WO2011142649A3 - Proceso para modificar las propiedades fisicoquímicas de zeolitas del tipo faujasita y - Google Patents

Proceso para modificar las propiedades fisicoquímicas de zeolitas del tipo faujasita y Download PDF

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Publication number
WO2011142649A3
WO2011142649A3 PCT/MX2011/000055 MX2011000055W WO2011142649A3 WO 2011142649 A3 WO2011142649 A3 WO 2011142649A3 MX 2011000055 W MX2011000055 W MX 2011000055W WO 2011142649 A3 WO2011142649 A3 WO 2011142649A3
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WIPO (PCT)
Prior art keywords
faujasite
type zeolite
altered
altering
physico
Prior art date
Application number
PCT/MX2011/000055
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English (en)
French (fr)
Other versions
WO2011142649A2 (es
Inventor
Héctor ARMENDÁRIZ HERRERA
María de Lourdes Alejandra GUZMÁN CASTILLO
Francisco Javier HERNÁNDEZ BELTRÁN
Patricia PÉREZ ROMO
Jaime SÁNCHEZ VALENTE
José Marie Maurice JULIEN FRIPIAT
Original Assignee
Instituto Mexicano Del Petróleo
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Instituto Mexicano Del Petróleo filed Critical Instituto Mexicano Del Petróleo
Priority to BR112012029079-7A priority Critical patent/BR112012029079B1/pt
Priority to EP11780865.9A priority patent/EP2570386B1/en
Priority to US13/697,566 priority patent/US9492817B2/en
Priority to CN201180034735.0A priority patent/CN103003202B/zh
Publication of WO2011142649A2 publication Critical patent/WO2011142649A2/es
Publication of WO2011142649A3 publication Critical patent/WO2011142649A3/es
Priority to US15/262,988 priority patent/US10300466B2/en

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/08—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the faujasite type, e.g. type X or Y
    • B01J29/084—Y-type faujasite
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/80—Mixtures of different zeolites
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/64—Pore diameter
    • B01J35/647—2-50 nm
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/64—Pore diameter
    • B01J35/651—50-500 nm
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/66—Pore distribution
    • B01J35/69—Pore distribution bimodal
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • B01J37/10—Heat treatment in the presence of water, e.g. steam
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/026—After-treatment
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/06—Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/20—Faujasite type, e.g. type X or Y
    • C01B39/24—Type Y
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G11/00—Catalytic cracking, in the absence of hydrogen, of hydrocarbon oils
    • C10G11/02—Catalytic cracking, in the absence of hydrogen, of hydrocarbon oils characterised by the catalyst used
    • C10G11/04—Oxides
    • C10G11/05—Crystalline alumino-silicates, e.g. molecular sieves
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G11/00—Catalytic cracking, in the absence of hydrogen, of hydrocarbon oils
    • C10G11/14—Catalytic cracking, in the absence of hydrogen, of hydrocarbon oils with preheated moving solid catalysts
    • C10G11/18—Catalytic cracking, in the absence of hydrogen, of hydrocarbon oils with preheated moving solid catalysts according to the "fluidised-bed" technique
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/10—After treatment, characterised by the effect to be obtained
    • B01J2229/22—After treatment, characterised by the effect to be obtained to destroy the molecular sieve structure or part thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30—After treatment, characterised by the means used
    • B01J2229/34—Reaction with organic or organometallic compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30—After treatment, characterised by the means used
    • B01J2229/40—Special temperature treatment, i.e. other than just for template removal
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/60—Synthesis on support
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/60—Synthesis on support
    • B01J2229/62—Synthesis on support in or on other molecular sieves
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/041—Mesoporous materials having base exchange properties, e.g. Si/Al-MCM-41
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • B01J31/0201—Oxygen-containing compounds
    • B01J31/0202—Alcohols or phenols
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • B01J31/0234—Nitrogen-, phosphorus-, arsenic- or antimony-containing compounds
    • B01J31/0235—Nitrogen containing compounds
    • B01J31/0239—Quaternary ammonium compounds
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/16—Pore diameter
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1037—Hydrocarbon fractions
    • C10G2300/1044—Heavy gasoline or naphtha having a boiling range of about 100 - 180 °C

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Geology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Catalysts (AREA)
  • Nanotechnology (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)

Abstract

La presente invención se relaciona con un proceso que modifica las propiedades de Zeolitas del tipo Faujasita Y, empleadas como base de catalizadores para el proceso FCC, de interés en la industria de la refinación del petróleo, en el cual se realiza la conversión de fracciones pesadas en fracciones más ligeras de alto valor comercial. En una sola etapa produce: una Zeolita de tipo Faujasita Y modificada, con un contenido de sodio menor que el de la Zeolita de tipo Faujasita Y de origen, hasta en un 75 %; y un material mesoporoso asociado a la Zeolita de tipo Faujasita Y modificada, con un tamaño promedio de poros de 2 a 100 nm, en donde los materiales producidos presentan una distribución bimodal o multimodal de poros, y la proporción de Zeolita de tipo Faujasita Y modificada, respecto al material mesoporoso asociado a dicha Zeolita, se regula mediante las condiciones de operación del proceso.
PCT/MX2011/000055 2010-05-14 2011-05-13 Proceso para modificar las propiedades fisicoquímicas de zeolitas del tipo faujasita y WO2011142649A2 (es)

