WO2014104393A8 - Procédé de fabrication d'une tôle d'acier électromagnétique à grains orientés - Google Patents

Procédé de fabrication d'une tôle d'acier électromagnétique à grains orientés Download PDF

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WO2014104393A8
WO2014104393A8 PCT/JP2013/085321 JP2013085321W WO2014104393A8 WO 2014104393 A8 WO2014104393 A8 WO 2014104393A8 JP 2013085321 W JP2013085321 W JP 2013085321W WO 2014104393 A8 WO2014104393 A8 WO 2014104393A8
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ppm
grain
mass
steel slab
oriented electrical
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PCT/JP2013/085321
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English (en)
Japanese (ja)
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WO2014104393A1 (fr
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早川 康之
之啓 新垣
山口 広
松田 広志
有衣子 脇阪
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Jfeスチール株式会社
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Priority to RU2015131084A priority Critical patent/RU2608258C1/ru
Priority to US14/650,387 priority patent/US9708682B2/en
Priority to JP2014543712A priority patent/JP5692479B2/ja
Priority to EP13869216.5A priority patent/EP2940160B1/fr
Priority to KR1020157019245A priority patent/KR101651797B1/ko
Priority to CN201380068330.8A priority patent/CN104884644B/zh
Publication of WO2014104393A1 publication Critical patent/WO2014104393A1/fr
Publication of WO2014104393A8 publication Critical patent/WO2014104393A8/fr

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  • Chemical Treatment Of Metals (AREA)

Abstract

L'invention concerne un procédé de fabrication d'une tôle d'acier électromagnétique à grains orientés utilisant, comme matière première à cette fin, une plaque en acier ayant une composition qui contient, en termes de % en masse ou de ppm en masse, jusqu'à 0,08% C, 2,0-4,5 Si et jusqu'à 0,5% Mn, a des teneurs en S, Se et O réduites à moins de 50 ppm chacune et une teneur en Al sol réduite à moins de 100 ppm, et a une teneur régulée à la plage [Al sol]x[14/27] ppm≤N≤80 ppm, le restant comprenant Fe et des impuretés inévitables, le procédé comprenant le laminage à froid de la plaque d'acier, après quoi on soumet la plaque d'acier, avant initiation de la recristallisation secondaire/recuit, à un traitement de nitruration par lequel la teneur en azote est régulée à 50-1000 ppm en masse, en incorporant un sulfure et/ou un sulfate dans un séparateur de recuit dans une quantité totale de 0,2-15% en masse, et en effectuant la recristallisation secondaire/recuit de sorte que la plaque d'acier, durant le chauffage, est maintenue pendant 5 heures ou plus dans la plage de température de 300-800°C, en précipitant de cette façon du nitrure de silicium (Si3N4) et du MnS et en utilisant le nitrure de silicium et le MnS en combinaison comme pouvoir d'inhibition de la croissance des grains normaux. Ainsi, les irrégularités de la propriété magnétique sont grandement réduites et on produit de manière stable et industrielle une tôle d'acier électromagnétique à grains orientés ayant des caractéristiques satisfaisantes.
PCT/JP2013/085321 2012-12-28 2013-12-25 Procédé de fabrication d'une tôle d'acier électromagnétique à grains orientés WO2014104393A1 (fr)

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RU2015131084A RU2608258C1 (ru) 2012-12-28 2013-12-25 Способ производства текстурированного листа из электротехнической стали
US14/650,387 US9708682B2 (en) 2012-12-28 2013-12-25 Production method for grain-oriented electrical steel sheet
JP2014543712A JP5692479B2 (ja) 2012-12-28 2013-12-25 方向性電磁鋼板の製造方法
EP13869216.5A EP2940160B1 (fr) 2012-12-28 2013-12-25 Methode de production d'une tôile d'acier électromagnétique à grains orientés
KR1020157019245A KR101651797B1 (ko) 2012-12-28 2013-12-25 방향성 전기 강판의 제조 방법
CN201380068330.8A CN104884644B (zh) 2012-12-28 2013-12-25 方向性电磁钢板的制造方法

