WO2012070835A2 - 모자반 추출물, 청각 추출물 및 참미역 추출물을 함유하는 화장료 조성물 - Google Patents
모자반 추출물, 청각 추출물 및 참미역 추출물을 함유하는 화장료 조성물 Download PDFInfo
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- WO2012070835A2 WO2012070835A2 PCT/KR2011/008910 KR2011008910W WO2012070835A2 WO 2012070835 A2 WO2012070835 A2 WO 2012070835A2 KR 2011008910 W KR2011008910 W KR 2011008910W WO 2012070835 A2 WO2012070835 A2 WO 2012070835A2
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- extract
- seaweed
- cosmetic composition
- skin
- auditory
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9706—Algae
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9706—Algae
- A61K8/9711—Phaeophycota or Phaeophyta [brown algae], e.g. Fucus
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
Definitions
- the present invention relates to a cosmetic composition containing an almond extract, an auditory extract, and a seaweed extract as an active ingredient, and more specifically, contains one or more selected from the group consisting of an alban extract, an auditory extract, and a seaweed extract as an active ingredient. It relates to a cosmetic composition that is excellent in antioxidant effects and improves skin elasticity and wrinkles.
- the skin is divided into three layers of epidermis, dermis and subcutaneous fat tissue in order from the outside, and protects the body from physical and chemical stimuli from the external environment. It controls the evaporation of ⁇ 70% of moisture out of the body.
- the epidermis is separated from the outside in the order of the stratum corneum, granule layer, polar layer, and basal layer.
- the stratum corneum contains about 10-20% moisture and is present at the outermost part of the human body to suppress evaporation of water from the body. Blocks excess penetration of material from outside ( J. Invest. Dermatol. 80 (Suppl.), 44-49. 1983 ).
- the dermis consists of a papillary layer and a reticular layer.
- the papillary layer is composed of connective tissue, which is tough and elastic due to collagenous fibers and some elastic fibers, which is important for skin elasticity (wrinkling). Play a role.
- Subcutaneous tissue is a layer of connective tissue, sometimes called adipose tissue layer.
- Subcutaneous tissue is basically composed of plastic connective tissue scattered in the subcutaneous fat layer, and these fat cells serve as a buffer for preserving and protecting heat and storing calories.
- ROS reactive oxygen species
- cosmetics are intended to clean the body, to make themselves beautiful and attractive, and to prevent aging by protecting the skin or hair from ultraviolet rays or drying.
- the self-consciousness to actively express oneself is increasing, and the desire to care for and maintain the health of one's own skin using cosmetics is increasing.
- the basic and color cosmetics of various forms and formulations are being researched and developed. Among them, skin elasticity improvement and wrinkle improvement cosmetics are recognized as the most important products in various categories.
- seaweed extract which maintains vitality in the extreme environment of the sea and has many good nutrients, is considered to be highly preferred by consumers who want more powerful effects.
- seaweed is a good source of vitamins and minerals as a food, so if you apply it to your skin, it will be a good material to deliver the effect directly to your skin.
- the present inventors conducted a study on the skin efficacy of the seaweed extract, as a result, it was found that the mother and child extract, auditory extract and seaweed extract to improve the oxidative stress of the skin, have the effect of improving the wrinkles of the skin and completed the present invention Was done.
- an object of the present invention is to provide a cosmetic composition excellent in antioxidant effect, skin elasticity and wrinkle improvement effect.
- the present invention provides a cosmetic composition for improving skin antioxidants, skin elasticity and wrinkles as an active ingredient containing an almond extract, auditory extract and seaweed extract.
- the cosmetic composition of the present invention contains an almond extract, an auditory extract, and a seaweed extract to increase skin antioxidant power, and also have an excellent skin elasticity improvement effect and wrinkle improvement effect.
- 1 is a graph showing the protective effect of keratinocytes damage by ultraviolet rays of the mother and child extract, auditory extract and seaweed extract of the present invention.
- the present invention contains at least one member selected from the group consisting of maban extract, auditory extract and seaweed extract as an active ingredient.
