WO2017003130A1 - 다공성 다면체 파우더를 포함하는 유중수형 화장료 조성물 - Google Patents

다공성 다면체 파우더를 포함하는 유중수형 화장료 조성물 Download PDF

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WO2017003130A1
WO2017003130A1 PCT/KR2016/006692 KR2016006692W WO2017003130A1 WO 2017003130 A1 WO2017003130 A1 WO 2017003130A1 KR 2016006692 W KR2016006692 W KR 2016006692W WO 2017003130 A1 WO2017003130 A1 WO 2017003130A1
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Prior art keywords
water
oil
powder
less
cosmetic composition
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PCT/KR2016/006692
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English (en)
French (fr)
Korean (ko)
Inventor
김세진
한고운
황정선
심민경
Original Assignee
(주)아모레퍼시픽
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Priority to CN201680048048.7A priority Critical patent/CN107920963B/zh
Publication of WO2017003130A1 publication Critical patent/WO2017003130A1/ko
Priority to HK18108304.4A priority patent/HK1248561A1/zh

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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/04—Dispersions; Emulsions
    • A61K8/06—Emulsions
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/25—Silicon; Compounds thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/02—Preparations containing skin colorants, e.g. pigments
    • A61Q1/04—Preparations containing skin colorants, e.g. pigments for lips
    • A61Q1/06—Lipsticks
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin

Definitions

  • the present specification relates to a water-in-oil cosmetic composition
  • a water-in-oil cosmetic composition comprising a porous polyhedron powder.
  • the skin acts as a protective film to protect the living body from the external environment. It prevents the loss of biological components such as water or electrolytes and prevents harmful substances from entering the body. .
  • Such skin is largely divided into epidermal layer, dermal layer and subcutaneous fat layer.
  • the epidermal layer is composed of keratinocytes and melanocytes. Since the outermost keratinocyte layers of skin are in direct contact with the external environment, they require strong resistance to physical, chemical, or permeation of substances, and prevent the loss of moisture from the body to the outside. At the same time, it should maintain flexibility by retaining adequate moisture on its own.
  • the moisture content of the skin is about 70% in the dermal layer, but decreases toward the epidermal layer, which is about 10 to 30% in the keratinocyte layer.
  • the water supplied from the dermal layer is mainly moved up the stratum corneum by passive diffusion and finally discharged to the outside. This is called Trans Epidermal Water Loss (TEWL), and it is known that it is the sebaceous component and the epidermal lipid which are the lipid membrane components of the keratinocyte layer to maintain the appropriate level of transdermal moisture loss.
  • TEWL Trans Epidermal Water Loss
  • the keratinocyte layer is known to play an important role in moisturizing the skin due to the presence of a substance having a hydrophilic water retention ability called a natural moisturizing factor (NMF).
  • NMF natural moisturizing factor
  • the skin When the moisture of the normal keratinocyte layer is maintained about 10 to 30%, the skin is smooth and soft, and the body protects normally. However, when the moisture content of the keratinocyte layer is less than 10%, the skin becomes rough and the body loses its protective function, resulting in aging. For example, in the case of dry skin, the aggregation force of keratinocytes is weakened, and a scale phenomenon in which keratinocytes are peeled off like a piece of scale from the surface of the skin appears. Thus, the dryness of the skin is a moisture content of the keratinocyte layer. This is because it is less than normal skin.
  • the conventional cosmetic composition for supplying proper moisture to the skin is made in the form of emulsifying a certain amount of water phase in the oil phase using an emulsifier (W / O emulsion).
  • W / O emulsion emulsifier
  • the existing W / O emulsions stably disperse the water in the oil using an emulsifier.
  • the use of emulsifiers is accompanied by a heavy feeling of use and sensitive to light, thereby oxidizing greatly affects the stability of the contents.
  • a water-in-oil cosmetic composition that stably disperses water in oil without the use of emulsifiers.
  • Patent Document 1 KR10-2013-0022096 A
  • Patent Document 2 JP4134073 B
  • One aspect of the present invention is to provide a water-in-oil cosmetic composition in which water is stably dispersed in an oil phase without an emulsifier.
  • Another aspect of the present invention is to provide a water-in-oil cosmetic composition
  • a water-in-oil cosmetic composition comprising an aqueous, oily and porous polyhedral powder.
