WO2016033932A1 - 蒸镀坩埚和蒸镀装置 - Google Patents
蒸镀坩埚和蒸镀装置 Download PDFInfo
- Publication number
- WO2016033932A1 WO2016033932A1 PCT/CN2015/071101 CN2015071101W WO2016033932A1 WO 2016033932 A1 WO2016033932 A1 WO 2016033932A1 CN 2015071101 W CN2015071101 W CN 2015071101W WO 2016033932 A1 WO2016033932 A1 WO 2016033932A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- crucible
- thermally conductive
- vapor deposition
- heat
- receiving cavity
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Ceased
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Classifications
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/22—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
- C23C14/24—Vacuum evaporation
- C23C14/243—Crucibles for source material
Definitions
- the present invention relates to the field of manufacturing technology of display devices, and in particular to an evaporation crucible and an evaporation device including the vapor deposition crucible.
- OLED organic light-emitting diode
- LTPS low temperature poly-silicon
- FMM high-precision metal mask
- FIG. 1 is a schematic structural view of a conventional vapor deposition crucible.
- the tantalum body 10 of the vapor-deposited crucible body is made of titanium (Ti), which results in poor temperature uniformity of the vapor-deposited crucible after heating, thereby making the evaporation uniformity of the vapor deposition material poor;
- the inside of the plating material is relatively slow due to the distance from the inner wall of the vapor deposition crucible, and the outer portion of the vapor deposition material directly contacting the inner wall is heated faster, causing some materials to not evaporate, and the other portion is excessively denatured by heat, thereby causing the material to be Waste and affect the evaporation effect.
- the present invention provides an evaporation crucible comprising a crucible body, the crucible body having a receiving cavity formed thereon, the vapor deposition crucible further comprising a heat conducting layer disposed on an inner wall of the crucible body The material is surrounded to surround the accommodating cavity, and the material of the heat conducting layer is made to have a thermal conductivity higher than that of the material from which the dam body is made.
- the material from which the crucible body is made comprises titanium or a titanium alloy
- the material from which the thermally conductive layer is made includes any one or more of copper, copper alloy, silver, and silver alloy.
- the vapor deposition crucible further comprises a heat conducting structure disposed in the receiving cavity, The heat conducting structure is connected to the heat conducting layer, and when the vapor deposition material is placed in the receiving cavity, the vapor deposition material is at least in contact with a portion of the heat conducting structure, and when the vapor deposition crucible is heated, The thermally conductive structure does not prevent the vapor deposition material from escaping from the open side of the receiving chamber.
- the heat conducting structure comprises a plurality of thermally conductive partitions, and the plurality of thermally conductive partitions divide the receiving cavity into a plurality of sub-cavities formed with openings.
- the plurality of thermally conductive spacers comprise at least one first spacer, the first spacer extending along a length of the receiving cavity, and/or
- the plurality of thermally conductive spacers includes at least one second spacer extending in a width direction of the receiving cavity.
- the plurality of thermally conductive spacers comprise a plurality of first spacers and a plurality of second spacers.
- the heat conducting structure comprises at least one heat conducting mesh that divides the receiving cavity into a plurality of sub-cavities along a depth direction of the receiving cavity.
- the heat conducting structure comprises a plurality of the heat conducting meshes arranged in a depth direction of the receiving cavity.
- the material from which the thermally conductive structure is made is the same as the material from which the thermally conductive layer is made.
- the present invention also provides an evaporation apparatus comprising the above-described vapor deposition crucible.
- the inner wall of the crucible body is provided with a heat conductive layer having a large thermal conductivity, when the temperature of the heat generated by the crucible body is not uniform, the heat conducting layer can rapidly and uniformly diffuse heat, thereby making the entire heat conducting layer The temperature is more uniform, and the vapor deposition material is uniformly heated.
- a heat conducting structure may be further disposed in the receiving cavity, and the heat conducting structure is connected to the heat conducting layer to quickly transfer heat to the inside of the vapor deposition material. In this way, different regions of the vapor deposition material in the vapor deposition crucible can be uniformly heated, thereby reducing the occurrence of material denaturation due to temperature unevenness and improving the vapor deposition effect.
- FIG. 1 is a schematic structural view of a vapor deposition crucible in the prior art
- FIG. 2 is a schematic structural view of an evaporating crucible according to a first embodiment of the present invention
- Figure 3 is a plan view of the vapor deposition crucible shown in Figure 2;
- FIG. 4 is a schematic structural view of an evaporating crucible according to a second embodiment of the present invention.
- Fig. 5 is a plan view of the vapor deposition crucible shown in Fig. 4.
