WO2013179434A1 - 固定砥粒ワイヤーソーとその製造方法、及びそれを用いたワークの切断方法 - Google Patents
固定砥粒ワイヤーソーとその製造方法、及びそれを用いたワークの切断方法 Download PDFInfo
- Publication number
- WO2013179434A1 WO2013179434A1 PCT/JP2012/064043 JP2012064043W WO2013179434A1 WO 2013179434 A1 WO2013179434 A1 WO 2013179434A1 JP 2012064043 W JP2012064043 W JP 2012064043W WO 2013179434 A1 WO2013179434 A1 WO 2013179434A1
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- WIPO (PCT)
- Prior art keywords
- abrasive
- fixed
- adhesive
- wire
- core wire
- Prior art date
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23D—PLANING; SLOTTING; SHEARING; BROACHING; SAWING; FILING; SCRAPING; LIKE OPERATIONS FOR WORKING METAL BY REMOVING MATERIAL, NOT OTHERWISE PROVIDED FOR
- B23D61/00—Tools for sawing machines or sawing devices; Clamping devices for these tools
- B23D61/18—Sawing tools of special type, e.g. wire saw strands, saw blades or saw wire equipped with diamonds or other abrasive particles in selected individual positions
- B23D61/185—Saw wires; Saw cables; Twisted saw strips
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B24—GRINDING; POLISHING
- B24B—MACHINES, DEVICES, OR PROCESSES FOR GRINDING OR POLISHING; DRESSING OR CONDITIONING OF ABRADING SURFACES; FEEDING OF GRINDING, POLISHING, OR LAPPING AGENTS
- B24B27/00—Other grinding machines or devices
- B24B27/06—Grinders for cutting-off
- B24B27/0633—Grinders for cutting-off using a cutting wire
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B24—GRINDING; POLISHING
- B24D—TOOLS FOR GRINDING, BUFFING OR SHARPENING
- B24D18/00—Manufacture of grinding tools or other grinding devices, e.g. wheels, not otherwise provided for
- B24D18/0072—Manufacture of grinding tools or other grinding devices, e.g. wheels, not otherwise provided for using adhesives for bonding abrasive particles or grinding elements to a support, e.g. by gluing
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B24—GRINDING; POLISHING
- B24D—TOOLS FOR GRINDING, BUFFING OR SHARPENING
- B24D3/00—Physical features of abrasive bodies, or sheets, e.g. abrasive surfaces of special nature; Abrasive bodies or sheets characterised by their constituents
- B24D3/02—Physical features of abrasive bodies, or sheets, e.g. abrasive surfaces of special nature; Abrasive bodies or sheets characterised by their constituents the constituent being used as bonding agent
- B24D3/04—Physical features of abrasive bodies, or sheets, e.g. abrasive surfaces of special nature; Abrasive bodies or sheets characterised by their constituents the constituent being used as bonding agent and being essentially inorganic
- B24D3/06—Physical features of abrasive bodies, or sheets, e.g. abrasive surfaces of special nature; Abrasive bodies or sheets characterised by their constituents the constituent being used as bonding agent and being essentially inorganic metallic or mixture of metals with ceramic materials, e.g. hard metals, "cermets", cements
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B28—WORKING CEMENT, CLAY, OR STONE
- B28D—WORKING STONE OR STONE-LIKE MATERIALS
- B28D5/00—Fine working of gems, jewels, crystals, e.g. of semiconductor material; apparatus or devices therefor
- B28D5/04—Fine working of gems, jewels, crystals, e.g. of semiconductor material; apparatus or devices therefor by tools other than rotary type, e.g. reciprocating tools
Definitions
- the present invention is, for example, a fixed abrasive wire saw suitable for slicing a workpiece made of hard and brittle materials such as large-diameter silicon, sapphire, silicon carbide, ceramics material, magnetic material, and the like, and its fixing method
- the present invention relates to a method for cutting the workpiece using an abrasive wire saw.
- Patent Document 1 discloses a method of energizing a metal wire passing through an abrasive grain layer settling in a plating bath.
- the fixed-abrasive wire saw by such electrodeposition has the advantage that the holding power of the abrasive grains is large and difficult to detach, but the abrasive grains are randomly fixed to the outer peripheral surface of the wire in the plating tank during production.
- a large number of abrasive grain groups in which a large number of abrasive grains are aggregated and fixed locally are likely to be formed, and individual differences are likely to occur depending on the product.
- the wire part in which such an abrasive grain group was formed since the pressing force to the workpiece
- the abrasive grain arrangement on the wire is a random arrangement depending on the probability, and the formation of the abrasive grains cannot be avoided, the wear rate of each abrasive grain varies due to grinding. As a result, the cut surface roughness of the workpiece, that is, the cut surface accuracy is lowered. Furthermore, in the wire portion in which the abrasive grain group is formed, chips are easily accumulated between the abrasive grains during crushing, and clogging is likely to occur. And in the wire part which caused clogging, since grinding resistance increases and a big concentrated stress acts, there exists a problem that a wire breaks easily and a product life falls. Such clogging also leads to a decrease in grinding efficiency and cut surface accuracy.
- attachment of the abrasive grains of the said wire group in the wire direction is mentioned.
- the applicant forms a point-like adhesive layer by spraying an adhesive on the outer peripheral surface of the wire in Patent Document 2, and the adhesive layer is used for grinding.
- a fixed abrasive wire saw formed by temporarily fixing the grains and permanently fixing the temporarily fixed abrasive grains by nickel plating was proposed.