Priority Applications (5)

Application Number Priority Date Filing Date Title
BR112012029079-7A BR112012029079B1 (pt) 2010-05-14 2011-05-13 Processo para modificar as propriedades físico-químicas de zeólitas do tipo faujasita y
EP11780865.9A EP2570386B1 (en) 2010-05-14 2011-05-13 Process for altering the physico-chemical properties of faujasite y-type zeolites
US13/697,566 US9492817B2 (en) 2010-05-14 2011-05-13 Process for altering the physico-chemical properties of Faujasite Y-type zeolites
CN201180034735.0A CN103003202B (zh) 2010-05-14 2011-05-13 改进八面沸石y型沸石的物理化学性质的方法
US15/262,988 US10300466B2 (en) 2010-05-14 2016-09-12 Process for modifying the physical and chemical properties of faujasite Y-type zeolites

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
MXMX/A/2010/005333 2010-05-14
MX2010005333A MX2010005333A (es) 2010-05-14 2010-05-14 Proceso para modificar las propiedades fisicoquimicas de zeolitas del tipo faujasita y.

Related Child Applications (2)

Application Number Title Priority Date Filing Date
US13/697,566 A-371-Of-International US9492817B2 (en) 2010-05-14 2011-05-13 Process for altering the physico-chemical properties of Faujasite Y-type zeolites
US15/262,988 Continuation US10300466B2 (en) 2010-05-14 2016-09-12 Process for modifying the physical and chemical properties of faujasite Y-type zeolites

Publications (2)

Publication Number Publication Date
WO2011142649A2 WO2011142649A2 (es) 2011-11-17
WO2011142649A3 true WO2011142649A3 (es) 2012-01-19

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PCT/MX2011/000055 WO2011142649A2 (es) 2010-05-14 2011-05-13 Proceso para modificar las propiedades fisicoquímicas de zeolitas del tipo faujasita y

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Country Link
US (2) US9492817B2 (es)
EP (1) EP2570386B1 (es)
CN (1) CN103003202B (es)
BR (1) BR112012029079B1 (es)
MX (1) MX2010005333A (es)
WO (1) WO2011142649A2 (es)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
MX2010005333A (es) * 2010-05-14 2011-11-23 Mexicano Inst Petrol Proceso para modificar las propiedades fisicoquimicas de zeolitas del tipo faujasita y.
CN103172082B (zh) * 2013-04-25 2014-10-22 哈尔滨工业大学 一种含介孔的y型分子筛的制备方法
CN106608640B (zh) * 2015-10-26 2019-02-01 中国石油化工股份有限公司 一种由NaY改性得到的分子筛
CN106608642B (zh) * 2015-10-26 2019-07-23 中国石油化工股份有限公司 一种介孔分子筛及其制备方法
CN106927477B (zh) * 2015-12-30 2019-04-16 中国石油化工股份有限公司 一种介孔y型分子筛的制备方法
CN106927480B (zh) * 2015-12-30 2019-03-22 中国石油化工股份有限公司 一种y型分子筛的改性方法
CN106927481B (zh) * 2015-12-30 2019-09-24 中国石油化工股份有限公司 一种介孔y型分子筛的制备方法
CN107344107B (zh) * 2016-05-05 2019-10-15 中国石油化工股份有限公司 一种加氢改质催化剂及其制备方法
MX2016016674A (es) 2016-12-15 2018-06-14 Mexicano Inst Petrol Proceso de despolimerizacion y desoxigenacion de lignina para la obtencion de compuestos aromaticos y su composicion catalitica de reaccion.
CN106955731B (zh) * 2017-03-29 2019-08-13 钦州学院 一种用于蒽氧化制备蒽醌的催化剂的制备方法
CN113120920B (zh) * 2019-12-31 2022-08-12 中国石油化工股份有限公司 一种y沸石处理方法

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Also Published As

Publication number Publication date
EP2570386A2 (en) 2013-03-20
EP2570386B1 (en) 2015-08-19
MX2010005333A (es) 2011-11-23
US20160375427A1 (en) 2016-12-29
BR112012029079B1 (pt) 2022-02-22
EP2570386A4 (en) 2014-01-29
CN103003202A (zh) 2013-03-27
BR112012029079A2 (pt) 2016-08-16
US9492817B2 (en) 2016-11-15
US10300466B2 (en) 2019-05-28
US20130171058A1 (en) 2013-07-04
WO2011142649A2 (es) 2011-11-17
CN103003202B (zh) 2015-07-01

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