  • Another aspect of the invention to provide a lipstick product comprising the water-in-oil cosmetic composition.
  • a water-in-oil cosmetic composition comprising an aqueous, oily and porous polyhedral powder.
  • the porous polyhedron powder functions as an emulsifier, and provides a water-in-oil cosmetic composition that does not include other emulsifiers other than the porous polyhedron powder.
  • the porous polyhedron powder provides a water-in-oil cosmetic composition is a polyhedron is a powder comprising any one or more of the shape of a tetrahedron, cube, octahedron, dodecahedron and icosahedron.
  • the porous polyhedron powder provides a water-in-oil cosmetic composition that is a powder containing 40% or less, 30% or less or 10% or less of spherical particles in the total powder.
  • the porous polyhedron powder provides a water-in-oil cosmetic composition having a pore size of 50 to 1000 mm 3.
  • the porous polyhedron powder provides a water-in-oil cosmetic composition having a pore distribution of 0.9 to 2.5 cc / g.
  • the porous polyhedron powder provides a water-in-oil cosmetic composition having a particle size of 1 to 8 ⁇ m.
  • the porous polyhedron powder provides a water-in-oil cosmetic composition having a particle size of 2 to 4 ⁇ m.
  • the porous polyhedron powder provides a water-in-oil cosmetic composition is a powder containing any one or more of silica powder and boron nitride powder.
  • the porous polyhedron powder is 1 to 20% by weight and the aqueous phase is 5 to 25% with respect to the total composition to provide a water-in-oil cosmetic composition.
  • a method for producing a water-in-oil cosmetic composition comprising the steps of mixing the oil phase and the amphipathic porous polyhedron to produce an oil phase mixture; It provides a water-in-oil type cosmetic composition comprising a; and mixing by adding an aqueous phase to the oil-based mixture.
  • a lipstick comprising the water-in-oil cosmetic composition.
  • composition according to one aspect of the present invention is excellent in the stability of the moisture in the oil phase.
  • composition according to an aspect of the present invention has a high oil content when applied to the skin, and has good adhesion and sustainability, and at the same time, has an effect of refreshing a frustrating film at the beginning of application.
  • composition according to one aspect of the present invention has a cooling effect when applied to the skin.
  • composition according to one aspect of the present invention provides aesthetic stability when applied to the skin.
  • composition according to an aspect of the present invention when applied to the skin is left in the skin in close contact as the water evaporates after application provides excellent moisture moisturizing power.
  • composition according to one aspect of the present invention provides an effect that the porous polyhedral fine powder adheres to the skin for a long time after application when applied to the skin.
  • FIG. 1 is a conceptual view of a porous polyhedron powder polyhedron shape according to an aspect of the present invention.
  • Figure 2 is a microscopic photograph of A: 100% oil composition, B: 85% oil, 10% moisture, spherical porous silica powder 5% and C: 85% oil, 10% moisture, 5% spherical porous silica powder. .
  • a water-in-oil cosmetic composition comprising an aqueous, oily and porous polyhedral powder.
  • the porous polyhedron powder functions as an emulsifier, and provides a water-in-oil cosmetic composition that does not include other emulsifiers other than the porous polyhedron powder.
  • the water phase may comprise water.
  • the water in addition to the water may include a water-soluble polymer and an active ingredient having a particular efficacy.
  • the water-soluble polymer is dissolved in water to act as a thickener, the type is not limited significantly, for example, there is a natural water-soluble polymer, a semi-synthetic water-soluble polymer or a synthetic water-soluble polymer.
  • Natural water-soluble polymers include, for example, plant-based polymers (such as gum arabic, tragacanth gum, galactan, guar gum, carob gum, karaya gum, carrageenan, pectin, agar, queens seed (marmelo), and algocolloids (algae). Concentrate), starch (rice, corn, potato, wheat), glycylisic acid); Microbial polymers (such as xanthan gum, dextran, succinoglucan, pullulan, etc.); Animal polymers such as collagen, casein, albumin, gelatin and the like.
