WO2014083957A1 - Agent de traitement et procédé de traitement pour stimuler l'adhérence entre des poils artificiels et des poils naturels - Google Patents

Agent de traitement et procédé de traitement pour stimuler l'adhérence entre des poils artificiels et des poils naturels Download PDF

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Publication number
WO2014083957A1
WO2014083957A1 PCT/JP2013/078131 JP2013078131W WO2014083957A1 WO 2014083957 A1 WO2014083957 A1 WO 2014083957A1 JP 2013078131 W JP2013078131 W JP 2013078131W WO 2014083957 A1 WO2014083957 A1 WO 2014083957A1
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Prior art keywords
hair
present
artificial
treatment
artificial hair
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PCT/JP2013/078131
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English (en)
Japanese (ja)
Inventor
並木秀男
菊田敏輝
澤寛
岩男和子
佐野郁子
原桜子
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株式会社フロンティア
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Publication of WO2014083957A1 publication Critical patent/WO2014083957A1/fr

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    • A—HUMAN NECESSITIES
    • A41—WEARING APPAREL
    • A41G—ARTIFICIAL FLOWERS; WIGS; MASKS; FEATHERS
    • A41G5/00—Hair pieces, inserts, rolls, pads, or the like; Toupées
    • A41G5/02—Artificial eyelashes; Artificial eyebrows
    • A—HUMAN NECESSITIES
    • A41—WEARING APPAREL
    • A41G—ARTIFICIAL FLOWERS; WIGS; MASKS; FEATHERS
    • A41G5/00—Hair pieces, inserts, rolls, pads, or the like; Toupées
    • A41G5/004—Hair pieces
    • A41G5/0053—Fastening thereof
    • A41G5/008—Fastening thereof by adhesives