- SARGASSUM FULVELLUM used as an active ingredient in the present invention is apparently distinct from the roots, stems, leaves, the roots are kabansang and one central branch to grow 1 to 3m or more.
- the stem is triangular columnar or triangular and twisted. Leaves bend from stem to base, curved, spatula or oval, and midrib to leaf center. The upper leaves are lancet-shaped and serrated at the edges, and bubbles are formed from the stems all over the body. It is dark tan and can be seen from all over Korea.
- the main ingredients are alginic acid, chlorophyll ac, ⁇ -carotene, fucoxanthin, laminarin and mannitol.
- the amount of fat is very low, but when analyzed in powder form, the amount of dietary fiber and fat is over 30%. Hatban is relatively higher in dietary fiber than sugar.
- many varieties of mother and child are usually edible, and are used as raw materials of the seaweed industry such as alginic acid or as fertilizer.
- Alginic acid helps digestion of the stomach and bowel movements, which is good for constipation and is effective in preventing colon cancer. It is good for high blood pressure and osteoporosis due to its high mineral content and good for thyroid dysfunction due to high iodine content.
- CODIUM FRAGILE used as an active ingredient in the present invention has a smooth texture, dark blue color, and a light taste to enhance the taste of kimchi, which is used as an ingredient in kimchi since ancient times. It can be seen that. In Japan, pine trees live in the sea. The height is 10-30cm, the thickness is 1.5-3mm, and the lower side is thicker. The branches are split into deer horns, grow straight, and reach the same height, forming a fan shape. The surface is smooth like a velvety, and under a microscope there is an irregular tangled texture of colorless transparent threads inside the branches. Young ones have hairs on the front, especially on top, but fall later and leave hairless marks.
- the whole body is a structure in which several cell nuclei are contained in one cell because they are all connected without a membrane between cells. Spore containing pouches are club-shaped, 5-7 times the thickness, the top is sharp. It is high in fiber and contains a lot of minerals such as calcium, iron, vitamin A, vitamin C and niacin.
- the seaweed (UNDARIA PINNATIFIDA) used in the present invention is a frond plant with distinct divisions of root, stem and leaf. It is distributed in all coasts of Korea, but not in areas strongly affected by cold currents. Inhabit rocks near low waters, but tend to live deeper in the south and shallower in the north. It is harvested mainly from winter to spring and is the most delicious at this time. Breed from spring to summer. It is the main food of abalone and turban and is mainly used for food in Korea, Japan and China. It is rich in dietary fiber, potassium, calcium, and iodine, which has been widely used since its early metabolism, excellent in postpartum care, prevention of constipation and obesity, and supplementation of iron and calcium.
- the dried product contains 12.7% protein, 52% sugar, 1.1% fat, 1300mg Ca, vitamin A ⁇ 140IU, B1 0.11mg%, B2 0.14mg%, nicotinic acid 10mg%, C 15mg%.
- Seaweed is high in calcium and comparable to powdered milk. It contains 100mg of iodine and is a strong alkaline food. In addition, the seaweed contains alginic acid as a viscous substance, but the root is less than the leaves or stems.
- the main carotenoid pigments in seaweed are fucoxanthine and violaxanthine, and lutein and ⁇ -carotene.
- Mother and child extract, auditory extract and seaweed extract of the present invention can be prepared according to methods conventional in the art.
- the freeze-dried hatpan, hearing, and seaweed may be distilled by steam, and then extracted and purified using glycerin as a solvent.
- the cosmetic composition of the present invention contains 0.001-30% by weight, respectively, of Mabanban extract, hearing extract and seaweed extract based on the total weight of the composition. This is because a pronounced effect can not be expected at less than 0.001% by weight, and if it exceeds 30% by weight, there is no apparent effect increase with increasing content.
- the cosmetic composition of the present invention may increase the skin antioxidant, anti-wrinkle and elasticity improvement effect when mixed with a yamban extract, an auditory extract and a seaweed extract, and three kinds of banban extract, auditory extract and seaweed extract If the mixture is contained, the synergistic effect among the active ingredients is the best skin antioxidant, wrinkle improvement and elasticity improvement effect.