  • plant-based polymers such as gum arabic, tragacanth gum, galactan, guar gum, carob gum, karaya gum, carrageenan, pectin, agar, queens seed (marmelo), and algocolloids (algae). Concentrate), starch (rice, corn, potato, wheat), glycylisic acid); Microbial
  • Semi-synthesized water-soluble polymers include, for example, starch-based polymers (eg, carboxymethyl starch, methylhydroxypropyl starch, etc.); Cellulose polymers (methyl cellulose, ethyl cellulose, methyl hydroxypropyl cellulose, hydroxyethyl cellulose, sodium cellulose sulfate, hydroxypropyl cellulose, carboxymethyl cellulose, sodium carboxymethyl cellulose, crystalline cellulose, cellulose powder, etc.); Alginate type polymers (for example, sodium alginate, propylene glycol ester, etc.) etc. are mentioned.
  • starch-based polymers eg, carboxymethyl starch, methylhydroxypropyl starch, etc.
  • Cellulose polymers methyl cellulose, ethyl cellulose, methyl hydroxypropyl cellulose, hydroxyethyl cellulose, sodium cellulose sulfate, hydroxypropyl cellulose, carboxymethyl cellulose, sodium carboxymethyl cellulose,
  • Examples of the synthesized water-soluble polymer include vinyl polymers (eg, polyvinyl alcohol, polyvinyl methyl ether, polyvinylpyrrolidone, carboxyvinyl polymer, etc.); Polyoxyethylene-based polymers (such as polyethylene glycol 20,000, 40,000,60,000 polyoxyethylene polyoxypropylene copolymers, etc.); Acrylic polymers (such as sodium polyacrylate, polyethylacrylate, polyacrylamide, etc.); Polyethyleneimine; Cationic polymers and the like.
  • vinyl polymers eg, polyvinyl alcohol, polyvinyl methyl ether, polyvinylpyrrolidone, carboxyvinyl polymer, etc.
  • Polyoxyethylene-based polymers such as polyethylene glycol 20,000, 40,000,60,000 polyoxyethylene polyoxypropylene copolymers, etc.
  • Acrylic polymers such as sodium polyacrylate, polyethylacrylate, polyacrylamide, etc.
  • Polyethyleneimine Cationic polymers and the like.
  • the water-soluble polymer constituting the water phase may be a copolymer of ammonium acryloyldimethyltaurate / VP copolymer in consideration of coordination with other components and stabilization of the water phase.
  • the content of the water-soluble polymer in the water phase is preferably 0.05 to 1 part by weight, more preferably 0.1 to 0.5 part by weight, in consideration of the thickening effect of the water-soluble polymer and the stabilization effect of the water phase.
  • the water phase in the composition according to the present invention preferably comprises an active ingredient having a particular efficacy, wherein the active ingredient is one that can be dissolved in water while having a particular effect such as anti-oxidation, moisturizing, whitening or wrinkle improvement, etc.
  • the kind is not particularly limited, and examples of the antioxidant component include phosphoric acid, citric acid, ascorbic acid, and the like.
  • a moisturizing component polyethylene glycol, propylene glycol, glycerin, 1,3-butylene glycol, xylitol, Sorbitol, maltitol, panthenol, chondroitin sulfate, hyaluronic acid, mucotin sulfate, caronic acid, atherocollagen, cholesteryl-12-hydroxystearate, sodium lactate, bile salt, dl-pyrrolidone carboxylate, short chain Soluble collagen, diglycerin (EO) PO adducts, Rosa roxburghii extract, yarrow extract, maryrod extract and the like.
  • EO diglycerin
  • the moisturizing component constituting the water phase in the cosmetic according to the present invention is composed of at least one member selected from the group consisting of propylene glycol, glycerin, and panthenol in view of harmony with other components. Can be.
  • the content of the active ingredient having a particular effect in the water phase, in particular the moisturizing component is preferably 10 to 30 parts by weight per 100 parts by weight of water, in consideration of coordination with other components and exhibiting predetermined efficacy, 15 to 25 weight It may be wealth.
  • the oil phase is a substance that constitutes the external appearance of the water-in-oil formulation, and is not particularly limited as long as it can be generally used in cosmetics and the like.
  • the oil phase may be one or more selected from the group consisting of liquid fats, solid fats, waxes, hydrocarbon oils, higher fatty acids, higher alcohols, synthetic ester oils and silicone oils.
  • the liquid fats and oils include olive oil, camellia oil, jojoba oil, triglyceride, trioctanoate glycerine, triisopalmitate glycerine and the like.
