WO2012148165A3 - Catalyseur pour synthèse de fischer-tropsch offrant une excellente capacité de transfert de chaleur - Google Patents

Catalyseur pour synthèse de fischer-tropsch offrant une excellente capacité de transfert de chaleur Download PDF

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Publication number
WO2012148165A3
WO2012148165A3 PCT/KR2012/003184 KR2012003184W WO2012148165A3 WO 2012148165 A3 WO2012148165 A3 WO 2012148165A3 KR 2012003184 W KR2012003184 W KR 2012003184W WO 2012148165 A3 WO2012148165 A3 WO 2012148165A3
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WO
WIPO (PCT)
Prior art keywords
catalyst
heat transfer
fischer
present
excellent heat
Prior art date
Application number
PCT/KR2012/003184
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English (en)
Korean (ko)
Other versions
WO2012148165A2 (fr
Inventor
하경수
천주영
이윤조
백승찬
곽근재
박선주
전기원
Original Assignee
한국화학연구원
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by 한국화학연구원 filed Critical 한국화학연구원
Priority to CN201280019333.8A priority Critical patent/CN103492074B/zh
Priority to CA2833774A priority patent/CA2833774C/fr
Priority to AU2012248972A priority patent/AU2012248972B2/en
Priority to US14/111,658 priority patent/US9012352B2/en
Priority to EP12777039.4A priority patent/EP2703082A4/fr
Publication of WO2012148165A2 publication Critical patent/WO2012148165A2/fr
Publication of WO2012148165A3 publication Critical patent/WO2012148165A3/fr

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/50—Catalysts, in general, characterised by their form or physical properties characterised by their shape or configuration
    • B01J35/51—Spheres
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/89—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with noble metals
    • B01J23/8913—Cobalt and noble metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/89—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with noble metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0215—Coating
    • B01J37/0221—Coating of particles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/024—Multiple impregnation or coating
    • B01J37/0244—Coatings comprising several layers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/024—Multiple impregnation or coating
    • B01J37/0248—Coatings comprising impregnated particles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2/00—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon
    • C10G2/30—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen
    • C10G2/32—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts
    • C10G2/33—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts characterised by the catalyst used
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2/00—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon
    • C10G2/30—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen
    • C10G2/32—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts
    • C10G2/33—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts characterised by the catalyst used
    • C10G2/331—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts characterised by the catalyst used containing group VIII-metals
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2/00—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon
    • C10G2/30—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen
    • C10G2/32—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts
    • C10G2/34—Apparatus, reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/02—Boron or aluminium; Oxides or hydroxides thereof
    • B01J21/04—Alumina

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • General Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

La présente invention concerne un catalyseur pour synthèse de Fischer-Tropsch offrant une excellente capacité de transfert de chaleur. Le catalyseur selon la présente invention comprend : (1) des particules de noyau central, constituées de matériaux de transfert de chaleur (HTM) choisis à partir d'un groupe constitué de métal, d'oxydes métalliques, de céramique, et de leur mélange ; et (2) des particules de couche externe, qui entourent les particules de noyau central, et qui sont fixées aux surfaces des particules de noyau central par une couche de matériau liant. La couche de particules externes comprend un support, ainsi que des particules de catalyseur sous forme de poudre et contenant des particules métalliques supportées sur ledit support. Le catalyseur présentant la double structure de particules susmentionnée, selon la présente invention, offre une excellente capacité de transfert de chaleur, et fait ainsi preuve d'une grande sélectivité sur les hydrocarbures cibles. De ce fait, le catalyseur selon la présente invention peut être efficacement utilisé dans un réacteur à lit fixe en vue d'une synthèse de Fischer-Tropsch servant à produire des hydrocarbures à partir de gaz de synthèse.
PCT/KR2012/003184 2011-04-26 2012-04-25 Catalyseur pour synthèse de fischer-tropsch offrant une excellente capacité de transfert de chaleur WO2012148165A2 (fr)

Priority Applications (5)