Definitions

  • the present invention relates to a treating agent and a treating method for increasing the adhesion between artificial hair and ground hair containing a reducing agent as an active ingredient.
  • the false eyelashes are typically manufactured from synthetic fibers, and various adhesives can be used to adhere the false eyelashes to the ground hair.
  • various types of adhesives ranging from safe and mild types used in human surgery to strong adhesives such as instant adhesives, but strong types.
  • Instant adhesives, such as Aron Alpha®, will adhere well, but may cause adverse events during use.
  • Patent Document 1 a preparation for improving the adhesion between ground hair and artificial hair is disclosed.
  • this preparatory agent contains polyvinylpyrrolidone (PVP), polyacrylate, ethanol, and the like, and is used to remove eyebrows oil, moisture, dust, and salt.
  • PVP polyvinylpyrrolidone
  • the present inventors have found that false eyelashes made of synthetic fibers strongly adhere to each other using any adhesive, but the adhesion between the eyelashes-lashes and the eyelashes-false eyelashes is very weak. I found it. This finding indicates that if the surface of the eyelashes is modified (treated), the false eyelashes can adhere strongly to the eyelashes. Accordingly, the present inventors have completed the present invention relating to a treatment agent containing a reducing agent as an active ingredient and a treatment method for increasing the adhesion between artificial hair and ground hair.
  • the present invention provides a treating agent for increasing the adhesion between artificial hair and ground hair, which contains a reducing agent as an active ingredient.
  • the reducing agent may be selected from one or more types from the group consisting of thioglycolic acid, cysteine, and salts thereof.
  • the artificial hair may be eyebrows, eyelashes, and / or artificial hair for head hair.
  • the artificial hair may contain a polyester polymer.
  • the base hair may be eyebrows, eyelashes, and / or hair.
  • the present invention provides a step of preparing the treatment agent; Brushing the bristles and / or treating the bristles with the treatment agent; Washing the bristles; A treatment method for increasing adhesion between artificial hair and ground hair, comprising the step of drying the ground hair.
  • the treatment method of the present invention may further include a step of adhering artificial hair to the base hair using an adhesive.
  • the adhesive may be a cyanoacrylate adhesive.
  • the artificial hair may be eyebrows, eyelashes, and / or artificial hair for head hair.
  • the artificial hair may contain a polyester polymer.
  • the ground hair may be eyebrows, eyelashes, and / or hair.
  • the present invention provides a composition for treatment for increasing the adhesion between artificial hair and ground hair containing a reducing agent as an active ingredient.
  • the reducing agent may be selected from one or more groups selected from the group consisting of thioglycolic acid, cysteine, and salts thereof.
  • the artificial hair may be eyebrows, eyelashes, and / or artificial hair for head hair.
  • the artificial hair may contain a polyester polymer.
  • the base hair may be eyebrows, eyelashes, and / or hair.
  • the present invention provides a compound selected from the group consisting of thioglycolic acid, cysteine, and salts thereof for treatment to increase the adhesion between artificial hair and ground hair.
  • the artificial hair may be eyebrows, eyelashes, and / or artificial hair for head hair.
  • the artificial hair may contain a polyester polymer.
  • the base hair may be eyebrows, eyelashes, and / or head hair.
  • the present invention provides the use of a reducing agent as an active ingredient of a treatment composition for increasing the adhesion between artificial hair and ground hair.
  • the reducing agent may be selected from one or more types from the group consisting of thioglycolic acid, cysteine, and salts thereof.
  • the artificial hair may be eyebrows, eyelashes, and / or artificial hair for head hair.
  • the artificial hair may contain a polyester polymer.
  • the base hair may be eyebrows, eyelashes, and / or head hair.
  • the present invention also provides a treatment for increasing the adhesion between artificial hair and ground hair of a compound selected from one or more compounds selected from the group consisting of thioglycolic acid, cysteine, and salts thereof. Provide use.
  • the artificial hair may be eyebrows, eyelashes, and / or artificial hair for head hair.
  • the artificial hair may contain a polyester polymer.
  • the base hair may be eyebrows, eyelashes, and / or head hair.
  • the present invention provides the use of a reducing agent to produce a treatment composition for increasing the adhesion between artificial hair and ground hair.
  • the reducing agent may be selected from one or more types from the group consisting of thioglycolic acid, cysteine, and salts thereof.
  • the artificial hair may be eyebrows, eyelashes and / or artificial hair for head hair.
  • the artificial hair may contain a polyester polymer.
  • the ground hair may be eyebrows, eyelashes, and / or hair.
  • the present invention provides a treatment composition for increasing the adhesion between artificial hair and ground hair, containing a reducing agent as an active ingredient and further containing one or more additives.