  • the solid fats and oils include palm oil, hardened palm oil, palm oil, hardened oil, hardened castor oil and the like.
  • waxes examples include beeswax, candelilla wax, carnauba wax, lanolin, jojoba wax, and the like.
  • Hydrocarbon oils include liquid paraffin, squalene, petrolatum, microcrystalline wax, and the like.
  • Higher fatty acids include lauric acid, myristic acid, palmitic acid, stearic acid, behenic acid, and the like.
  • Higher alcohols include cetyl alcohol, stearyl alcohol, behenyl alcohol, myristyl alcohol, cetos tearyl alcohol and the like.
  • Synthetic ester oils include isopropyl myristate, cetyloctanoate, octyl dodecyl myritate, isopropyl palmitate, hexyl laurate, myristyl myristate, cetyl lactate, isocetyl isostearate, neopentyl glycol dicaprate , Ethylhexylglycerin, cetylethylhexanoate, ethylhexyl palmitate, cetostearyl alcohol and the like are exemplified.
  • silicone oil examples include chain-type silicone oils such as dimethylpolysiloxane, methylphenylpolysiloxane and methylhydrogenpolysiloxane, and cyclic silicone oils such as dodecamethylcyclohexasiloxane, octamethylcyclotetrasiloxane, and decamethylcyclopentasiloxane.
  • chain-type silicone oils such as dimethylpolysiloxane, methylphenylpolysiloxane and methylhydrogenpolysiloxane
  • cyclic silicone oils such as dodecamethylcyclohexasiloxane, octamethylcyclotetrasiloxane, and decamethylcyclopentasiloxane.
  • the oil phase may be included in an amount of 55 to 99% by weight based on the total composition. Preferably it may be 60 to 95% by weight, more preferably 80 to 90% by weight. If the content is less than 55% by weight, the content of the trauma is too small to form a stable formulation, and if the content is more than 99% by weight, the formulation stability and the feeling of use are deteriorated. It is included in the oil phase in the cosmetic composition.
  • the oil phase may optionally contain additive components within a range that does not impair the effects of the present invention.
  • additive components for example, other oily components, oil-soluble polymers, powders, polymer granules, etc. can be mix
  • polyhedron is a structure having two or more flat polygonal faces.
  • the porous polyhedron powder may include various polyhedron shapes, but the shape of the polyhedron is not limited to a specific polyhedron.
  • the shape of the polyhedron may be n-sided, and the n-sided may be a regular n-hedron (regular polyhedron) having the same shape and size as the surface.
  • n is a tetrahedron
  • n is 20 or less.
  • the polyhedron may be a polyhedron having a different size than the regular polyhedron.
  • it may be a convex polyhedron which does not cut the inside of the polyhedron even if any surface of the polyhedron is extended, and if the surface is extended, the plane may be a concave polyhedron to cut the inside of the polyhedron.
  • polyhedron does not include spherical cases.
  • the porous polyhedron powder may include spherical particles.
  • the porous polyhedron powder provides a water-in-oil type cosmetic composition is a powder including any one or more of the shape of the polyhedron, tetrahedron, cube, octahedron, dodecahedron and icosahedron as shown in FIG.
  • the powder of the present specification is a polyhedral particle of 60% or more of the total powder, and may include spherical particles in addition to the polyhedron.
  • the polyhedral particles of the porous powder is at least 60%, at least 65%, at least 70%, at least 75%, at least 80%, at least 85%, at least 90%, at least 95%, at least 96%, 97% or more, 98% or more, or 99% or more.
  • the porous polyhedron powder is 40% or less, 38% or less, 36% or less, 34% or less, 32% or less, 30% or less, 28% or less, 26% or less, 24% or less of spherical particles in the whole powder, 22% or less, 20% or less, 19% or less, 18% or less, 17% or less, 16% or less, 15% or less, 14% or less, 13% or less, 12% or less, 11% or less, 10% or less, 9% 8% or less, 7% or less, 6% or less, 5% or less, 4% or less, 3% or less, 2% or less, 1% or less, 0.9% or less, 0.8% or less, 0.7% or less, 0.6% or less, 0.5% or less, 0.4% or less, 0.3% or less, 0.2% or less, 0.1% or less, or 0.01% or less.