- the vapor deposition crucible of the present invention includes a crucible body 10 on which a housing chamber 30 is formed.
- the vapor-deposited crucible of the present invention further includes a heat-conducting layer 11 which is disposed on the inner wall of the crucible body 10 to surround the accommodation chamber 30, and the material of which the heat-conducting layer 11 is made has a thermal conductivity higher than that of the material from which the crucible body 10 is made. rate.
- the manner in which the heat conductive layer 11 is provided on the inner wall of the crucible body 10 is not particularly limited.
- a material having a large thermal conductivity may be directly applied to the inner wall of the crucible body 10 to form the heat conductive layer 11 by using a plating layer or the like; or, a material having a large thermal conductivity may be preliminarily formed to conform to the shape of the receiving chamber.
- the heat conducting layer 11 is then nested within the receiving cavity.
- the vapor deposition crucible when the vapor deposition crucible is heated, since the inner wall of the crucible body 10 is provided with the heat conduction layer 11 having a large thermal conductivity, heat can be quickly transferred to the evaporation chamber in the accommodation chamber 30 through the heat conduction layer 11. material. In this way, different regions of the vapor deposition material in the vapor deposition crucible can be uniformly heated, thereby reducing the occurrence of material denaturation due to temperature unevenness, thereby improving the vapor deposition effect.
- the crucible body 10 will have a higher temperature region and temperature after being heated. Low area. Since the heat-conducting layer 11 having a large thermal conductivity is disposed on the crucible body 10, heat in the region of the crucible body 10 at a higher temperature is more transmitted to the heat-conducting layer 11. The heat conducting layer 11 can quickly diffuse the heat transferred from the higher temperature region, so that the temperature of the entire heat conducting layer 11 is relatively uniform, thereby achieving the purpose of uniformly heating the vapor deposition material.
- the material from which the crucible body 10 is made may include titanium or a titanium alloy (for example, TC 4 ) to make the vapor-deposited crucible have greater heat resistance.
- the material from which the heat conductive layer 11 is made may include any one or more of copper, copper alloy, silver, and silver alloy.
- the material from which the heat conductive layer 11 is made may be other materials as long as the material has a large thermal conductivity and does not react with the vapor deposition material.
- the vapor deposition crucible may further include a heat conductive structure disposed in the accommodation chamber 30.
- the heat conducting structure is connected to the heat conducting layer 11.
- a part of the vapor deposition material may be in contact with the heat conductive structure, and when the ruthenium is heated, the vapor deposition material may be The inside of the accommodating chamber 30 escapes. It can be seen that the thermally conductive structure does not prevent the vapor deposition material from escaping from the open side of the receiving chamber 30.
- the specific form of the heat conducting structure is not limited in the present invention as long as heat can be transferred from the heat conducting layer 11 to the inside of the vapor deposition material without impeding evaporation of the vapor deposition material.
- the thermally conductive structure may include a plurality of thermally conductive wires, thermally conductive rods or thermally conductive plates connected to the thermally conductive layer 11. When the vapor deposition material is placed in the accommodating chamber 30, the heat conductive structure may pass through the inside of the vapor deposition material to rapidly transfer heat to the inside of the vapor deposition material.
- the heat conductive structure can be regarded as an extended portion of the heat conductive layer, and the heat conductive structure is provided for the purpose of increasing the contact area with the vapor deposition material, thereby heating the vapor deposition material more quickly and uniformly.
- the thermally conductive structure can include a plurality of thermally conductive separators 12.
- a plurality of thermally conductive partitions 12 divide the receiving chamber 30 into a plurality of sub-cavities 13 formed with openings such that vapor deposition material placed in the plurality of sub-cavities 13 can escape from the openings.
- the heat conducting partition 12 is connected to the heat conducting layer 11 to transfer heat into the plurality of sub-cavities 13.
- the evaporation material is divided into portions to make the temperature of the evaporation material more uniform.
- the evaporation material is uniformly distributed in each of the sub-cavities 13.
- the plurality of thermally conductive spacers 12 may include at least one first spacer 121 extending along the length of the receiving cavity, and/or a plurality of thermally conductive spacers 12 At least one second partition 122 is included, and the second partition 122 extends in the width direction of the accommodating chamber.
- the plurality of thermally conductive spacers 12 include a plurality of first spacers 121 and a plurality of second spacers 122, and the plurality of first spacers 121 and the plurality of second spacers 122
- the accommodating chamber 30 is partitioned into a plurality of sub-cavities 13.
- the top of the sub-cavity 13 is formed with an opening from which the vapor deposition material can escape when heated.