- the wire saw described in Patent Document 2 since the arrangement of the abrasive grains is controlled by spraying, it is suppressed to some extent that a large number of abrasive grains are locally agglomerated and fixed as compared with that in Patent Document 1. It is possible to do.
- the technical problem of the present invention is that it is possible to improve the cut surface accuracy and grinding efficiency of the workpiece, and further, it is possible to extend the life of the product, a fixed abrasive wire saw and a manufacturing method thereof, and It is providing the processing method of the workpiece
- a large number of abrasive grains having a uniform particle size coat the outer peripheral surface of the core wire on the outer peripheral surface of the high-strength core wire.
- the core wire is made of a metal wire and the binder layer is made of a plated metal.
- the abrasive grains are arranged on a large number of dot-like adhesive layers arranged at regular pitch intervals linearly along the axis of the core wire, and The abrasive grains arranged on the adhesive layers adjacent to each other are fixed in a state of being separated from each other. Therefore, it is possible to suppress formation of a group of abrasive grains in which a large number of abrasive grains are locally aggregated and fixed, and in particular, it is possible to suppress adhesion between abrasive grains in the axial direction of the core wire. Therefore, when the workpiece is ground, the cutting depth by each abrasive grain can be sufficiently secured, and the grinding efficiency can be improved.
- the adhesive layer is made of a rubber-based adhesive and has elasticity. It is desirable to form a buffer layer that allows movement in a direction intersecting the outer peripheral surface of the core wire. By doing so, the height from the outer peripheral surface of the core wire to the tip of the abrasive grain, that is, the variation in the height of the abrasive grain, can be absorbed by the buffer layer, and the cut surface accuracy can be further improved.
- the adhesive layers may be arranged at equal pitch intervals in each of the adhesive layer rows. At this time, the pitch interval of the abrasive grains in the adhesive layer sequence may be even.
- the adhesive layers forming the respective adhesive layer rows may be disposed on at least one spiral. By doing so, it becomes possible to further improve the discharge of chips.
- the minimum pitch interval of the abrasive grains in these adhesive layer rows is longer than the maximum interval between adjacent adhesive layer rows in the circumferential direction of the core wire. It is desirable from the viewpoint of efficiency and chip discharge.
- the adhesive layer has a circular shape and the diameter is equal to or less than the average abrasive grain size and 30% or more of the average abrasive grain size, a plurality of abrasive grains are fixed on one adhesive layer. Or an adhesive layer to which the abrasive grains are not fixed can be suppressed, and the abrasive grains can be efficiently disposed without waste.
- the step of disposing a roller having a plurality of fine holes formed in the outer periphery in the circumferential direction on the traveling path of the core wire A step of filling an adhesive into the micropores of the roller, a step of running the core wire in a state in which the outer peripheral surface thereof is in contact with the outer periphery of the roller, and an outer peripheral surface of the core wire that runs with the micropores of the rotating roller
- the fixed abrasive wire saw and the workpiece are pressed against each other under a predetermined wire tension, and the fixed abrasive wire saw is moved in one direction or reciprocating direction to cut the workpiece. Then, the workpiece can be cut efficiently and accurately.
- FIG. 2 is a schematic AA cross-sectional view of the fixed abrasive wire saw shown in FIG. 1. It is a rough cross-sectional view which shows one modification of 1st Embodiment of the fixed abrasive wire saw which concerns on this invention. It is a schematic front view which shows a part of 2nd Embodiment of the fixed abrasive wire saw which concerns on this invention. It is a schematic front view which shows a part of 3rd Embodiment of the fixed abrasive wire saw which concerns on this invention.
- the fixed abrasive wire saw according to the present invention has a large number of abrasive grains 2 having a uniform grain size on the outer peripheral surface of a high-strength core wire 1. It is formed by fixing with a binder layer 4 covering the whole. At this time, a large number of dot-like adhesive layers 3 are coated on the outer peripheral surface of the core wire 1 so as to be spaced apart from each other.
- the abrasive grains 2 are temporarily fixed (adhered) by the dotted adhesive layer 3 and are permanently fixed by the binder layer 4.
- the abrasive grains 2 are fixed to the outer peripheral surface of the core wire 1 in a single layer.
- the abrasive grains 2 disposed on the adhesive layers 3 adjacent to each other are fixed in a state of being separated from each other.
- the said core wire 1 consists of a metal wire which has a uniform circular cross section over the whole longitudinal direction (namely, axial direction).
- a wire made of heat-treated spring steel such as high carbon steel and medium carbon low alloy steel
- a wire made of processed spring steel such as hard steel wire, piano wire, stainless wire, cold rolled steel wire, oil tempered wire, Low-strength steel, medium-alloy steel, high-alloy steel, maraging steel and other super-strong steel wires, tungsten, molybdenum, beryllium and other metal wires, or amorphous metals such as Fe-Si-B and Al-Y-Ni
- a wire rod made of fiber is preferably used.
- the diameter D is preferably in the range of 0.08 mm to 0.20 mm. If the diameter of the core wire 1 is smaller than 0.08 mm, sufficient strength of the wire saw 1 cannot be secured. If it is thicker than 0.20 mm, the cutting allowance required for machining the workpiece is large. As a result, waste of materials increases.
- the abrasive 2 is preferably one or more selected from diamond abrasive, CBN abrasive, Al2O3 abrasive, or SiC abrasive.
- the average diameter of the abrasive grains 2 to be used is appropriately set according to the type of workpiece to be ground, the diameter of the core wire 1, and the arrangement of the abrasive grains 2.
- the adhesive layer 3 defines the arrangement of the abrasive grains 2 on the outer peripheral surface of the core wire 1, and as a result, the abrasive grains 2 are fixed along the adhesive layer sequence li.