  • the content of the polyhedron particles and spherical particles in the porous polyhedron powder is within the above range, it is applied to the composition to show an effect of close contact with the skin for a long time.
  • the adhesion to the skin is excellent, there is a property that does not erase well when applied to lipstick or gloss products.
  • porous polyhedron powder is amphiphilic because it has both lipophilic and hydrophilic properties.
  • the dispersed particles are rigid (fine particles (hundreds of nm or more)) and have a spherical shape (silica bead, nylon powder, or acrylic resin powder), the blowing is severe.
  • the porous polyhedron powder of the present invention has a polyhedral shape particle shape, and because the particle size is 8 ⁇ m or less, the oil absorption power is large and the skin adhesion is good.
  • the porous polyhedron powder has a particle size of at least 1.0 ⁇ m, at least 1.1 ⁇ m, at least 1.2 ⁇ m, at least 1.3 ⁇ m, at least 1.4 ⁇ m, at least 1.5 ⁇ m, at least 1.6 ⁇ m, at least 1.7 ⁇ m, at least 1.8 ⁇ m.
  • ⁇ m or more 2.0 ⁇ m or more, 2.1 ⁇ m or more, 2.2 ⁇ m or more, 2.3 ⁇ m or more, 2.4 ⁇ m or more, 2.5 ⁇ m or more, 2.6 ⁇ m or more, 2.7 ⁇ m or more, 2.8 ⁇ m or more, 2.9 ⁇ m or more, 3.0 ⁇ m or more, 3.1 May be at least 3.2 ⁇ m, at least 3.3 ⁇ m, at least 3.4 ⁇ m, at least 3.5 ⁇ m, at least 3.6 ⁇ m, at least 3.7 ⁇ m, at least 3.8 ⁇ m, at least 3.9 ⁇ m, or at least 4.0 ⁇ m.
  • the porous polyhedron powder has a particle size of 8.0 ⁇ m, 7.5 ⁇ m, 7.0 ⁇ m, 6.5 ⁇ m, 6.0 ⁇ m, 5.5 ⁇ m, 5.4 ⁇ m, 5.3 ⁇ m, 5.2 ⁇ m, 5.1 ⁇ m, 5.0 ⁇ m, 4.9 ⁇ m, 4.8 ⁇ m, 4.7 ⁇ m, 4.6 ⁇ m, 4.5 ⁇ m, 4.4 ⁇ m, 4.3 ⁇ m, 4.2 ⁇ m, 4.1 ⁇ m, 4.0 ⁇ m, 3.9 ⁇ m, 3.8 ⁇ m 3.7 ⁇ m, 3.6 ⁇ m, 3.5 ⁇ m, 3.4 ⁇ m, 3.3 ⁇ m, 3.2 ⁇ m, 3.1 ⁇ m, 3.0 ⁇ m, 2.9 ⁇ m, 2.8 ⁇ m, 2.7 ⁇ m, 2.6 ⁇ m or less May be 2.5 ⁇ m or less.
  • the particle size of the porous polyhedron powder is within the above range, it is used in the water-in-oil cosmetic composition, and the oil absorption is great, but the adhesion to the skin is excellent.
  • the dispersibility is excellent in the manufacturing process of the water-in-oil type makeup product, the long floating time in the oil does not require strong agitation while working, the product quality is constant.
  • diffuse reflection on the particle surface is minimized, the transmitted light is minimized, so that the color is developed in a vivid color, and in the case of a light-colored lipstick, the amount of titanium dioxide is reduced, thereby producing a transparent product.
  • the porous polyhedron powder provides a water-in-oil cosmetic composition having a pore size of 50 to 1000 mm 3 on the particle surface.
  • the pore size is more than 50 ,, 60 ⁇ , 70 ⁇ , 80 ⁇ , 90 ⁇ , 100 ⁇ , 120 ⁇ , 140 ⁇ , 160 ⁇ , 180 ⁇ , 200 ⁇ , 220 ⁇ , 240 ⁇ , 26 ⁇ , 280 ⁇ , 300 ⁇ .
  • the pore size may be 1000 mW or less, 900 mW or less, 800 mW or less, 700 mW or less, 600 mW or less, 550 mW or less.