- the external preparation composition for skin contains a cosmetically and dermatologically acceptable medium and / or base.
- a cosmetically and dermatologically acceptable medium and / or base are all formulations suitable for topical application, for example emulsions, suspensions, microemulsions, microcapsules, microgranules or ionic (liposomes) obtained by dispersing an oil phase in a solution, gel, solid or pasty anhydrous product, aqueous phase, and / or It may be provided in the form of a nonionic vesicle dispersant or in the form of a cream, skin, lotion, powder, ointment, spray or cone stick.
- these compositions can be prepared according to conventional methods in the art.
- the topical skin composition according to the present invention may be used in the form of a foam or in the form of an aerosol composition further containing a compressed propellant.
- the external preparation composition for skin is a fatty substance, an organic solvent, a dissolving agent, a thickening agent and a gelling agent, an emollient, an antioxidant, a suspending agent, a stabilizer, a blowing agent, a fragrance, a surfactant, water, an ionic or nonionic emulsifier, Cosmetics or skin such as fillers, metal ion sequestrants and chelating agents, preservatives, vitamins, blockers, wetting agents, essential oils, dyes, pigments, hydrophilic or lipophilic actives, lipid vesicles or any other ingredients commonly used in cosmetics And auxiliaries commonly used in the scientific field. These adjuvants are introduced in amounts generally used in the cosmetic or dermatological fields.
- the lyophilized hatpan, auditory and seaweed were mixed in a 1: 1: 1 weight ratio and distilled with steam for 12 hours.
- the distilled product was obtained by 70% glycerinization and cooling at 4 ° C. for 7 days, followed by purification. .
- the freeze-dried hatpan and auditory were mixed in a 1: 1 weight ratio and distilled with steam for 12 hours, and the distilled product was obtained by purifying at 70 ° C. for 7 days after cooling at 4 ° C. for 7 days.
- the lyophilized mother board and seaweed were mixed in a 1: 1 weight ratio and distilled with steam for 12 hours.
- the distilled product was obtained by purifying at 70 ° C. for 7 days at 4 ° C. and then purifying it.
- Freeze-dried auditory and seaweed was mixed in a 1: 1 weight ratio and distilled with steam for 12 hours.
- the distilled product was obtained by 70% glycerinization, cooled at 4 ° C. for 7 days, and then purified.
- the keratinocytes isolated from the skin tissue of the person in each well of cell culture plate 96 welhyeong 1 ⁇ 10 4 by one insert was attached for 24 hours. After 18 hours, 50 ⁇ l phosphate buffered saline (PBS) was added to each well.
- PBS phosphate buffered saline
- the keratinocytes were irradiated with UV light 30mJ / cm 2 using an ultraviolet B lamp (Model: F15T8, UV B 15W, Sankyo Dennki, Japan), and then PBS was removed and each cell was subjected to keratinocyte culture medium ( keratinocyte growth media, Clonetics, BioWhittacker, MD, USA) 200 ⁇ l was added.
- the mother and child extract, auditory extract, and seaweed extract of the present invention were excellent in protecting skin cells against external stimuli such as ultraviolet rays.
- the group treated with Hatban, auditory and seaweed extract alone increased skin elasticity, and the skin elasticity enhancing effect of the group treated with the mixture was further improved.
- the group treated with a mixture of maban, auditory and seaweed extract had the best skin elasticity enhancing effect.
- the mother and child extract, auditory extract, seaweed extract of the present invention was excellent in improving skin elasticity.
- Fibroblast cell line (cell line) hs68 was used to compare the type 1 procollagen production ability and collagenase synthesis inhibition ability.
- Fibroblasts were attached to a FALCON 48-well plate with 5 ⁇ 10 4 / well and attached, and then treated with Hatban extract, auditory extract, seaweed extract or mixed extract thereof at a concentration of 1 ppm. After 24 hours of incubation, the type 1 procollagen production in the culture layer was determined using a type 1 pN collagen EIA kit. Type 1 procollagen production was corrected by total protein and then compared with each control and experimental group. The results are shown in Table 3 below.