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JP2012-288612 2012-12-28
JP2012288612 2012-12-28

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WO2014104393A1 WO2014104393A1 (fr) 2014-07-03
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EP (1) EP2940160B1 (fr)
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KR (1) KR101651797B1 (fr)
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Families Citing this family (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2014125840A1 (fr) * 2013-02-18 2014-08-21 Jfeスチール株式会社 Procédé de nitruration pour tôles d'acier électromagnétique orienté et dispositif de nitruration
JP5942885B2 (ja) * 2013-02-18 2016-06-29 Jfeスチール株式会社 方向性電磁鋼板の窒化処理方法および窒化処理装置
JP6471807B2 (ja) * 2015-09-28 2019-02-20 新日鐵住金株式会社 方向性電磁鋼板及び方向性電磁鋼板用の熱延鋼板
RU2692136C1 (ru) * 2016-02-22 2019-06-21 ДжФЕ СТИЛ КОРПОРЕЙШН Способ изготовления листа из текстурированной электротехнической стали
JP6455468B2 (ja) * 2016-03-09 2019-01-23 Jfeスチール株式会社 方向性電磁鋼板の製造方法
KR101919528B1 (ko) * 2016-12-22 2018-11-16 주식회사 포스코 방향성 전기강판 및 이의 제조방법
BR112019009604B1 (pt) * 2017-01-16 2022-08-02 Nippon Steel Corporation Chapa de aço elétrica não orientada
JP6512386B2 (ja) 2017-02-20 2019-05-15 Jfeスチール株式会社 方向性電磁鋼板の製造方法
CN110651058B (zh) * 2017-05-12 2021-09-07 杰富意钢铁株式会社 取向性电磁钢板及其制造方法
US11145446B2 (en) 2017-07-13 2021-10-12 Nippon Steel Corporation Grain-oriented electrical steel sheet
KR102044322B1 (ko) * 2017-12-26 2019-11-13 주식회사 포스코 방향성 전기강판 및 그의 제조방법
KR102164329B1 (ko) * 2018-12-19 2020-10-12 주식회사 포스코 방향성의 전기강판 및 그 제조 방법
BR112021012842A2 (pt) * 2019-01-08 2021-09-28 Nippon Steel Corporation Chapa de aço elétrico de grão orientado, método para fabricar chapa de aço elétrico de grão orientado, e, separador de recozimento usado para fabricar chapas de aço elétricos de grão orientado
MX2022002590A (es) * 2019-09-06 2022-03-25 Jfe Steel Corp Lamina de acero electrico de grano orientado y metodo de produccion de la misma.
JP2022055869A (ja) 2020-09-29 2022-04-08 株式会社日立製作所 軟磁性鉄板、該軟磁性鉄板の製造方法、該軟磁性鉄板を用いた鉄心および回転電機
CN113416901B (zh) * 2021-06-29 2022-03-01 宝武集团鄂城钢铁有限公司 一种低温韧性优异的高磁感性耐候软磁钢及其生产方法