  • the porosity of the porous polyhedron powder is within the above range, so that it has excellent oil absorption function when preparing the composition, and the shape of the particles is polyhedron and the size is less than 8 ⁇ m, so that it adheres well to the skin while absorbing sebum. The effect is excellent.
  • the porous polyhedron powder may have a pore distribution of 0.9 ⁇ 2.5 cc / g.
  • the pore distribution is the volume of air contained in 1 g of the porous polyhedron powder.
  • the porous polyhedron powder has a pore distribution of at least 0.9 cc / g, at least 1.0 cc / g, at least 1.1 cc / g, at least 1.2 cc / g, at least 1.3 cc / g, at least 1.4 cc / g , 1.5 cc / g or more, 1.51 cc / g or more, 1.52 cc / g or more, 1.53 cc / g or more, 1.54 cc / g or more, 1.55 cc / g or more, 1.56 cc / g or more, 1.57 cc / g or more, 1.58 cc / g or more, 1.59 cc / g or more, 1.60 cc / g or more, 1.61 cc / g or more, 1.62 cc / g or more, 1.63 ccc / g or more
  • the porous polyhedron powder has a pore distribution of 2.5 cc / g or less, 2.4 cc / g or less, 2.3 cc / g or less, 2.2 cc / g or less, 2.1 cc / g or less, 2.0 cc / g or less, 1.9 cc / g Or less, 1.89 cc / g or less, 1.88 cc / g or less, 1.87 cc / g or less, 1.86 cc / g or less, 1.85 cc / g or less, 1.84 cc / g or less, 1.83 cc / g or less, 1.82 cc / g or less, 1.81 cc / g or less, 1.80 cc / g or less, 1.79 cc / g or less, 1.78 cc / g or less, 1.77 cc / g or less,
  • the pore distribution of the porous polyhedron powder is within the above range, the oil absorption in the preparation of the water-in-oil type cosmetic composition is great, and the adhesion to the skin is excellent.
  • the porous polyhedron powder provides a water-in-oil cosmetic composition is a powder containing any one or more of silica powder and boron nitride powder.
  • the porous polyhedron powder may be a porous polyhedral fine silica powder.
  • the porous polyhedral powder with respect to the total composition is at least 1.0 wt%, at least 1.5 wt%, at least 2.0 wt%, at least 2.5 wt%, at least 3.0 wt%, at least 3.5 wt%, at least 4.0 wt% , At least 4.5 wt%, at least 5.0 wt%, at least 5.5 wt%, at least 6.0 wt%, at least 6.5 wt%, at least 7.0 wt%, at least 7.5 wt%, at least 8.0 wt%, at least 8.5 wt%, at least 9.0 wt% , At least 9.5 wt%, at least 10.0 wt%, or at least 11 wt%.
  • the porous polyhedron powder is 20 wt% or less, 19 wt% or less, 18 wt% or less, 17 wt% or less, 16 wt% or less, 15 wt% or less, 14 wt% or less, and 13 wt% or less based on the total composition. , 12 wt% or less, 11 wt% or less, 10 wt% or less, 9 wt% or less, or 8 wt% or less.
  • the content of the porous polyhedron powder is within the above range, the oil absorption in the preparation of the water-in-oil type cosmetic composition is great, but also excellent adhesion when applied to the skin.
  • the water phase relative to the total composition is at least 5%, at least 6%, at least 7%, at least 8%, at least 9%, at least 10%, at least 11%, 12 Or at least 13 wt%, at least 14 wt%, at least 15 wt%, at least 16 wt%, at least 17 wt%, at least 18 wt%, at least 19 wt% or at least 20 wt%.
  • the total weight of the water phase is 25% by weight, 24% by weight, 23% by weight, 22% by weight, 21% by weight, 20% by weight, 19% by weight, 18% by weight, 17 It may be up to 16% by weight or up to 15% by weight.
  • the skin moisturizing power is excellent when the composition is applied to the skin, and the cooling effect is excellent.
  • a method for producing a water-in-oil cosmetic composition comprising the steps of mixing the oil phase and the amphipathic porous polyhedron to produce an oil phase mixture; It provides a water-in-oil type cosmetic composition comprising a; and mixing by adding an aqueous phase to the oil-based mixture.
  • a lipstick or gloss comprising the water-in-oil cosmetic composition.