- the group treated with Maban, auditory and seaweed extract alone promoted the production of collagen, and the effect of promoting the production of collagen in the group treated with the mixture was increased.
- the group treated with a mixture of maban, auditory and seaweed extract had the best collagen production promoting effect.
- the mother and child extract, auditory extract, seaweed extract of the present invention was excellent in improving skin wrinkles by promoting collagen production.
- Fibroblasts were attached to a FALCON 48-well plate by 5 ⁇ 10 4 / well, followed by irradiation of 15 mJ / cm 2 of UVB, followed by Hatban extract, auditory extract, seaweed extract or their The mixed extract was treated at 1 ppm concentration. After 24 hours of incubation, the production amount of matrix metalloproteinases (MMP-1), one of collagenases, in the culture supernatant was measured using an MMP-1 ELISA kit. After correcting the amount of MMP-1 to the total protein amount, the results are summarized in Table 4 below.
- MMP-1 matrix metalloproteinases
- the group treated with Maban, auditory, and seaweed extract alone inhibited the synthesis of collagenase
- the effect of inhibiting the synthesis of collagenase of the group treated with a mixture thereof Improved.
- the group treated with a mixture of moth, hearing and seaweed extract was the most effective in inhibiting the synthesis of collagenase.
- the mother and child extract, auditory extract, and seaweed extract of the present invention effectively inhibited collagenase synthesis, thereby improving skin wrinkles.
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Abstract
Description
성분 | 실시예 1 | 실시예 2 | 실시예 3 | 실시예 4 | 실시예 5 | 실시예 6 | 실시예 7 | 비교예 1 | |
1 | 제조예 1 | 1 | 0 | 0 | 0 | 0 | 0 | 0 | 0 |
2 | 제조예 2 | 0 | 1 | 0 | 0 | 0 | 0 | 0 | 0 |
3 | 제조예 3 | 0 | 0 | 1 | 0 | 0 | 0 | 0 | 0 |
4 | 제조예 4 | 0 | 0 | 0 | 1 | 0 | 0 | 0 | 0 |
5 | 제조예 5 | 0 | 0 | 0 | 0 | 1 | 0 | 0 | 0 |
6 | 제조예 6 | 0 | 0 | 0 | 0 | 0 | 1 | 0 | 0 |
7 | 제조예 7 | 0 | 0 | 0 | 0 | 0 | 0 | 1 | 0 |
8 | 정제수 | 잔량 | 잔량 | 잔량 | 잔량 | 잔량 | 잔량 | 잔량 | 잔량 |
9 | 글리세린 | 8 | 8 | 8 | 8 | 8 | 8 | 8 | 8 |
10 | 부틸렌글리콜 | 4 | 4 | 4 | 4 | 4 | 4 | 4 | 4 |
11 | 히알루론산 추출물 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | 5 |
12 | 베타글루칸 | 7 | 7 | 7 | 7 | 7 | 7 | 7 | 7 |
13 | 카보머 | 0.15 | 0.15 | 0.15 | 0.15 | 0.15 | 0.15 | 0.15 | 0.15 |
14 | 트리에탄올아민 | 적량 | 적량 | 적량 | 적량 | 적량 | 적량 | 적량 | 적량 |
15 | 카프릴릭/카프릭 트리글리세라이드 | 8 | 8 | 8 | 8 | 8 | 8 | 8 | 8 |