- the pitch interval m of the adhesive layers 3 in the axial direction of the core wire 1 and the number and arrangement of the adhesive layers in the circumferential direction are ground between the abrasive grains 2 disposed on the adjacent adhesive layers 3.
- the binder layer 4 does not come into contact with the workpiece during processing, and a gap larger than the average abrasive grain size is secured. Further, in consideration of grinding efficiency and chip discharge performance, the shortest pitch interval m of the adhesive layers 3 adjacent in the axial direction is longer than the longest interval n of the adhesive layer rows li adjacent in the circumferential direction. Longer ones are desirable.
- the adhesive layer 3 has a substantially circular shape and the diameter d is 30% or more of the average abrasive grain size and not more than the average abrasive grain size.
- the diameter of the adhesive layer 3 is smaller than 30% of the average abrasive grain size, the adhesive layer to which the abrasive grain 2 is not adhered.
- the average grain size is larger than the average abrasive grain size, the probability that a plurality of abrasive grains 2 are bonded to one adhesive layer 3 is increased.
- the diameter of the adhesive layer 3 is appropriately set so that two or three abrasive grains 2 are easily adhered to one adhesive layer 3 as necessary. Is also possible.
- the adhesive for forming the adhesive layer 3 is not particularly limited as long as it can be temporarily fixed by adhering the abrasive grains 2, but acrylic rubber, styrene rubber, butadiene rubber, nitrile rubber, A rubber-based adhesive such as butyl rubber is preferably used from the viewpoints of fluidity and adhesiveness.
- the adhesive layer 3 also functions as a buffer layer for the abrasive grains 2, the direction in which each abrasive grain in contact with the workpiece intersects the outer peripheral surface of the core wire 1 during grinding of the workpiece.
- the adhesive layer 3 can absorb the variation in the height from the outer peripheral surface of the core wire 1 to the tip of the abrasive grain (that is, the abrasive grain height).
- the binder layer 4 is made of a plated metal, and its film thickness t is thinner than the average abrasive grain size. A part of the abrasive grains 2 is exposed from the surface of the binder layer 4.
- the thickness of the binder layer 4 is preferably in the range of 30% to 50% of the average particle size of the abrasive grains 2, and more preferably 30 to 40%. If the thickness of the binder layer is less than 30%, there is a possibility that the holding power of the abrasive grains 2 cannot be sufficiently secured. On the other hand, if the thickness is larger than 50%, there is a possibility that the protruding amount of the abrasive grains 4 from the surface of the binder layer cannot be secured sufficiently.
- nickel, copper, or chromium is preferably used as the plating metal as the binder.
- the entire surface of the abrasive grains 2 is coated with the binder layer 4 together with the surface of the core wire 1 as necessary. May be.
- the abrasive grains 2 are arranged on a large number of dotted adhesive layers 3 arranged in a line at regular pitch intervals along the metal core wire 1. And the abrasive grain 2 arrange
- positioned on the mutually adjacent adhesive bond layer 3 is adhering in the state mutually spaced apart. Therefore, it is possible to suppress formation of a group of abrasive grains in which a large number of abrasive grains are locally aggregated and fixed, and in particular, it is possible to suppress adhesion between the abrasive grains 2 in the axial direction of the core wire 1.
- the cutting depth by each abrasive grain 2 can be sufficiently secured, and the grinding efficiency can be improved. Further, variation in the wear rate of each abrasive grain 2 due to grinding can be suppressed, and the cut surface roughness of the workpiece, that is, the cut surface accuracy can be improved. Furthermore, the chip discharge performance of the workpiece is improved and clogging between the abrasive grains 2 can be suppressed, so that not only disconnection can be prevented and the product life can be extended, but also the grinding efficiency and cutting surface can be improved. It also helps prevent accuracy loss.
- the dotted adhesive is disposed on the outer peripheral surface of the core wire 1.
- the layers 3 are linearly arranged at equal pitch intervals m along the axis of the core wire 1 to form six (FIGS. 1 and 2) or five (FIG. 3) adhesive layer rows li in the circumferential direction. is doing.
- the adhesive layer 3 in each of the adhesive layer rows li, the adhesive layer 3 is not only applied at an equal pitch interval m in the axial direction, but also between the adhesive layer rows li.
- the pitch interval m of the adhesive layer 3 is uniform.
- the position (that is, the phase) of the adhesive layer 3 in the axial direction is substantially the same between the adhesive layer rows li, so that the adhesive layer 3 forms an annular row s perpendicular to the axis in the circumferential direction.
- the annular rows s are arranged side by side at equal intervals m in the axial direction.
- these adhesive layer rows li are arranged in parallel at equal intervals n in the circumferential direction.
- the pitch interval m of the adhesive layer 3 is not necessarily equal between the adhesive layer rows li.
- two types of adhesive layer rows having different pitch intervals m are used.
- li may be alternately arranged in the circumferential direction, or the pitch intervals m of the adhesive layers 3 may be all different between the adhesive layer rows li.
- any pitch interval m is preferably a multiple of the minimum pitch interval mmin.
- the number of the adhesive layer rows li is not limited to that shown in the drawing, and may be at least three.
- the interval n in the circumferential direction of the adhesive layer row li is not necessarily equal.
- the adhesive layer 3 in each of the adhesive layer rows li, the adhesive layer 3 is applied at an equal pitch interval m in the axial direction.
- the pitch interval m of the adhesive layers 3 is uniform between the adhesive layer rows li.
- the intervals in the circumferential direction of the adhesive layer row li are also uniform.