  • the reducing agent is one kind from the group consisting of thioglycolic acid, cysteine, and salts thereof, or Two or more types may be selected.
  • the artificial hair may be eyebrows, eyelashes, and / or artificial hair for hair.
  • the artificial hair may contain a polyester polymer.
  • the ground hair may be eyebrows, eyelashes, and / or hair.
  • the present invention comprises a step of preparing the treatment composition; Brushing the bristles and / or treating the bristles with the treatment agent; Washing the bristles; A treatment method for increasing adhesion between artificial hair and ground hair, comprising the step of drying the ground hair.
  • the treatment method using the composition of the present invention may further include a step of adhering artificial hair to the base hair using an adhesive.
  • the adhesive may be a cyanoacrylate adhesive.
  • the artificial hair may be eyebrows, eyelashes, and / or artificial hair for head hair.
  • the artificial hair may contain a polyester polymer.
  • the ground hair may be eyebrows, eyelashes, and / or hair.
  • the hair treated with a reducing agent for example, thioglycolic acid, cysteine
  • a reducing agent for example, thioglycolic acid, cysteine
  • the adhesion between the base hair and the artificial hair can be increased synergistically by combining the base hair with a treatment agent and brushing the base hair.
  • FIG. 2 is a typical chart showing the adhesive strength of untreated hair-polyester fibers (the oblique lines are attached after the measurement of the adhesive strength to show the waveform chart portion where the integrated value of the adhesive strength is calculated).
  • the vertical axis represents the adhesive force (N), and the horizontal axis represents the stroke (mm).
  • FIG. 3 is a representative chart showing the adhesive strength of treated hair-polyester fibers (the oblique lines are attached after the measurement of the adhesive strength to show the waveform chart portion where the integrated value of the adhesive strength is calculated).
  • the vertical axis represents the adhesive force (N), and the horizontal axis represents the stroke (mm).
  • the graph which shows the maximum value of the adhesive force in an untreated hair-polyester fiber and a treated hair-polyester fiber.
  • the vertical axis represents the maximum value (N) of the adhesive force
  • the horizontal axis represents each experimental condition.
  • the graph which shows the adhesive strength of untreated hair-polyester fiber, and the adhesive strength of treated hair-polyester fiber.
  • the vertical axis represents the adhesive strength (N ⁇ mm), and the horizontal axis represents each experimental condition.
  • the graph which shows the adhesive force of hair and false eyelashes.
  • the vertical axis represents the adhesive strength (Newton (N)), and the horizontal axis represents each experimental condition.
  • the error bar for each experimental condition indicates the standard deviation of the measured value of the experimental result repeated 10 to 20 times under the same condition.
  • the “treatment agent” refers to a compound for changing the physical and / or chemical properties of artificial hair such as for eyebrows, eyelashes and / or head hair, or a composition containing the compound.
  • composition refers to a product or a mixture containing a plurality of types of specific components.
  • the specific component is a specific active ingredient and / or a specific additive, and is included in the product or mixture in a specific amount or proportion, but is not limited thereto.
  • reducing agent refers to a compound capable of reductively cleaving a disulfide group (—S—S—).
  • examples of the reducing agent include, but are not limited to, thioglycolic acid, cysteine, glutathione, ammonium thioglycolate, thioglycolic acid monoethanolamine, acetylcysteine, 2-mercaptoethanol, dithiothreitol, and salts thereof.
  • salt includes metal salts, ammonium salts, amine salts, acetates, hydrochlorides, and the like.
  • the metal salt may be an alkali metal salt, an alkaline earth metal salt, or the like.
  • the amine salt may be a triethylamine salt, a benzylamine salt, or the like.
  • the treatment agent of the present invention contains, in addition to the reducing agent, other components used in cosmetics, quasi-drugs, pharmaceuticals, etc. on the condition that the effect of increasing the adhesion between ground hair and artificial hair is not impaired.
  • additive it can be blended as needed.
  • the other components include oil, surfactant, water, alcohol, chelating agent, silicone, antioxidant, fragrance, preservative, pH adjuster, carbohydrate, protein, nucleic acid, vitamin, Contains minerals.
  • the form of the treatment agent and treatment composition of the present invention may be any form used for conventional quasi-drugs, cosmetics, and the like, including, for example, solutions, creams, emulsions, gels, powders, and sprays. It is not limited.
  • the pH of the treatment agent and the treatment composition of the present invention is not particularly limited as long as it does not impair the effect of increasing the adhesion between the ground hair and the artificial hair.
  • the pH is preferably pH 7.0-10.5, more preferably pH 7.5-10.0, and most preferably pH 8.0-9.5.