16 | 스쿠알란 | 5 | 5 | 5 | 5 | 5 | 5 | 5 | 5 |
17 | 세테아릴 글루코사이드 | 1.5 | 1.5 | 1.5 | 1.5 | 1.5 | 1.5 | 1.5 | 1.5 |
18 | 소르비탄 스테아레이트 | 0.4 | 0.4 | 0.4 | 0.4 | 0.4 | 0.4 | 0.4 | 0.4 |
19 | 세테아릴 알코올 | 2 | 2 | 2 | 2 | 2 | 2 | 2 | 2 |
20 | 방부제 | 적량 | 적량 | 적량 | 적량 | 적량 | 적량 | 적량 | 적량 |
시험물질 | 피부탄력효과 |
실시예 1 | 0.31±0.10 |
실시예 2 | 0.27±0.10 |
실시예 3 | 0.37±0.10 |
실시예 4 | 0.49±0.10 |
실시예 5 | 0.33±0.10 |
실시예 6 | 0.40±0.10 |
실시예 7 | 0.41±0.10 |
비교예 1 | 0.22±0.09 |
그룹 | 콜라겐 생성능 |
비타민 C | 27.8% 증가 |
모자반 추출물 | 15.2% 증가 |
청각 추출물 | 11.5% 증가 |
참미역 추출물 | 18.1% 증가 |
모자반 및 청각의 혼합 추출물 | 15.2% 증가 |
모자반 및 참미역의 혼합 추출물 | 20.4% 증가 |
청각 및 참미역의 혼합 추출물 | 19.2% 증가 |
모자반, 청각 및 참미역의혼합 추출물 | 22.9% 증가 |
그룹 | MMP-1 합성능 |
레티노익산 (1M) | 51.6 % 감소 |
모자반 추출물 | 23.1% 감소 |
청각 추출물 | 19.7 % 감소 |
참미역 추출물 | 28.1 % 감소 |
모자반 및 청각의 혼합 추출물 | 23.6% 감소 |
모자반 및 참미역의 혼합 추출물 | 33.1% 감소 |
청각 및 참미역의 혼합 추출물 | 30.9% 감소 |
모자반, 청각 및 참미역의혼합 추출물 | 46.7% 감소 |
Claims (5)
- 유효성분으로 모자반 추출물, 청각 추출물 및 참미역 추출물로 이루어진 군에서 선택된 1종 이상을 유효성분으로 함유하는 화장료 조성물.
- 제 1항에 있어서, 상기 모자반 추출물, 청각 추출물 및 참미역 추출물은 조성물 총 중량에 대하여 각각 0.001~30중량%의 양으로 함유됨을 특징으로 하는 화장료 조성물.
- 제 1항에 있어서, 상기 조성물은 항노화용임을 특징으로 하는 화장료 조성물.
- 제 1항에 있어서, 상기 조성물은 피부 탄력 증진용임을 특징으로 하는 화장료 조성물.
- 제 1항에 있어서, 상기 조성물은 피부 주름 개선용임을 특징으로 하는 화장료 조성물.
Priority Applications (4)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2013540888A JP6007188B2 (ja) | 2010-11-25 | 2011-11-22 | ホンダワラ抽出物、ミル抽出物及びワカメ抽出物を含む化粧料組成物 |
CN201180056083.0A CN103228262B (zh) | 2010-11-25 | 2011-11-22 | 含有马尾藻提取物、海鹿角提取物和褐海藻提取物的化妆品组合物 |
SG2013033550A SG190095A1 (en) | 2010-11-25 | 2011-11-22 | Cosmetic composition containing gulfweed extract, sea staghorn extract, and brown seaweed extract |
HK13114372.4A HK1186966A1 (zh) | 2010-11-25 | 2013-12-30 | 含有馬尾藻提取物、海鹿角提取物和褐海藻提取物的化妝品組合物 |
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Application Number | Priority Date | Filing Date | Title |
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KR1020100118214A KR101839013B1 (ko) | 2010-11-25 | 2010-11-25 | 모자반 추출물, 청각 추출물 및 참미역 추출물을 함유하는 화장료 조성물 |
KR10-2010-0118214 | 2010-11-25 |
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WO2012070835A2 true WO2012070835A2 (ko) | 2012-05-31 |
WO2012070835A3 WO2012070835A3 (ko) | 2012-09-27 |
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PCT/KR2011/008910 WO2012070835A2 (ko) | 2010-11-25 | 2011-11-22 | 모자반 추출물, 청각 추출물 및 참미역 추출물을 함유하는 화장료 조성물 |
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JP (1) | JP6007188B2 (ko) |
KR (1) | KR101839013B1 (ko) |
CN (1) | CN103228262B (ko) |
HK (1) | HK1186966A1 (ko) |