- the position (phase) in the axial direction of the adhesive layer 3 is sequentially shifted substantially evenly between the adhesive layer rows li, and as a result, one abrasive grain forming each adhesive layer li is provided. It is arranged on the spiral.
- the interval n in the circumferential direction of the adhesive layer row li is not necessarily equal.
- an adhesive layer row li formed by applying the adhesive layer 3 at an equal pitch interval m in the axial direction, and the adhesive layer 3 with a pitch interval m and 2 m. are repeatedly arranged in the circumferential direction.
- the two adhesive layer rows li are arranged with the axial phase shifted by 180 degrees.
- the present invention is not necessarily limited to this, and the phases of both may be matched. Note that all the adhesive layer rows li may be formed by repeating combinations of different pitch intervals like the latter.
- the above-mentioned binder is positioned in the state where the above-mentioned abrasive grains 2 are positioned by the adhesive layer 3 arranged as described above. It is fixed by a layer (plated metal layer). As a result, an abrasive grain row substantially along each of the adhesive layer rows li is formed.
- this manufacturing method is generally performed by transferring an adhesive from the micropores on the outer periphery of the roller onto the outer peripheral surface of the high-strength core wire 1, so A step of applying the point-like adhesive layer 3 at regular pitch intervals, a step of temporarily adhering the abrasive grains 2 to the adhesive layer 3 and positioning, and an outer peripheral surface of the core wire 1 is simply made of a plated metal.
- the core wire 1 drawn horizontally from the first bobbin 5 at a constant speed is degreased in the immersion degreasing tank 6, then passed through the acid immersion tank 7 and acid-washed. It is washed with water in the washing tank 8.
- the degreasing liquid used in the immersion degreasing tank 6 is a commonly used alkaline degreasing liquid, and examples include aqueous solutions of sodium triphosphate, orthosilicate sodium, sodium carbonate, and the like, but are particularly limited. Not what you want.
- the acid solution used in the acid dipping bath 7 is a mixed solution composed of commonly used sulfuric acid, hydrochloric acid, nitric acid, etc., but prepared by changing the composition depending on the core wire material, and the optimum acid treatment conditions. Must be selected.
- the core wire 1 washed with water in the first water rinsing tank 8 is sent to the adhesive application device 10, where the adhesive 3 a is transferred to the outer peripheral surface of the core wire 1, whereby a large number of dot-like adhesive layers 3 are transferred. Is applied to the outer peripheral surface of the core wire 1 with the arrangement being controlled.
- the adhesive application device 10 wraps the sent core wire 1 around the outer periphery of the rotating adhesive transfer roller 18 and brings it into contact with the outer periphery of the roller 18.
- the adhesive 3 a discharged in the form of dots is transferred to the outer peripheral surface of the core wire 1.
- a row of fine holes 18a is formed along the circumferential direction, and these fine holes 18a are supplied from an adhesive (adhesive dissolved in an organic solvent). (Not shown).
- the adhesive is filled into the fine holes 18a from the supply source, and a small amount of the adhesive 3a is discharged to the outer peripheral surface of the roller 18 through the fine holes 18a.
- the adhesive layer 3 can be applied in a more appropriate range of the diameter d, In the subsequent process, the probability that only one abrasive grain is fixed to one adhesive layer is increased, and a wire saw in which single particles are arranged can be manufactured.
- the adhesive used here is not particularly limited as long as it can temporarily fix the abrasive grains 2 in the subsequent process, as described above, but rubber systems such as acrylic, styrene, butadiene, nitrile, and butyl rubber. An adhesive is suitable from the viewpoint of fluidity and adhesiveness.
- the organic solvent is not particularly limited as long as the target adhesive can be dissolved, but aromatic hydrocarbons such as xylene and toluene or aliphatic hydrocarbons such as butadiene and normal hexane are easy to handle. Suitable from aromatic hydrocarbons such as xylene and toluene or aliphatic hydrocarbons such as butadiene and normal hexane are easy to handle. Suitable from aromatic hydrocarbons such as xylene and toluene or aliphatic hydrocarbons such as butadiene and normal hexane are easy to handle. Suitable from
- the core wire 1 sent from the previous process is wound around the outer peripheral surface of the roller 18 along the fine hole 18 a.
- the roller 18 is rotated in the feed direction of the core wire 1 so that the peripheral speed thereof matches the feed speed of the core wire 1.
- the outer peripheral surface of the roller 18 and the core wire 1 can be brought into contact with each other in a state where the relative speed is zero.
- the adhesive layer sequence li is formed by accurately transferring the dotted line as the dotted adhesive layer 3 on the outer peripheral surface of the core wire 1.
- the diameter D of the core wire 1 is 100 ⁇ m
- the diameter d and the pitch interval m of the adhesive layer 3 are 10 ⁇ m and 100 ⁇ m, respectively.
- the micro holes 18a are formed in only one row in the flat portion of the outer peripheral surface of the roller, but the present invention is not limited to this.
- the micro holes 18a may be formed in a curved concave surface or convex surface.
- sequence of the adhesive bond layer 3 applied to the core wire 1 it is possible to arrange
- the adhesive layer sequence li can be formed.
- these rollers 18 are rotated at the same peripheral speed as the feeding speed of the core wire 1, and the adhesive 3 a discharged from the fine holes 18 a is applied to the outer peripheral surface of the core wire 1 in a state where the rotational phase between these rollers is adjusted. Transcript to.
- the adhesive layer 3 is applied to the outer peripheral surface of the core wire 1 to form the adhesive layer row li.