- the thermally conductive structure may include at least one thermally conductive mesh 20 that divides the receiving cavity 30 into a plurality of sub-cavities along a depth direction of the receiving cavity. .
- the heat conductive mesh can divide the accommodating cavity 30 into two upper and lower sub-cavities.
- Figure 5 shows a top view of an evaporating crucible provided with a heat conducting mesh 20. The evaporation material can escape from the mesh of the heat transfer mesh 20.
- the heat conductive mesh 20 is preferably disposed at a lower portion of the accommodating cavity 30 such that the vapor deposition material in the accommodating cavity may cover the heat conductive mesh 20 (in other words, the heat conductive mesh 20 is located inside the vapor deposition material) Thereby, the heat of the heat transfer mesh 20 is transferred to the inside of the vapor deposition material. In this manner, the inside and the outside of the vapor-deposited material can be simultaneously heated by the heat-conducting layer 11 and the heat-conducting mesh 20, thereby making the temperature of the vapor-deposited material uniform.
- the heat conducting structure includes a plurality of heat conducting meshes 20 arranged along the depth direction of the receiving cavity 30.
- the plurality of heat conductive webs 20 may be arranged in an equally spaced manner or may be arranged in other ways. It should be understood that the evaporation material within the containment chamber 30 covers at least one of the heat transfer webs 20.
- the plurality of heat transfer webs 20 can uniformly transfer heat to the inside of the vapor deposition material.
- the plurality of heat transfer webs 20 can improve the temperature uniformity of the vapor deposition material and improve the vapor deposition effect.
- the material for forming the heat-conducting structure may be the same as the material for forming the heat-conducting layer 11, and is a material having a large thermal conductivity, so as to quickly transfer heat to the inside of the vapor-deposited material to improve temperature uniformity.
- the material of the heat conducting structure can be made Any one or more of copper, copper alloy, silver, and silver alloy are included.
- the vapor deposition crucible provided by the present invention has been described above. It can be seen that since the inner wall of the crucible body is provided with a heat conducting layer having a large thermal conductivity, when the heating temperature of the crucible body is not uniform, the heat conducting layer can rapidly and uniformly diffuse heat, thereby making the temperature of the entire heat conducting layer more. Evenly, the vapor deposition material is uniformly heated.
- a heat conducting structure may be further disposed in the receiving cavity, and the heat conducting structure is connected to the heat conducting layer to quickly transfer heat to the inside of the vapor deposition material. In this way, different regions of the vapor deposition material in the vapor deposition crucible can be uniformly heated, thereby reducing the occurrence of material denaturation due to temperature unevenness and improving the vapor deposition effect.
- an evaporation apparatus includes the above-described vapor deposition crucible provided by the present invention.
- the evaporation apparatus may include a vacuum chamber in which the vapor deposition chamber is disposed. Since the vapor deposition apparatus has the above-described vapor deposition crucible, the vapor deposition apparatus of the present invention can also achieve a better vapor deposition effect.