  • artificial hair includes artificial eyelashes, so-called false eyelashes, which are commercially available.
  • the artificial hair material is not particularly limited, but includes, but is not limited to, synthetic fibers (eg, polyethylene polymer, polypropylene polymer, polybutylene terephthalate polymer, polyester polymer, nylon polymer, vinyl chloride polymer), carbon fiber, and glass fiber.
  • synthetic fibers eg, polyethylene polymer, polypropylene polymer, polybutylene
  • ground hair is an attached organ of the skin of animals including mammals and birds, and refers to a biological polymer mainly composed of keratin.
  • the animal species include, but are not limited to, humans, monkeys, horses, cows, sheep, goats, mice, guinea pigs, dogs, cats and chickens.
  • the animal species is preferably a human.
  • the human ground hair includes, but is not limited to, eyebrows, eyelashes, head hair, and eyelids (mouth, chin, cheek).
  • the ground hair and / or artificial hair is washed with water and / or a detergent before the ground hair and / or artificial hair is treated with the treatment agent or treatment composition of the present invention.
  • the said detergent is not specifically limited on the condition that the effect which increases the adhesiveness of ground hair and artificial hair is not impaired, it may be sodium dodecyl sulfate (SDS).
  • SDS sodium dodecyl sulfate
  • the ground hair and / or artificial hair is preferably washed with water.
  • the ground hair and / or artificial hair is preferably dried after the washing. The drying may be air drying or heat drying.
  • the treatment agent or composition for treatment of the present invention in the step of treating ground hair and / or artificial hair with the treatment agent, is contacted with the ground hair and / or artificial hair.
  • the processing time by the said processing agent or the composition for a process is not specifically limited.
  • the treatment time is preferably 1 to 11 minutes, more preferably 3 to 9 minutes. Most preferably, it is 5 to 7 minutes.
  • the processing temperature by the said processing agent and the composition for a process is not specifically limited on the condition that the effect which increases the adhesiveness of ground hair and artificial hair is not impaired, it may be room temperature.
  • the ground hair and / or artificial hair may be brushed before or after the ground hair and / or artificial hair is treated with the treatment agent or treatment composition of the present invention.
  • the brushing can be performed using a comb, a dental rotary wrinkle, a melamine sponge, a styrene polymer foam, or the like.
  • an operation for stopping the treatment may be performed after the treatment with the treatment agent or the composition for treatment of the present invention.
  • the ground hair and / or artificial hair may be washed and / or dried after treatment with the treatment agent or treatment composition of the present invention.
  • the ground hair and / or artificial hair may be washed and / or dried after an operation for stopping the treatment is performed.
  • the conditions for washing and / or drying are not particularly limited as long as the effect of increasing the adhesion between the ground hair and the artificial hair is not impaired.
  • the cleaning may be running water cleaning, wiping cleaning, or the like. In the cleaning, the detergent may be used.
  • the drying may be air drying or heat drying.
  • the adhesive for bonding the ground hair and the artificial hair includes, for example, an acrylate adhesive, a hot melt adhesive, a silicone adhesive, and the like.
  • the acrylate adhesive may be a cyanoacrylate adhesive.
  • the adhesive is preferably an adhesive conventionally used for skin and / or hair. The adhesive can be obtained commercially.
  • Adhesiveness can be evaluated by measuring adhesive strength, adhesive strength, and the like.
  • the adhesive force can be measured using a commercially available analytical measuring instrument (for example, Autograph AG-Xplus series (Shimadzu Corporation)) or a self-made measuring instrument (for example, a spring balance).
  • the measured value may be used as it is.
  • the measured value may be used after being converted into a comparable value.
  • Image analysis software can be used to calculate the comparable values.
  • the comparable values may be adhesive strength (N) and adhesive strength (N ⁇ mm).
  • the treatment agent, treatment composition and / or treatment method of the present invention are appropriately applied according to the constitution, age, sex, etc. of the subject.
  • the subject is not particularly limited, but is preferably a human.
  • Adhesive strength evaluation test (1) Materials and Methods A synthetic fiber (catalog number 1104-000596, Kate of Tokyo Co., Ltd., diameter 0.15 mm) (hereinafter referred to as “polyester fiber”) was used as the artificial hair. Healthy human hair (5.0 cm each) was used as the ground hair.
  • Treatment with treatment agent Hair is treated with an aqueous solution of 5% thioglycolic acid (Wako Pure Chemical Industries, Ltd.) adjusted to pH 8.5 with 5% aqueous ammonia (Wako Pure Chemical Industries, Ltd.) for 7 minutes. Treated (hereinafter referred to as “treated hair”). As a control, hair was not treated with the mixed solution (hereinafter referred to as “untreated hair”). Thereafter, the treated hair and the untreated hair were washed for 10 minutes under running water and dried with a dryer.