- the rotational phase between the rollers is preferably adjusted so that the transfer positions of the adhesive 3a with respect to the axial direction of the core wire 1 by the respective rollers 18 substantially coincide with each other.
- the core wire 1 in which the adhesive layer row li is formed on the outer peripheral surface as described above is then sent to the abrasive grain adhesion device 11.
- the abrasive grains 2 are dispersed from the periphery of the core wire 1 to the outer peripheral surface thereof.
- the abrasive grains 2 are temporarily fixed to the outer peripheral surface of the core wire 1 by the adhesive layer 3.
- the metal plate 14 connected to the anode passes through the electrolytic plating tank 13 in which the electrolytic plating solution is immersed.
- a plated metal as a binding material is deposited on the outer peripheral surface of the core wire 1 connected to the cathode 9.
- the metal plate 14 serving as an anode is made of the same metal as the plating metal selected as the binder, and the electrolytic plating solution also contains the same metal as the plating metal selected as the binder.
- the film thickness t of the binder layer 4 is set so that a part of the abrasive grains 2 is exposed from the surface thereof, that is, thinner than the average abrasive grain diameter.
- the method for manufacturing a fixed abrasive wire saw as described above, there is no variation in quality in order to securely fix the abrasive grains to the necessary locations, and only in the locations necessary to achieve optimum grinding efficiency. Since the abrasive grains can be arranged without waste, they can be produced economically. Further, as in the case of random fixing of abrasive grains, it is possible to prevent defective products due to the aggregation of abrasive grains and the difference between the front and back of the abrasive density, so that the manufacturing yield can be improved.
- achieve desired grinding efficiency and a cut surface precision can be manufactured by setting an appropriate abrasive grain arrangement pitch according to the material and size of a workpiece
- a processing apparatus as shown in FIG. 11 is used.
- the processing apparatus winds the wire saw Y drawn from the supply-side reel 31 around the two main rollers 32 and 32 provided with a spiral guide groove 32a on the outer periphery along the guide groove 32a.
- a wire saw row YR in which the wire saws Y are parallel to each other at a constant pitch is formed between the upper portions of the main rollers 32 and 32, and the tip of the wire saw Y is wound around the collection-side reel 33.
- each wire saw Y in the wire saw row YR travels in one direction or reciprocates in both directions.
- a predetermined wire tension is applied to the wire saw Y, and the ingot 30 is brought into pressure contact with the wire saw Y and the ingot 30 as the workpiece at a predetermined processing speed or processing load F. It is possible to process a wafer in a short time and obtain a wafer with good surface accuracy.
- the fixed abrasive wire saw according to the present invention, the manufacturing method thereof, and the work cutting method using the fixed abrasive wire saw are not particularly limited to the above-described embodiment, and are the gist of the present invention. Various modifications can be made without departing from the scope.
- the fixed abrasive wire saw according to the present invention corresponds to the embodiment shown in FIGS. 1 and 2, specifically shown in FIG. 10, and the core wire is manufactured by the manufacturing method shown in FIGS.
- the core wire is manufactured by the manufacturing method shown in FIGS.
- six adhesive layer rows in which a large number of dot-like adhesive layers are linearly arranged at a constant pitch interval of 200 ⁇ m are arranged in parallel at equal angular intervals in the circumferential direction of the core wire,
- the diamond abrasive grains are temporarily fixed to the adhesive layer and are made by permanent fixing by nickel electrodeposition. At this time, the diameter of the adhesive layer was set to 10 ⁇ m.
- the fixed abrasive wire saw used as a comparative example is one in which diamond abrasive grains are dispersed almost uniformly on the wire surface and nickel is electrodeposited.
- the adhesive application process of the manufacturing process shown in FIG. While sending the wire at a constant speed, by spraying the adhesive dissolved in the organic solvent from the surroundings, a large number of dot-like adhesive layers are formed on the outer peripheral surface of the piano wire.
- Abrasive grains were temporarily fixed to the adhesive layer on the single layer, and in a subsequent step, the electrode was made to pass through an electrolytic plating tank and electrodeposited with nickel.
- the thickness of the binder layer formed by nickel electrodeposition was set to be the same as in the above example.
- a fixed-abrasive wire saw was produced using a core wire composed of a piano wire having a diameter of 160 ⁇ m and abrasive grains having an average abrasive grain size of 30.4 ⁇ m.
- the adhesive filling the adhesive transfer roller a solution of 15% acrylic rubber and 85% normal hexane was used, and the plating solution of the electrolytic plating tank 11 was nickel sulfamate 500 g / l, nickel chloride 10 g / l. l
- the abrasive grains were fixed by nickel plating at a liquid temperature of 50 ° C.
- the nickel film thickness was set to 10 ⁇ m, which is about 30% of the average abrasive grain size.
- the resulting fixed abrasive wire saw had a substantially uniform abrasive height, and the average wire diameter was 239 ⁇ m.
- the total length of the fixed abrasive wire saw was 10 km.
- a single-layer fixed abrasive wire saw was produced with a core wire composed of a piano wire having a diameter of 160 ⁇ m and abrasive grains having an average abrasive grain size of 30.4 ⁇ m.
- a 15% acrylic rubber and 85% normal hexane solution is used as the adhesive to be sprayed, and the plating solution in the electrolytic plating bath is 500 g / l nickel sulfamate, 10 g / l nickel chloride, and 20 g / l boric acid.
- main fixing of the abrasive grains by nickel plating was performed at a liquid temperature of 50 ° C.
- the nickel film thickness was set to 10 ⁇ m, which is about 30% of the average abrasive grain size.