Family Cites Families (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1965559A (en) 1933-08-07 1934-07-03 Cold Metal Process Co Electrical sheet and method and apparatus for its manufacture and test
US3333992A (en) * 1964-06-29 1967-08-01 Armco Steel Corp Production of oriented silicon-iron using grain growth inhibitor during primary recrystallization heat treatment
JPS5113469B2 (fr) 1972-10-13 1976-04-28
AT329358B (de) 1974-06-04 1976-05-10 Voest Ag Schwingmuhle zum zerkleinern von mahlgut
JPS5844152B2 (ja) * 1978-12-27 1983-10-01 川崎製鉄株式会社 下地被膜をほとんど有しない方向性珪素鋼板の製造方法
JPS6474817A (en) 1987-09-17 1989-03-20 Asahi Glass Co Ltd Ultrasonic delay line
JPH0230740A (ja) * 1988-04-23 1990-02-01 Nippon Steel Corp 鉄損の著しく優れた高磁束密度一方向性電磁鋼板及びその製造方法
EP0392534B1 (fr) * 1989-04-14 1998-07-08 Nippon Steel Corporation Procédé de fabrication de tÔles d'acier électrique à grains orientés ayant des propriétés magnétiques supérieures
JP2782086B2 (ja) 1989-05-29 1998-07-30 新日本製鐵株式会社 磁気特性、皮膜特性ともに優れた一方向性電磁鋼板の製造方法
JPH06158167A (ja) * 1992-11-19 1994-06-07 Nippon Steel Corp 高磁束密度方向性電磁鋼板およびその製造法
US5643370A (en) * 1995-05-16 1997-07-01 Armco Inc. Grain oriented electrical steel having high volume resistivity and method for producing same
JP3415377B2 (ja) * 1996-11-13 2003-06-09 Jfeスチール株式会社 極めて鉄損の低い高磁束密度方向性電磁鋼板の製造方法
IT1290172B1 (it) 1996-12-24 1998-10-19 Acciai Speciali Terni Spa Procedimento per la produzione di lamierino magnetico a grano orientato, con elevate caratteristiche magnetiche.
IT1290171B1 (it) * 1996-12-24 1998-10-19 Acciai Speciali Terni Spa Procedimento per il trattamento di acciaio al silicio, a grano orientato.
JP3707268B2 (ja) 1998-10-28 2005-10-19 Jfeスチール株式会社 方向性電磁鋼板の製造方法
US6309473B1 (en) * 1998-10-09 2001-10-30 Kawasaki Steel Corporation Method of making grain-oriented magnetic steel sheet having low iron loss
JP4123653B2 (ja) * 1999-10-12 2008-07-23 Jfeスチール株式会社 方向性電磁鋼板の製造方法
EP1279747B1 (fr) * 2001-07-24 2013-11-27 JFE Steel Corporation Procédé pour la fabrication de tôles d'acier électrique à grains orientés
JP4258349B2 (ja) * 2002-10-29 2009-04-30 Jfeスチール株式会社 方向性電磁鋼板の製造方法
JP4501655B2 (ja) * 2004-11-29 2010-07-14 Jfeスチール株式会社 方向性電磁鋼板の製造方法
JP4714637B2 (ja) 2006-05-24 2011-06-29 新日本製鐵株式会社 磁束密度の高い方向性電磁鋼板の製造方法
JP5419459B2 (ja) * 2006-11-22 2014-02-19 新日鐵住金株式会社 被膜密着性に優れた一方向性電磁鋼板およびその製造法
US8303730B2 (en) * 2008-09-10 2012-11-06 Nippon Steel Corporation Manufacturing method of grain-oriented electrical steel sheet
EP2455498B1 (fr) * 2009-07-17 2019-03-27 Nippon Steel & Sumitomo Metal Corporation Procédé de fabrication d'une tôle d'acier magnétique á grains orientés
JP5994981B2 (ja) * 2011-08-12 2016-09-21 Jfeスチール株式会社 方向性電磁鋼板の製造方法

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EP2940160A1 (fr) 2015-11-04
KR101651797B1 (ko) 2016-08-26
JPWO2014104393A1 (ja) 2017-01-19
JP5692479B2 (ja) 2015-04-01
CN104884644A (zh) 2015-09-02
WO2014104393A1 (fr) 2014-07-03
US9708682B2 (en) 2017-07-18
EP2940160B1 (fr) 2017-02-01
KR20150095911A (ko) 2015-08-21
US20150299819A1 (en) 2015-10-22
RU2608258C1 (ru) 2017-01-17
CN104884644B (zh) 2017-03-15
EP2940160A4 (fr) 2016-04-06

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