  • Adhesion Treated hair-polyester fiber and non-treated hair-polyester fiber were each adhered by 1.5 cm using a cyanoacrylate adhesive (Pigments Glue (trademark), catalog number 1002001322, Kate of Tokyo Co., Ltd.). . After standing overnight, the adhesion was evaluated.
  • a cyanoacrylate adhesive Pigments Glue (trademark), catalog number 1002001322, Kate of Tokyo Co., Ltd.).
  • Adhesive strength evaluation In order to evaluate the adhesive strength of treated hair-polyester fibers and non-treated hair-polyester fibers, the end portion on the opposite side to the adhesion site is bonded to the drawing paper (1.5 cm x 1.5 cm). It was adhered with an agent (cemedine (registered trademark), Cemedine Co., Ltd.). Each drawing paper was pulled in a direction perpendicular to the bonding surface, and the stress at the time of peeling the hair and the polyester fiber was measured as an adhesive force. The adhesive force was measured with a tensile tester (AG-250 kNI, Shimadzu Corporation) at 5 mm / min. Adhesion measurements were recorded from the beginning of peeling until the completion of peeling.
  • a tensile tester AG-250 kNI, Shimadzu Corporation
  • FIG. 1 is a typical chart showing the adhesive strength of untreated hair-polyester fibers (the oblique lines are attached after the measurement of the adhesive strength in order to show the waveform chart portion where the integrated value of the adhesive strength is calculated. )
  • FIG. 2 is a typical chart showing the adhesive strength of the treated hair-polyester fiber (the oblique lines are attached after the measurement of the adhesive strength in order to show the waveform chart portion where the integrated value of the adhesive strength is calculated) .
  • the vertical axis represents the adhesive force (N)
  • the horizontal axis represents the stroke (mm).
  • FIG. 3 is a graph showing the maximum values of the adhesive strength of untreated hair-polyester fibers and treated hair-polyester fibers.
  • FIG. 4 is a graph showing the non-treated hair-polyester fiber adhesive strength and the treated hair-polyester fiber adhesive strength.
  • the vertical axis indicates the adhesive strength (N ⁇ mm), and the horizontal axis indicates each experimental condition.
  • the bond strength of the treated hair-polyester fibers was about 3.6 times higher than the bond strength of the untreated hair-polyester fibers. From these results, it has been clarified that the adhesiveness between the natural hair and the artificial hair is remarkably increased by treating the natural hair with a treatment agent containing a reducing agent (thioglycolic acid).
  • Adhesive strength evaluation test (2) Materials and Methods As artificial hair (polyester fiber), false eyelashes (catalog number 1104-000596, Kate of Tokyo Co., Ltd., diameter 0.15 mm) were used. Healthy human hair (5.0 cm each) was used as the ground hair.
  • the hair was brushed using a dental rotary wrinkle. As a control, the hair was not brushed.
  • Treatment with treatment agent Hair was treated with a treatment agent (pH 9) containing 5% cysteine for 7 minutes, then washed under running water for 10 minutes, and dried with a drier. As a control, the hair was not treated with the treatment.
  • Adhesive hair that is not brushed and not treated with a treatment (brushing-, treatment-), brushed hair (brushing +), hair treated with a treatment (treatment agent +), and brushed
  • the hair treated with the treatment agent was adhered to the false eyelashes using a cyanoacrylate adhesive, respectively.
  • the bonding condition was 5 minutes at room temperature. Thereafter, the adhesive strength was evaluated.
  • Adhesive strength evaluation In order to evaluate the adhesive strength, the end portion on the opposite side to the adhesion site was respectively adhered to the drawing paper (1.5 cm ⁇ 1.5 cm) with an adhesive (Cemedine (registered trademark), Cemedine Co., Ltd.). It was. The adhesive force when peeling hair and false eyelashes was measured with a self-made spring balance. 100 g weight was converted as 1 Newton (N).
  • FIG. 5 is a graph showing the adhesive strength between hair and false eyelashes.
  • the vertical axis indicates the adhesive force (Newton (N)), and the horizontal axis indicates each experimental condition.
  • the error bar for each experimental condition indicates the standard deviation of the measured value of the experimental result repeated 10 to 20 times under the same condition.
  • Adhesive strength (N) is 0.19N for hair (brushing-, treatment agent-)-false eyelashes, and 0.38N for hair (treatment agent +)-false eyelashes, and hair (brushing +)-false eyelashes was 0.40 N, and 0.99 N for hair (brushing +, treatment agent +)-pasted eyelashes.
  • the adhesive force between the hair and false eyelashes is statistically significant (p ⁇ 0.001, Student) by brushing the hair or treating the hair with a treatment containing a reducing agent (cysteine). T-test).
  • the adhesive force between the hair and false eyelashes is statistically significant (p ⁇ 0.001, Student's t-test) by brushing the hair and treating it with a treating agent containing a reducing agent (cysteine).
  • the treatment agent containing other reducing agents for example, thioglycolic acid etc.