- the single-layer fixed abrasive wire saw obtained had a substantially uniform abrasive height, and the average wire diameter was 238 ⁇ m.
- the total length of the fixed abrasive wire saw was 10 km.
- a plurality of these wire saws are arranged in parallel and reciprocated at a linear speed of 500 m / min, a wire tension of 35 N, a wire pitch of 1.1 mm, a workpiece feed speed of 18 mm / h, a new Sapphire (hardness of about 2000 Hv) was cut using a water-soluble processing liquid under the condition of a wire supply rate of 1.0 m / min. Then, using the total number of cut pieces (size: ⁇ 2 inch ⁇ length 30 mm, number of cut pieces 27) obtained as a result, a surface consisting of thickness variation TV5 (the center and four points at 90 ° intervals around it). The difference between the maximum value and the minimum value of the thickness at 5 points) was determined. Table 1 below shows performance comparison results between the fixed abrasive wire saw according to the example of the present invention and the fixed abrasive wire saw according to the comparative example.
- the thickness variation TV5 of the wafer is improved by about 10% compared with the comparative example. It was confirmed that the surface roughness, that is, the cut surface accuracy was improved.
- the fixed abrasive wire saw based on the present invention shows a higher value for the initial grinding ability than that of the comparative example. From these results, it was confirmed that according to the wire saw according to the example of the present invention, the grinding efficiency of the workpiece was improved.
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Abstract
Description
さらに、上記砥粒群が形成されたワイヤー部分においては、研削時に、切屑が砥粒間に集積されて目詰まりを起こし易くなる。そして、目詰まりを起こしたワイヤー部分においては、研削抵抗が増大して大きな集中応力が作用するため、ワイヤーが断線し易くなり製品寿命が低下するという問題がある。また、このような目詰まりは、研削効率や切断面精度の低下にもつながる。
ここで、このような砥粒の磨耗速度のばらつきや目詰まりの主たる要因としては、上記砥粒群におけるワイヤー方向の砥粒同士の密着が挙げられる。
この特許文献2に記載のワイヤーソーにおいては、砥粒配置がスプレーによりコントロールされることから、特許文献1のものと比べ、多数の砥粒が局所的に凝集して固着されるのをある程度抑制することは可能である。しかしながら、図14に示すように、依然として確率に依存したランダムな砥粒配置にならざるを得えないため、上記各問題点に対する懸念が払拭されるものではなく、更なる改善の余地が残されている。
このとき、上記芯線が金属線材から成っていて、上記結合材層がメッキ金属から成っていることが望ましい。
図1~図5に示すように、本発明に係る固定砥粒ワイヤーソーは、高強度の芯線1の外周面上に、均等な粒度を有する多数の砥粒2を、該芯線1の外周面全体を被覆する結合材層4で固着することにより形成されている。このとき、上記芯線1の外周面上には、多数の点状の接着剤層3が相互に離間して配置されるように制御して塗着されている。そして、上記砥粒2が、その点状の接着剤層3により仮固着(接着)されると共に、上記結合材層4により本固着されている。その結果、該砥粒2は、上記芯線1の外周面に対し単層に固着されている。その結果、互いに隣接する各接着剤層3上に配された砥粒2は、相互に離間した状態で固着されている。
この製造方法は、図6に示すように、概略的には、高強度の芯線1の外周面上に、ローラー外周の微小孔から接着剤を転写することにより、該芯線1に沿って多数の点状の接着剤層3を規則的なピッチ間隔で塗着させる工程と、その接着剤層3に砥粒2を仮固着させて位置決めする工程と、芯線1の外周面をメッキ金属から成る単層の結合材層4で被覆することにより、上記仮固着された砥粒2を、その一部を結合材層4の表面から露出させた状態で、芯線1の外周面に本固着させる工程とから成っている。
ここで、浸漬脱脂槽6で用いられる脱脂液は、一般的に使用されているアルカリ脱脂液であり、3リン酸ソーダや、オルソ珪酸ソーダ及び炭酸ソーダ等における各水溶液が挙げられるが、特に限定するものではない。また、酸浸漬槽7で用いられる酸液は、一般的に使用されている硫酸、塩酸、硝酸等から成る混合溶液であるが、芯線素材により組成を変えて調製し、最適な酸処理条件を選択する必要がある。
上記接着剤転写ローラー18の外周面には、その周方向に沿って微細孔18aの列が開設されていて、これら微細孔18aは、接着剤(有機溶剤に溶解させた接着剤)の供給源(図示略)へと接続されている。そして、該接着剤がその供給源から上記微細孔18aにそれぞれ充填され、これら微細孔18aを通じて上記ローラー18の外周面に微量の接着剤3aが吐出されるようになっている。
