel obtained after the treatment, the separation of oil and water was evaluated, and a combustion test (combustion time: 25 minutes) was performed using a warm air machine, and the exhaust gas temperature was measured to evaluate the calorific value. The evaluation results are shown in Table 2.
  • the emulsion fuel obtained by the liquid processing apparatus of the present invention does not separate for a long time even if it is mixed with 35% water by volume, even after being left for 20 days. It was confirmed that a stable emulsion fuel was produced.
  • the temperature rise value is substantially the same as that of the original heavy oil (crude oil) not mixed with tap water, and the obtained emulsion fuel has a volume of about 20 compared to the crude oil. Since it has increased by ⁇ 35%, it can be estimated that the total calorific value has increased even if the increase in fuel supply to the burner due to the decrease in viscosity is taken into account. Furthermore, it is a matter of course that the generation of carbon dioxide can be reduced as compared with crude oil.

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Abstract

La présente invention concerne un dispositif de traitement de liquide pour traiter de l'eau ou un liquide dans lequel une autre substance est mélangée dans de l'eau. Ce dispositif de traitement de liquide peut être développé pour des utilisations distinctives telles que la possibilité, lors du traitement de l'eau, d'améliorer la perméabilité, la solubilité, etc., de l'eau et de générer des ions d'hydrogène, des ions d'hydroxyde, etc., en effectuant de façon proactive la décomposition de l'eau, et lors du traitement d'un liquide dans lequel une autre substance est mélangée avec de l'eau, par exemple, dans le cas d'un liquide mixte d'eau et de mazout, étant capable de former un carburant en émulsion qui ne se sépare pas sur de longues périodes sans utiliser des additifs. Le dispositif de traitement de liquide est caractérisé : en ce qu'il est configuré de sorte qu'une section remplie de céramique, qui comprend un minerai qui émet des ondes électromagnétiques consécutives avec une plage de vibration principale dans la bande de fréquence de 0,3 à 3 THz et qui comporte SiO2 et Al2O3 en tant que composants principaux, est disposée dans le canal d'écoulement pour le liquide étant traité, et le liquide étant traité est traité en passant à travers la section remplie de céramique; et en ce qu'il est configuré de sorte qu'un dispositif de génération d'ondes ultrasonores pour émettre des ondes ultrasonores vers la section remplie de céramique est disposé et le liquide en cours de traitement est en outre traité avec des ondes ultrasonores.
PCT/JP2017/019394 2016-05-27 2017-05-24 Dispositif de traitement de liquide WO2017204255A1 (fr)

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JP2016105887A JP6746081B2 (ja) 2016-05-27 2016-05-27 液体処理装置
JP2016-105887 2016-05-27

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CN113293040A (zh) * 2021-07-07 2021-08-24 中改低碳科技(上海)有限公司 一种高原野战坦克柴油动力推进剂及其制备方法
CN113477148A (zh) * 2021-07-28 2021-10-08 中改低碳科技(上海)有限公司 一种燃油添加剂在线式太赫兹超声均质器及生产装置
JP7204037B1 (ja) 2021-08-27 2023-01-13 創美環境技研合同会社 機能水の製造装置および製造方法

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CN113443856B (zh) * 2021-07-21 2022-12-27 泉州慈光科技有限公司 太赫兹波共振陶瓷材料、其制备方法及应用其的净水器
JP7403756B1 (ja) 2023-07-12 2023-12-25 年明 恒松 水含有燃料の製造方法及び製造装置

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CN113293040A (zh) * 2021-07-07 2021-08-24 中改低碳科技(上海)有限公司 一种高原野战坦克柴油动力推进剂及其制备方法
CN113477148A (zh) * 2021-07-28 2021-10-08 中改低碳科技(上海)有限公司 一种燃油添加剂在线式太赫兹超声均质器及生产装置
JP7204037B1 (ja) 2021-08-27 2023-01-13 創美環境技研合同会社 機能水の製造装置および製造方法
JP2023033145A (ja) * 2021-08-27 2023-03-09 創美環境技研合同会社 機能水の製造装置および製造方法
WO2024024666A1 (fr) * 2021-08-27 2024-02-01 創美環境技研合同会社 Dispositif et procédé de production d'eau fonctionnelle

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