WO2012026755A3 - 산화철 나노 입자를 포함하는 메조포러스 카본의 제조방법 - Google Patents

산화철 나노 입자를 포함하는 메조포러스 카본의 제조방법 Download PDF

Info

Publication number
WO2012026755A3
WO2012026755A3 PCT/KR2011/006250 KR2011006250W WO2012026755A3 WO 2012026755 A3 WO2012026755 A3 WO 2012026755A3 KR 2011006250 W KR2011006250 W KR 2011006250W WO 2012026755 A3 WO2012026755 A3 WO 2012026755A3
Authority
WO
WIPO (PCT)
Prior art keywords
mesoporous carbon
iron oxide
oxide nanoparticles
present
preparing
Prior art date
Application number
PCT/KR2011/006250
Other languages
English (en)
French (fr)
Other versions
WO2012026755A9 (ko
WO2012026755A2 (ko
Inventor
김요한
최희철
박호식
Original Assignee
광주과학기술원
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 광주과학기술원 filed Critical 광주과학기술원
Priority to US13/701,978 priority Critical patent/US20130079223A1/en
Priority to CN2011800278172A priority patent/CN102958833A/zh
Publication of WO2012026755A2 publication Critical patent/WO2012026755A2/ko
Publication of WO2012026755A3 publication Critical patent/WO2012026755A3/ko
Publication of WO2012026755A9 publication Critical patent/WO2012026755A9/ko

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/28—Treatment of water, waste water, or sewage by sorption
    • C02F1/288—Treatment of water, waste water, or sewage by sorption using composite sorbents, e.g. coated, impregnated, multi-layered
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00—Carbon; Compounds thereof
    • C01B32/30—Active carbon
    • C01B32/312—Preparation
    • C01B32/342—Preparation characterised by non-gaseous activating agents
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/06—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising oxides or hydroxides of metals not provided for in group B01J20/04
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/20—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising free carbon; comprising carbon obtained by carbonising processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28002—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their physical properties
    • B01J20/28004—Sorbent size or size distribution, e.g. particle size
    • B01J20/28007—Sorbent size or size distribution, e.g. particle size with size in the range 1-100 nanometers, e.g. nanosized particles, nanofibers, nanotubes, nanowires or the like
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28054—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J20/28078—Pore diameter
    • B01J20/28083—Pore diameter being in the range 2-50 nm, i.e. mesopores
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B01J20/3202—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the carrier, support or substrate used for impregnation or coating
    • B01J20/3204—Inorganic carriers, supports or substrates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/32—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating
    • B01J20/3231—Impregnating or coating ; Solid sorbent compositions obtained from processes involving impregnating or coating characterised by the coating or impregnating layer
    • B01J20/3234—Inorganic material layers
    • B01J20/3236—Inorganic material layers containing metal, other than zeolites, e.g. oxides, hydroxides, sulphides or salts
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/28—Treatment of water, waste water, or sewage by sorption
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/28—Treatment of water, waste water, or sewage by sorption
    • C02F1/281—Treatment of water, waste water, or sewage by sorption using inorganic sorbents
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/28—Treatment of water, waste water, or sewage by sorption
    • C02F1/283—Treatment of water, waste water, or sewage by sorption using coal, charred products, or inorganic mixtures containing them
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2305/00—Use of specific compounds during water treatment
    • C02F2305/08—Nanoparticles or nanotubes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Analytical Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • Nanotechnology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Materials Engineering (AREA)
  • Water Supply & Treatment (AREA)
  • Hydrology & Water Resources (AREA)
  • Environmental & Geological Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Composite Materials (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Water Treatment By Sorption (AREA)

Abstract

본 발명은 산화철 나노 입자를 포함하는 메조포러스 카본의 제조방법에 관한 것으로서, 본 발명에 따른 산화철 나노 입자를 포함하는 메조포러스 카본의 제조방법은 1) 산화철 나노 입자를 메조포러스 카본의 표면에 분산 및 포화시키는 단계, 및 2) 상기 메조포러스 카본을 하소시키는 단계를 포함한다. 본 발명에 따라 제조되는 산화철 나노 입자를 포함하는 메조포러스 카본은 유기 물질의 흡착에 매우 뛰어난 효과를 보이며, 반응시간의 단축에 의한 경제성, 편리성의 장점을 지닌다. 따라서, 본 발명에 따른 산화철 나노 입자를 포함하는 메조포러스 카본을 수처리용 흡착제에 적용하여 오염물질 처리효율을 극대화시킬 수 있다.
PCT/KR2011/006250 2010-08-25 2011-08-24 산화철 나노 입자를 포함하는 메조포러스 카본의 제조방법 WO2012026755A2 (ko)

Priority Applications (2)