  • the cosmetic composition is not particularly limited in formulation, and may be appropriately selected as desired.
  • Lotion, Milk Lotion, Moisture Lotion, Nutrition Lotion, Massage Cream, Nutrition Cream, Moisture Cream, Hand Cream, Foundation, Essence, Nutrition Essence, Pack, Soap, Cleansing Foam, Cleansing Lotion, Cleansing Cream, Lipstick, Gloss It may be prepared in any one or more formulations selected from the group consisting of, body lotion and body cleanser, but is not limited thereto.
  • the content of the composition is oil phase (40% by weight of hydrogenated polyisobutene, 15% by weight of dimethicone, 10% by weight of octyldodecyl neopentanoate, 6% by weight of dextrin palmitate, 9% by weight of octyldodecanol, phenyltri 5% by weight of methicone), 85% by weight, 10% by weight of aqueous phase (distilled water) and 5% by weight of polyhedral porous silica powder.
  • the pore distribution of the porous silica powder is 1.7 ⁇ 0.1 cc / g, the surface having both lipophilic and hydrophilic properties is maximized to a porosity (particle distribution having a pore size of 100 to 500 ⁇ or more than 95% of the total), The particle distribution having a particle size of 3 to 4 ⁇ m is 95% or more of the whole.
  • the oil phase and the silica powder were warmed and mixed at 95 ° C, and then cooled to 80 ° C.
  • the aqueous phase cooled to 80 ° C in advance was added and mixed for 15 minutes with a homogenizer. After 10 minutes, the mixture was cooled and degassed to remove air bubbles, thereby preparing a water-in-oil cosmetic composition containing a porous polyhedral silica powder.
  • a water-in-oil cosmetic composition was prepared in the same manner as in Example 1, except that Comparative Example 1 had an oil phase of 100% by weight, and Comparative Example 2 used HDK H13L manufactured by WACKER SILICONES instead of polyhedral porous silica powder.
  • Example 1 and Comparative Examples 1 to 2 are shown in Table 1.
  • Comparative Example 1 A 100% oil composition Comparative Example 2 B 85% oil, 10% moisture, 5% spherical porus silica powder
  • Example 1 C 85% by weight of oil, 10% by weight of water, 5% by weight of polyhedral porus silica powder
  • Comparative Example 2 and Example 1 showed a refreshing feeling due to moisture, while A gave a conventional rough coating.
  • the difference in the usability of the comparative example 2 and the example 1 is understood to be largely determined by the silica powder.
  • Comparative Example 2 (B) is a form in which the water is forcibly loosened in the oil phase somewhat unstable as shown in the photograph, and there is a possibility that it may be aggregated over time, Example 1 (C) was not observed directly under the microscope, It was confirmed that the net structure was closely dispersed. Therefore, it was confirmed that Example 1 is more excellent in moisture stability than Comparative Example 2.

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KR102114277B1 (ko) * 2018-08-23 2020-05-22 주식회사 매스컨 고체 화장품 조성물 및 그 제조방법
KR102253136B1 (ko) * 2018-11-01 2021-05-17 주식회사 엘지생활건강 윤기 지속형 화장료 조성물
KR102151804B1 (ko) * 2020-01-08 2020-09-03 에이스틴 주식회사 비(非)계면활성제형 오일-물(o/w) 분산 조성물, 비(非)계면활성제형 물-오일(w/o) 분산 조성물 및 이들의 제조방법
KR102151802B1 (ko) * 2020-01-08 2020-09-03 에이스틴 주식회사 비(非)계면활성제형 오일-물(o/w) 분산 조성물, 비(非)계면활성제형 물-오일(w/o) 분산 조성물 및 이들의 제조방법
KR102151803B1 (ko) * 2020-01-08 2020-09-03 에이스틴 주식회사 비(非)계면활성제형 오일-물(o/w) 분산 조성물, 비(非)계면활성제형 물-오일(w/o) 분산 조성물 및 이들의 제조방법
KR102622118B1 (ko) * 2021-09-30 2024-01-08 주식회사 엘지생활건강 투명한 유중수형 입술용 화장료 조성물
CN116589453A (zh) * 2023-05-30 2023-08-15 广州丽康堂生物科技有限公司 一种抗氧化精华液及其制备方法

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