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Cosmetics (AREA)

Abstract

La présente invention a pour objet de mettre au point un agent de traitement et un procédé de traitement pour stimuler l'adhérence entre des poils artificiels et des poils naturels, ledit agent de traitement et ledit procédé de traitement étant extrêmement sûrs et capables d'obtenir un effet d'adhérence élevé. L'agent de traitement selon la présente invention pour stimuler l'adhérence entre des poils artificiels et des poils naturels comprend un agent réducteur en tant qu'un ingrédient actif. L'agent réducteur peut être un ou plusieurs des éléments sélectionné(s) dans le groupe composé d'acide thioglycolique, de cystéine et de sels de ceux-ci. Le procédé de traitement selon la présente invention pour stimuler l'adhérence entre des poils artificiels et des poils naturels comprend une étape de préparation de l'agent de traitement de la présente invention, une étape de brossage des poils naturels et/ou une étape de traitement des poils naturels avec l'agent de traitement, une étape de lavage des poils naturels et une étape de séchage des poils naturels. Les poils artificiels peuvent être des poils artificiels pour des sourcils, des cils et/ou des cheveux. Les poils naturels peuvent être des sourcils, des cils et/ou des cheveux.
PCT/JP2013/078131 2012-11-29 2013-10-17 Agent de traitement et procédé de traitement pour stimuler l'adhérence entre des poils artificiels et des poils naturels WO2014083957A1 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2012260888A JP2016040416A (ja) 2012-11-29 2012-11-29 人工毛と地毛との接着性を増大するための処理剤及び処理方法
JP2012-260888 2012-11-29

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WO2014083957A1 true WO2014083957A1 (fr) 2014-06-05

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JP2018162548A (ja) * 2017-03-27 2018-10-18 株式会社松風 人工まつげの製造方法、人工まつげおよび人工まつげの取付け方法
JP2019014981A (ja) * 2017-07-04 2019-01-31 株式会社松風 まつげエクステンション、まつげエクステンションの製造方法および取付け方法
JP7208760B2 (ja) * 2018-10-22 2023-01-19 株式会社日本アイラッシュ総研 まつげエクステンション用の接着強度試験方法
JP2021031422A (ja) * 2019-08-21 2021-03-01 株式会社 菊星 接着増強組成物及びそれを用いるまつ毛エクステンションの施術方法

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