Application Number Priority Date Filing Date Title
US13/701,978 US20130079223A1 (en) 2010-08-25 2011-08-24 Method for preparing mesoporous carbon having iron oxide nanoparticles
CN2011800278172A CN102958833A (zh) 2010-08-25 2011-08-24 包含氧化铁纳米粒子的介孔碳的制备方法

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
KR1020100082231A KR20120021993A (ko) 2010-08-25 2010-08-25 산화철 나노 입자를 포함하는 메조포러스 카본의 제조방법
KR10-2010-0082231 2010-08-25

Publications (3)

Publication Number Publication Date
WO2012026755A2 WO2012026755A2 (ko) 2012-03-01
WO2012026755A3 true WO2012026755A3 (ko) 2012-05-18
WO2012026755A9 WO2012026755A9 (ko) 2012-07-05

Family

ID=45723931

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/KR2011/006250 WO2012026755A2 (ko) 2010-08-25 2011-08-24 산화철 나노 입자를 포함하는 메조포러스 카본의 제조방법

Country Status (4)

Country Link
US (1) US20130079223A1 (ko)
KR (1) KR20120021993A (ko)
CN (1) CN102958833A (ko)
WO (1) WO2012026755A2 (ko)

Families Citing this family (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2012158194A1 (en) 2010-10-25 2012-11-22 William Marsh Rice University Composite materials for reversible co2 capture
US9597656B2 (en) 2012-01-11 2017-03-21 William Marsh Rice University Porous carbon materials for CO2 separation in natural gas
WO2013106712A1 (en) 2012-01-11 2013-07-18 William Marsh Rice University Composites for carbon dioxide capture
CA2859256A1 (en) 2013-08-13 2015-02-13 William Marsh Rice University Nucleophilic porous carbon materials for co2 and h2s capture
CN103466719B (zh) * 2013-09-22 2014-11-12 南京理工大学 一种在有序介孔碳基体中负载铁状态可控的纳米复合材料的制备方法
CN104190385B (zh) * 2014-08-29 2016-09-14 湖南大学 聚吡咯/Fe3O4/石墨烯复合材料及其制备方法和应用
CN105289111A (zh) * 2015-12-01 2016-02-03 佛山市农业总公司 用于去除饮用水中三氯生的过滤介质、滤芯以及制备方法
CN105964225A (zh) * 2016-07-05 2016-09-28 江苏省海洋资源开发研究院(连云港) 一种吸附剂及其制备方法以及在去除地下水中低浓度砷的应用
CN106512976A (zh) * 2016-10-20 2017-03-22 中国石油化工股份有限公司 有序介孔碳负载纳米二氧化钛催化剂的制备方法及在有机废水处理中的应用
JP6981763B2 (ja) * 2017-03-28 2021-12-17 日鉄ケミカル＆マテリアル株式会社 水質改善材
CN107394168A (zh) * 2017-07-27 2017-11-24 扬州大学 Fe2O3/有序多孔碳复合材料的制备方法
JP6960817B2 (ja) * 2017-09-29 2021-11-05 日鉄ケミカル＆マテリアル株式会社 有価金属回収のための金属捕集材、その製造方法及び有価金属回収方法
JP7237640B2 (ja) * 2018-03-26 2023-03-13 三菱ケミカルアクア・ソリューションズ株式会社 酸性凝集物含有廃液の処理方法および水処理装置
JP7376244B2 (ja) * 2018-03-28 2023-11-08 日鉄ケミカル＆マテリアル株式会社 水質改善材及びその製造方法
CN110142023A (zh) * 2019-04-18 2019-08-20 中国科学院南京土壤研究所 一种纳米四氧化三铁/改性生物炭复合材料及其制备方法和应用
CN111635007A (zh) * 2020-06-05 2020-09-08 江苏启创环境科技股份有限公司 一种水处理磁碳填料的制备方法及应用
CN114887609A (zh) * 2022-05-16 2022-08-12 南京工程学院 一种高效去除腐殖酸的胺化介孔碳材料的制备方法及应用
CN115771890B (zh) * 2022-11-28 2024-02-27 云南中烟工业有限责任公司 一种二维介孔碳的批量化制备方法及用途

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20060157419A1 (en) * 2005-01-14 2006-07-20 Clemson University Activated carbon exhibiting enhanced removal of dissolved natural organic matter from water
KR100917840B1 (ko) * 2009-07-13 2009-09-21 (주)디알씨엔씨 나노구조 탄소구조체 및 그 제조방법
US20090246528A1 (en) * 2006-02-15 2009-10-01 Rudyard Lyle Istvan Mesoporous activated carbons
US20100122708A1 (en) * 2008-11-20 2010-05-20 R. J. Reynolds Tobacco Company Adsorbent Material Impregnated with Metal Oxide Component