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Physical Vapour Deposition (AREA)
Abstract
Description
Claims (10)
- 一种蒸镀坩埚,包括坩埚本体,所述坩埚本体上形成有容纳腔,其特征在于,所述蒸镀坩埚还包括导热层,所述导热层设置在所述坩埚本体的内壁上以包围所述容纳腔,并且制成所述导热层的材料的热传导率大于制成所述坩埚本体的材料的热传导率。
- 根据权利要求1所述的蒸镀坩埚,其特征在于,制成所述坩埚本体的材料包括钛或钛合金,制成所述导热层的材料包括铜、铜合金、银和银合金中的任一种或几种材料。
- 根据权利要求1或2所述的蒸镀坩埚,其特征在于,所述蒸镀坩埚还包括设置在所述容纳腔内的导热结构,所述导热结构与所述导热层相连,当蒸镀材料放置在所述容纳腔内时,所述蒸镀材料至少与所述导热结构的一部分接触,并且在加热所述蒸镀坩埚时,所述导热结构不会妨碍所述蒸镀材料从所述容纳腔的敞开侧逸出。
- 根据权利要求3所述的蒸镀坩埚,其特征在于,所述导热结构包括多个导热隔板,多个所述导热隔板将所述容纳腔分隔成多个形成有开口的子腔体。
- 根据权利要求4所述的蒸镀坩埚,其特征在于,所述多个导热隔板包括至少一个第一隔板,所述第一隔板沿所述容纳腔的长度方向延伸,和/或所述多个导热隔板包括至少一个第二隔板,所述第二隔板沿所述容纳腔的宽度方向延伸。
- 根据权利要求5所述的蒸镀坩埚,其特征在于,多个所述导热隔板包括多个第一隔板和多个第二隔板。
- 根据权利要求3所述的蒸镀坩埚,其特征在于,所述导热结构包括至少一个导热网,所述导热网沿所述容纳腔的深度方向将所述容纳腔分隔成多个子腔体。
- 根据权利要求7所述的蒸镀坩埚,其特征在于,所述导热结构包括沿所述容纳腔的深度方向排列的多个所述导热网。
- 根据权利要求3所述的蒸镀坩埚,其特征在于,制成所述导热结构的材料与制成所述导热层的材料相同。
- 一种蒸镀装置,其特征在于,所述蒸镀装置包括权利要求1至9中任意一项所述的蒸镀坩埚。
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US14/762,109 US20160251750A1 (en) | 2014-09-01 | 2015-01-20 | An evaporating crucible and an evaporating device |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410440677.7A CN104233196B (zh) | 2014-09-01 | 2014-09-01 | 蒸镀坩埚和蒸镀装置 |
| CN201410440677.7 | 2014-09-01 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| WO2016033932A1 true WO2016033932A1 (zh) | 2016-03-10 |
Family
ID=52222076
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PCT/CN2015/071101 Ceased WO2016033932A1 (zh) | 2014-09-01 | 2015-01-20 | 蒸镀坩埚和蒸镀装置 |
Country Status (3)
| Country | Link |
|---|---|
| US (1) | US20160251750A1 (zh) |
| CN (1) | CN104233196B (zh) |
| WO (1) | WO2016033932A1 (zh) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104233196B (zh) * | 2014-09-01 | 2017-04-19 | 京东方科技集团股份有限公司 | 蒸镀坩埚和蒸镀装置 |
| CN104694883A (zh) * | 2015-03-27 | 2015-06-10 | 京东方科技集团股份有限公司 | 一种坩埚 |
| CN104831237B (zh) * | 2015-05-25 | 2017-02-22 | 京东方科技集团股份有限公司 | 一种蒸镀装置和蒸镀系统 |
| CN105112855A (zh) * | 2015-09-29 | 2015-12-02 | 京东方科技集团股份有限公司 | 蒸镀坩埚和蒸镀系统 |
| CN106025102A (zh) * | 2016-05-27 | 2016-10-12 | 京东方科技集团股份有限公司 | 一种蒸镀坩埚 |
| CN108914068A (zh) * | 2018-08-02 | 2018-11-30 | 京东方科技集团股份有限公司 | 坩埚和蒸镀装置 |
| CN109136855B (zh) * | 2018-09-05 | 2021-03-02 | 京东方科技集团股份有限公司 | 一种蒸发源及蒸镀装置 |
| CN109898059A (zh) * | 2019-04-15 | 2019-06-18 | 湖畔光电科技(江苏)有限公司 | 一种新型蒸镀坩埚装置 |
| US20230279536A1 (en) * | 2021-01-07 | 2023-09-07 | Ulvac, Inc. | Vapor deposition source for vacuum vapor deposition apparatus |
| CN118600373B (zh) * | 2024-07-11 | 2025-06-06 | 国鲸合创(青岛)科技有限公司 | 大面积蒸发舟 |
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| FI20085547A0 (fi) * | 2008-06-04 | 2008-06-04 | Dca Instr Oy | Höyrystyslaite, höyrystysupokas sekä menetelmä kalvon kasvattamiseksi substraatin pinnalle |
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-
2014
- 2014-09-01 CN CN201410440677.7A patent/CN104233196B/zh not_active Expired - Fee Related
-
2015
- 2015-01-20 WO PCT/CN2015/071101 patent/WO2016033932A1/zh not_active Ceased
- 2015-01-20 US US14/762,109 patent/US20160251750A1/en not_active Abandoned
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| CN1606632A (zh) * | 2001-12-18 | 2005-04-13 | 高级技术材料公司 | 用于挥发性/热敏感固体和液体化合物的蒸发器/输送容器 |
| CN101268210A (zh) * | 2005-09-20 | 2008-09-17 | 国立大学法人东北大学 | 成膜装置、蒸发夹具及测定方法 |
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| CN104233196A (zh) * | 2014-09-01 | 2014-12-24 | 京东方科技集团股份有限公司 | 蒸镀坩埚和蒸镀装置 |
Also Published As
| Publication number | Publication date |
|---|---|
| CN104233196B (zh) | 2017-04-19 |
| US20160251750A1 (en) | 2016-09-01 |
| CN104233196A (zh) | 2014-12-24 |
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