SG (1) | SG190095A1 (ko) |
WO (1) | WO2012070835A2 (ko) |
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KR101893250B1 (ko) | 2015-12-21 | 2018-10-04 | 부경대학교 산학협력단 | 톱니모자반 추출물 또는 이의 분획물을 유효성분으로 포함하는 항산화 조성물 |
KR102564539B1 (ko) * | 2022-12-16 | 2023-08-09 | 부경대학교 산학협력단 | 청각 추출물을 유효성분으로 포함하는 수면장애 또는 불면증의 예방, 개선 또는 치료용 조성물 |
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KR20140097865A (ko) * | 2013-01-30 | 2014-08-07 | 한태준 | 김 추출물을 유효성분으로 함유하는 미백 또는 주름 개선용 화장료 조성물 |
CN105030587B (zh) * | 2015-07-07 | 2017-12-15 | 海南海润生物科技股份有限公司 | 一种含海藻提取物的抗衰老化妆品及其制备方法 |
KR101883543B1 (ko) * | 2016-01-22 | 2018-07-30 | 테 퐁 민 인터내셔널 코., 엘티디. | 알레르기-억제 모자반 추출물, 이의 제조 방법 및 이의 응용 |
JP7278564B2 (ja) * | 2018-05-31 | 2023-05-22 | 日本メナード化粧品株式会社 | ヒアルロン酸産生促進剤、コラーゲン産生促進剤、mmp阻害剤、シワ改善剤、医薬品又は食品組成物 |
KR102049698B1 (ko) | 2019-06-28 | 2020-01-22 | 주식회사 신세계인터코스코리아 | 피부 개선용 화장료 조성물 |
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JP3825882B2 (ja) * | 1997-05-30 | 2006-09-27 | 株式会社ノエビア | 線維芽細胞賦活剤およびこれを含有してなる皮膚外用剤 |
JPH10330280A (ja) * | 1997-05-30 | 1998-12-15 | Noevir Co Ltd | コラーゲン産生促進剤及びこれを含有して成る老化防止用皮膚外用剤 |
US20040219124A1 (en) * | 2003-05-01 | 2004-11-04 | Gupta Shyam K. | Cosmetic and Pharmaceutical Masks Based on Ion-Pair Delivery System |
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- 2011-11-22 CN CN201180056083.0A patent/CN103228262B/zh not_active Expired - Fee Related
- 2011-11-22 WO PCT/KR2011/008910 patent/WO2012070835A2/ko active Application Filing
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KR100576968B1 (ko) * | 2002-07-10 | 2006-05-10 | 시라코 가부시키가이샤 | 해조의 유용성 성분 추출 방법 및 추출액의 용도 |
JP2008239493A (ja) * | 2007-03-23 | 2008-10-09 | Naris Cosmetics Co Ltd | 皮膚外用剤 |
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CN104288083A (zh) * | 2014-09-04 | 2015-01-21 | 杨珍 | 螺旋藻当归活力养肤粉 |
KR101893250B1 (ko) | 2015-12-21 | 2018-10-04 | 부경대학교 산학협력단 | 톱니모자반 추출물 또는 이의 분획물을 유효성분으로 포함하는 항산화 조성물 |
KR102564539B1 (ko) * | 2022-12-16 | 2023-08-09 | 부경대학교 산학협력단 | 청각 추출물을 유효성분으로 포함하는 수면장애 또는 불면증의 예방, 개선 또는 치료용 조성물 |
Also Published As
Publication number | Publication date |
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KR101839013B1 (ko) | 2018-03-15 |
JP6007188B2 (ja) | 2016-10-12 |
WO2012070835A3 (ko) | 2012-09-27 |
SG190095A1 (en) | 2013-06-28 |
CN103228262B (zh) | 2016-02-17 |
JP2013543890A (ja) | 2013-12-09 |
CN103228262A (zh) | 2013-07-31 |
KR20120056594A (ko) | 2012-06-04 |
HK1186966A1 (zh) | 2014-03-28 |
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