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1789507A (en) * 1928-03-22 1931-01-20 Aarts Christianus J Godefridus Process of making an adsorbent comprising carbon, iron, and iron oxide
EP0490317B1 (en) * 1990-12-13 1994-06-08 Mitsubishi Gas Chemical Company, Inc. Active carbon materials, process for the preparation thereof and the use thereof
DE10213016B4 (de) * 2002-03-22 2006-08-17 Helsa-Automotive Gmbh & Co. Kg Mechanisch stabiler, poröser Aktivkohleformkörper, Verfahren zu dessen Herstellung und dessen Verwendung
KR100552697B1 (ko) * 2003-11-13 2006-02-20 삼성에스디아이 주식회사 금속 산화물-탄소 복합체로 이루어진 촉매 담체 및 이를이용한연료전지

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20060157419A1 (en) * 2005-01-14 2006-07-20 Clemson University Activated carbon exhibiting enhanced removal of dissolved natural organic matter from water
US20090246528A1 (en) * 2006-02-15 2009-10-01 Rudyard Lyle Istvan Mesoporous activated carbons
US20100122708A1 (en) * 2008-11-20 2010-05-20 R. J. Reynolds Tobacco Company Adsorbent Material Impregnated with Metal Oxide Component
KR100917840B1 (ko) * 2009-07-13 2009-09-21 (주)디알씨엔씨 나노구조 탄소구조체 및 그 제조방법

Also Published As

Publication number Publication date
WO2012026755A9 (ko) 2012-07-05
KR20120021993A (ko) 2012-03-09
US20130079223A1 (en) 2013-03-28
WO2012026755A2 (ko) 2012-03-01
CN102958833A (zh) 2013-03-06

Similar Documents

Publication Publication Date Title
WO2012026755A3 (ko) 산화철 나노 입자를 포함하는 메조포러스 카본의 제조방법
MX2014002914A (es) Filtro de polímero-nanomaterial a base de carbono de nanomaterial compuesto para la eliminación simultánea de bacterias y metales pesados.
WO2008093661A1 (ja) ナノカーボン集合体、及び、その製造方法
WO2009134492A3 (en) Functionalized graphene sheets having high carbon to oxygen ratios
WO2012166471A3 (en) Hydrocarbon transformations using carbocatalysts
WO2013015559A3 (ko) 그래핀의 원자층 식각 방법
WO2011090993A3 (en) High-capacitance and low-oxygen porous carbon for edlcs
EP2611549A4 (en) METALLIC SUBSTRATES HAVING CARBON NANOTUBES DEVELOPED THEREON AND PROCESSES FOR PRODUCING THE SAME
WO2013003836A3 (en) Hybrid materials and nanocomposite materials, methods of making same, and uses thereof
WO2012082717A3 (en) Porous metal dendrites for high efficiency aqueous reduction of co2 to hydrocarbons
WO2008133181A1 (ja) NOｘ 吸着材の製造方法及びNOｘ 吸着材
MY167237A (en) Dopant ink composition and method of fabricating a solar cell there from
JP2012099494A5 (ko)
PH12014502878B1 (en) Apparatus and method for biological sewage treatment
GB2472373B (en) A runflat device and a method for fitting the same
MY161878A (en) Method for the production of an scr-active zeolite catalyst, and scr-active zeolite catalyst
WO2011156906A3 (en) Process for treating a flue gas
WO2014099843A3 (en) Photocatalytic system for the reduction of carbon dioxide
Zhang et al. Porous Mn2O3/p SiO2 nanocomposites on bio-scaffolds for tetracycline degradation
IN2014DN10937A (ko)
CN109529888A (zh) 三维石墨烯基非均相芬顿催化剂、其制备方法及其应用
SG2013043237A (en) Adsorbent for chloride removal
Liu et al. Insights into nitrogen doped sulfur-existed carbonaceous material toward acetaminophen removal by peroxymonosulfate activation
CN103058353A (zh) 一种膜法催化臭氧化去除水中污染物的方法
WO2012057445A3 (en) Gas storage material and method for gas storage

Legal Events

Date Code Title Description
WWE Wipo information: entry into national phase

Ref document number: 201180027817.2

Country of ref document: CN

121 Ep: the epo has been informed by wipo that ep was designated in this application

Ref document number: 11820182

Country of ref document: EP

Kind code of ref document: A2

WWE Wipo information: entry into national phase

Ref document number: 13701978

Country of ref document: US

NENP Non-entry into the national phase

Ref country code: DE

122 Ep: pct application non-entry in european phase

Ref document number: 11820182

Country of ref document: EP

Kind code of ref document: A2