Application Number Priority Date Filing Date Title
CN201280019333.8A CN103492074B (zh) 2011-04-26 2012-04-25 具有优良传热能力的用于费-托合成的催化剂
CA2833774A CA2833774C (fr) 2011-04-26 2012-04-25 Catalyseur pour synthese de fischer-tropsch offrant une excellente capacite de transfert de chaleur
AU2012248972A AU2012248972B2 (en) 2011-04-26 2012-04-25 Catalyst for Fischer-Tropsch synthesis having excellent heat transfer capability
US14/111,658 US9012352B2 (en) 2011-04-26 2012-04-25 Catalyst for Fischer-Tropsch synthesis having excellent heat transfer capability
EP12777039.4A EP2703082A4 (fr) 2011-04-26 2012-04-25 Catalyseur pour synthèse de fischer-tropsch offrant une excellente capacité de transfert de chaleur

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
KR1020110038819A KR101297599B1 (ko) 2011-04-26 2011-04-26 우수한 열전달 성능을 갖는 피셔-트롭시 합성용 촉매
KR10-2011-0038819 2011-04-26

Publications (2)

Publication Number Publication Date
WO2012148165A2 WO2012148165A2 (fr) 2012-11-01
WO2012148165A3 true WO2012148165A3 (fr) 2012-12-27

Family

ID=47072898

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/KR2012/003184 WO2012148165A2 (fr) 2011-04-26 2012-04-25 Catalyseur pour synthèse de fischer-tropsch offrant une excellente capacité de transfert de chaleur

Country Status (7)

Country Link
US (1) US9012352B2 (fr)
EP (1) EP2703082A4 (fr)
KR (1) KR101297599B1 (fr)
CN (1) CN103492074B (fr)
AU (1) AU2012248972B2 (fr)
CA (1) CA2833774C (fr)
WO (1) WO2012148165A2 (fr)

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KR101432763B1 (ko) * 2013-01-22 2014-10-01 한국과학기술연구원 피셔-트롭쉬 합성 반응에 사용되는 코발트 담지촉매의 제조방법
CN104289226B (zh) * 2014-09-08 2016-07-06 芜湖市纽泰知识产权信息咨询有限公司 一种多功能固体催化剂
CN104148119B (zh) * 2014-09-08 2016-09-28 芜湖市纽泰知识产权信息咨询有限公司 一种滚动成型的催化剂
CN104162430A (zh) * 2014-09-09 2014-11-26 安徽工程大学 一种蛋壳型的催化剂
CN104162431A (zh) * 2014-09-09 2014-11-26 安徽工程大学 一种滚动成型的蛋壳型催化剂
CN104174443B (zh) * 2014-09-09 2016-04-27 安徽工程大学 一种核壳结构的催化剂
GB2560317A (en) * 2017-03-06 2018-09-12 Sibelco Nederland N V Bed materials for fluidised bed reaction methods and fluidised bed reaction methods
US20210245139A1 (en) * 2018-06-06 2021-08-12 Nexceris Innovation Holdings, Llc. Catalyst support materials, catalyst supports, catalysts and reaction methods using catalysts
KR102572062B1 (ko) * 2021-09-16 2023-08-29 한국화학연구원 이산화탄소의 직접 수소화 반응용 촉매

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US4992406A (en) * 1988-11-23 1991-02-12 Exxon Research And Engineering Company Titania-supported catalysts and their preparation for use in Fischer-Tropsch synthesis
KR20070010190A (ko) * 2004-04-30 2007-01-22 엥겔하드 코포레이션 코어-쉘 촉매, 이의 제조법 및 이의 피셔-트롭시 합성 용도
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Also Published As

Publication number Publication date
US20140038813A1 (en) 2014-02-06
WO2012148165A2 (fr) 2012-11-01
CA2833774C (fr) 2016-07-05
US9012352B2 (en) 2015-04-21
EP2703082A4 (fr) 2014-11-19
AU2012248972B2 (en) 2016-02-04
CN103492074B (zh) 2016-06-22
AU2012248972A1 (en) 2013-11-21
EP2703082A2 (fr) 2014-03-05
KR20120121071A (ko) 2012-11-05
CN103492074A (zh) 2014-01-01
KR101297599B1 (ko) 2013-08-19
CA2833774A1 (fr) 2012-11-01

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