また、ここで用いる接着剤に関しては、上述したように、後工程で砥粒2を仮固着できるものであれば特に限定されるものでないが、アクリル、スチレン、ブタジエン、ニトリル、ブチルゴム等のゴム系接着剤が、流動性・接着性等の面から適している。有機溶剤に関しても、目的の接着剤を溶解できるものであれば特に限定されるものではないが、キシレン、トルエン等の芳香族炭化水素またはブタジエン、ノルマルヘキサン等の脂肪族炭化水素が取扱い性の面から適している。
したがって、上記ローラー18の数や配置、並びに、該ローラー18の外周面の形状、及びそこに開設する微細孔18aの数や配置等を適宜調整することにより、芯線1の外周面に様々な形態の接着剤層列liを形成することができる。
この場合、上記接着剤塗布装置10においては、芯線1の周方向に6本の接着剤層列liを並設するため、図7に示すように、6個の接着剤転写ローラー18が、芯線1の走行経路に沿って順次配置されている。そして、該芯線1がこれらローラー18に巻き架けられている。このとき、接着剤層liを芯線1の周方向に均等な間隔で形成するため、これら6個のローラー18は、等角度(すなわち60度)毎に傾斜させた状態で配置されている。また、上記接着剤層3を芯線1の軸方向に均等なピッチ間隔で一列に配列させるため、上記各ローラー18の外周面にも、同様の均等なピッチ間隔で一列に上記微細孔18aが開設されている。
以上のようにして、外周面に接着剤層列liが形成された芯線1は、次に砥粒付着装置11に送られる。この砥粒付着装置11では、芯線1の周囲からその外周面に砥粒2が散布される。その結果、砥粒2が、上記接着剤層3により芯線1の外周面に対し仮固着される。
ここで、陽極となる金属板14は、結合材として選択されたメッキ金属と同じ金属から成っており、電解メッキ液も、結合材として選択されたメッキ金属と同じ金属を含んでいる。また、結合材層4の膜厚tは、砥粒2の一部がその表面から露出する程度、すなわち平均砥粒径よりも薄く設定する。
そしてその後、外周面に砥粒2が本固着された芯線1を、第3水洗槽15にて水洗し、次に防錆剤槽16で防錆処理を施した後、第2ボビン17で巻き取る。その結果、図10に示すような固定砥粒ワイヤーソーを得ることができる。
なお、本発明に係る固定砥粒ワイヤーソー、及びその製造方法、並びに該固定砥粒ワイヤーソーを用いたワークの切断方法は、上記の実施形態に特に限定されるものではなく、本発明の主旨を逸脱しない範囲で種々変更を加えることが可能である。
直径160μmのピアノ線から成る芯線と平均砥粒径30.4μmの砥粒とにより固定砥粒ワイヤーソーを作製した。ここで、上記接着剤転写ローラーに充填する接着剤には、アクリルゴム15%とノルマルヘキサン85%の溶液を用い、電解メッキ槽11のメッキ液にはスルファミン酸ニッケル500g/l、塩化ニッケル10g/l、硼酸20g/lによりpH4.0に調整した水溶液を用い、液温50℃、電流密度15A/dm2でニッケルメッキによる砥粒の本固着を施した。ニッケル膜厚は平均砥粒径の約30%の10μmに設定した。その結果として得られた固定砥粒ワイヤーソーは、ほぼ均等な砥粒高さを有しており、その平均線径は239μmであった。なお、固定砥粒ワイヤーソーの全長は10kmとした。
直径160μmのピアノ線から成る芯線と平均砥粒径30.4μmの砥粒とにより単層固定砥粒ワイヤーソーを作製した。ここで、スプレーする接着剤には、アクリルゴム15%とノルマルヘキサン85%の溶液を用い、電解メッキ槽のめっき液にはスルファミン酸ニッケル500g/l、塩化ニッケル10g/l、硼酸20g/lによりpH4.0に調整した水溶液を用い、液温50℃、電流密度15A/dm2でニッケルめっきによる砥粒の本固着を施した。ニッケル膜厚は平均砥粒径の約30%の10μmに設定した。その結果として得られた単層固定砥粒ワイヤーソーは、ほぼ均等な砥粒高さを有しており、その平均線径は238μmであった。なお、固定砥粒ワイヤーソーの全長は10kmとした。
以下の表1は、上記本発明の実施例に係る固定砥粒ワイヤーソーと、上記比較例に係る固定砥粒ワイヤーソーとの性能比較結果である。
2 砥粒
3 接着剤層
3a 接着剤
4 結合材層
5 第1ボビン
6 浸漬脱脂槽
7 酸浸漬槽
8 第1水洗槽
9 陰極
10 接着剤塗布装置
11 砥粒付着装置
12 第2水洗槽
13 電解メッキ槽
14 金属板(陽極)
15 第3水洗槽
16 防錆剤槽
17 第2ボビン
18 接着剤転写ローラー
18a 微細孔
30 ワーク(インゴット)
31 供給側リール
32 メインローラー
Claims (10)
- 高強度の芯線の外周面上に、均等な粒度を有する多数の砥粒が、該芯線の外周面を被覆する結合材層により、単層に固着されて成る固定砥粒ワイヤーソーであって、
上記芯線の外周面上に、多数の点状の接着剤層が、相互に離間して塗着されていると共に、上記芯線の軸に沿って直線状に規則的なピッチ間隔で配列されて少なくとも3本の接着剤層列を形成しており、
上記砥粒が、上記接着剤層により仮固着されると共に上記結合材層により本固着されていて、互いに隣接する接着剤層上に配置された砥粒が、相互に離間した状態で固着されている、
ことを特徴とする固定砥粒ワイヤーソー。 - 上記芯線が金属線材から成っていて、
上記結合材層がメッキ金属から成っている、
ことを特徴とする請求項1に記載の固定砥粒ワイヤーソー。 - 上記接着剤層が、ゴム系接着剤から成っていて弾性を有しており、ワークの加工時に、ワークに当接する各砥粒が上記芯線の外周面に対して交差する方向へ動くことを許容する緩衝層を成している、
ことを特徴とする請求項2に記載の固定砥粒ワイヤーソー。 - 上記接着剤層列のそれぞれにおいて、上記接着剤層が均等なピッチ間隔で配列されている、
ことを特徴とする請求項1~3の何れかに記載の固定砥粒ワイヤーソー。 - さらに、上記接着剤層列相互における砥粒のピッチ間隔も均等になっている、
ことを特徴とする請求項4に記載の固定砥粒ワイヤーソー。 - さらに、上記各接着剤層列を形成する接着剤層が、少なくとも1本の螺旋上に配置されている、
ことを特徴とする請求項5に記載の固定砥粒ワイヤーソー。 - 上記芯線の周方向における隣接する接着剤層列の最大間隔よりも、これら接着剤層列における砥粒の最小ピッチ間隔が長くなっている、
ことを特徴とする請求項1~6の何れかに記載の固定砥粒ワイヤーソー。 - 上記接着剤層が円形状を成していて、その径が平均砥粒径以下で平均砥粒径の30%以上である、
ことを特徴とする請求項1~7の何れかに記載の固定砥粒ワイヤーソー。 - 請求項1~8の何れかに記載の固定砥粒ワイヤーソーを製造する方法であって、
外周に複数個の微細孔が周方向に開設されて成るローラーを、上記芯線の走行経路上に配設する工程と、
上記ローラーの微細孔に接着剤を充填する工程と、
上記芯線を、その外周面を上記ローラーの外周に接触させた状態で走行させる工程と、
回転する上記ローラーの微細孔と走行する芯線の外周面との相対速度がゼロとなるように調整した状態において、上記芯線の外周面上に、上記微細孔から接着剤を転写することにより、点状の接着剤層を塗着させる工程と、
接着剤が転写された該芯線の外周面に砥粒を散布して、該接着剤により仮固定する工程と、
砥粒が仮固定された該芯線の外周面を更に結合材で被覆して、該砥粒を該結合材層により本固着する工程とを含む、
ことを特徴とする方法。 - 請求項1~8の何れかに記載の固定砥粒ワイヤーソー、又は請求項9に記載の方法により製造された固定砥粒ワイヤーソーを用いたワークの切断方法であて、
上記固定砥粒ワイヤーソーとワークとを、所定のワイヤー張力の下で相互に圧接させた状態で、該固定砥粒ワイヤーソーを一方向又は往復方向に走行させることにより、該ワークを切断する、
ことを特徴とする方法。
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US14/386,071 US20150040884A1 (en) | 2012-05-31 | 2012-05-31 | Fixed abrasive grain wire saw, its manufacturing method, and method of cutting workpiece by using it |
JP2014518165A JP6352176B2 (ja) | 2012-05-31 | 2012-05-31 | 固定砥粒ワイヤーソーとその製造方法、及びそれを用いたワークの切断方法 |
EP12877662.2A EP2857143A4 (en) | 2012-05-31 | 2012-05-31 | GRINDING WIRE SAW, METHOD FOR THE PRODUCTION THEREOF, AND METHOD FOR CUTTING A WORKPIECE THEREWITH |
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MYPI2014703520A MY185161A (en) | 2012-05-31 | 2012-05-31 | Fixed abrasive grain wire saw, its manufacturing method, and method of cutting workpiece by using it |
CN201280068460.7A CN104136169A (zh) | 2012-05-31 | 2012-05-31 | 固定磨粒钢丝锯和其制造方法及使用它的工件的切断方法 |
PH12014502652A PH12014502652A1 (en) | 2012-05-31 | 2014-11-27 | Fixed abrasive grain wire saw, its manufacturing method, and method of cutting workpiece by using it |
HK15101379.2A HK1200759A1 (en) | 2012-05-31 | 2015-02-06 | Fixed-abrasive-grain wire-saw, method for manufacturing same, and method for cutting workpiece using same |
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-
2012
- 2012-05-31 EP EP12877662.2A patent/EP2857143A4/en not_active Withdrawn
- 2012-05-31 US US14/386,071 patent/US20150040884A1/en not_active Abandoned
- 2012-05-31 WO PCT/JP2012/064043 patent/WO2013179434A1/ja active Application Filing
- 2012-05-31 MY MYPI2014703520A patent/MY185161A/en unknown
- 2012-05-31 KR KR20147029066A patent/KR20150020527A/ko not_active Application Discontinuation
- 2012-05-31 CN CN201280068460.7A patent/CN104136169A/zh active Pending
- 2012-05-31 JP JP2014518165A patent/JP6352176B2/ja active Active
-
2014
- 2014-11-27 PH PH12014502652A patent/PH12014502652A1/en unknown
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2015
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CN106413993A (zh) * | 2014-05-28 | 2017-02-15 | 信越半导体株式会社 | 固定磨粒钢线及线锯并用的工件的切断方法 |
CN106413993B (zh) * | 2014-05-28 | 2019-09-17 | 信越半导体株式会社 | 固定磨粒钢线及线锯并用的工件的切断方法 |
JP2018034294A (ja) * | 2016-08-31 | 2018-03-08 | 山形県 | ナノカーボン繊維含有固定砥粒ワイヤーソーとその製造方法 |
CN107599193A (zh) * | 2017-05-24 | 2018-01-19 | 浙江好亚能源股份有限公司 | 采用金钢线高精度切割的单晶硅片切片机 |
Also Published As
Publication number | Publication date |
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CN104136169A (zh) | 2014-11-05 |
KR20150020527A (ko) | 2015-02-26 |
HK1200759A1 (en) | 2015-08-14 |
EP2857143A4 (en) | 2016-05-18 |
EP2857143A1 (en) | 2015-04-08 |
PH12014502652A1 (en) | 2015-01-21 |
JPWO2013179434A1 (ja) | 2016-01-14 |
MY185161A (en) | 2021-04-30 |
JP6352176B2 (ja) | 2018-07-04 |
US20150040884A1 (en) | 2015-02-12 |
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