WO2011102037A1 - 無段変速機用潤滑油組成物 - Google Patents

無段変速機用潤滑油組成物 Download PDF

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Publication number
WO2011102037A1
WO2011102037A1 PCT/JP2010/070914 JP2010070914W WO2011102037A1 WO 2011102037 A1 WO2011102037 A1 WO 2011102037A1 JP 2010070914 W JP2010070914 W JP 2010070914W WO 2011102037 A1 WO2011102037 A1 WO 2011102037A1
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Prior art keywords
mass
continuously variable
kinematic viscosity
variable transmission
viscosity
Prior art date
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Ceased
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PCT/JP2010/070914
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English (en)
French (fr)
Japanese (ja)
Inventor
裕 藤田
俊彦 市橋
小島　健嗣
慶江 荒川
前田　誠
臼木　秀樹
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Idemitsu Kosan Co Ltd
JATCO Ltd
Original Assignee
Idemitsu Kosan Co Ltd
JATCO Ltd
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Publication date
Application filed by Idemitsu Kosan Co Ltd, JATCO Ltd filed Critical Idemitsu Kosan Co Ltd
Priority to CN201080064070.3A priority Critical patent/CN102770516B/zh
Priority to EP10846168.2A priority patent/EP2537914B1/en
Priority to US13/579,636 priority patent/US9725672B2/en
Priority to KR1020127024013A priority patent/KR101777892B1/ko
Publication of WO2011102037A1 publication Critical patent/WO2011102037A1/ja
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

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    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
    • C10M2219/044—Sulfonic acids, Derivatives thereof, e.g. neutral salts
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
    • C10M2219/046—Overbased sulfonic acid salts
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/10—Heterocyclic compounds containing sulfur, selenium or tellurium compounds in the ring
    • C10M2219/104—Heterocyclic compounds containing sulfur, selenium or tellurium compounds in the ring containing sulfur and carbon with nitrogen or oxygen in the ring
    • C10M2219/106—Thiadiazoles
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
    • C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
    • C10M2223/04—Phosphate esters
    • C10M2223/045—Metal containing thio derivatives
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2229/00—Organic macromolecular compounds containing atoms of elements not provided for in groups C10M2205/00, C10M2209/00, C10M2213/00, C10M2217/00, C10M2221/00 or C10M2225/00 as ingredients in lubricant compositions
    • C10M2229/02—Unspecified siloxanes; Silicones
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2020/00—Specified physical or chemical properties or characteristics, i.e. function, of component of lubricating compositions
    • C10N2020/01—Physico-chemical properties
    • C10N2020/02—Viscosity; Viscosity index
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2020/00—Specified physical or chemical properties or characteristics, i.e. function, of component of lubricating compositions
    • C10N2020/01—Physico-chemical properties
    • C10N2020/04—Molecular weight; Molecular weight distribution
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/02—Pour-point; Viscosity index
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/04—Oil-bath; Gear-boxes; Automatic transmissions; Traction drives
    • C10N2040/045—Oil-bath; Gear-boxes; Automatic transmissions; Traction drives for continuous variable transmission [CVT]

Definitions

  • the present invention relates to a lubricating oil composition for a continuously variable transmission. Specifically, the present invention relates to a lubricating oil composition for continuously variable transmissions having a low viscosity and a high viscosity index, good shear stability, and a long fatigue life.
  • Patent Document 1 reports that a lubricating oil composition capable of maintaining the transmission characteristics and the like for a long period of time is blended and optimized with various additives.
  • the kinematic viscosity is high, and the fatigue life when the viscosity is reduced has not been studied.
  • so-called high viscosity index that lowers the low temperature side viscosity while maintaining the high temperature side viscosity is desired.
  • the lubricating oil composition disclosed in Patent Document 2 uses polymethacrylate (PMA) as a viscosity index improver to improve the viscosity index.
  • the lubricating oil compositions disclosed in Patent Document 3 and Patent Document 4 are high-viscosity synthetic oils (poly- ⁇ -olefins: PAO) that improve viscosity characteristics and are effective in improving fatigue life. (OCP) is blended.
  • Patent Document 2 has a problem that the viscosity index is improved but the oil film maintenance property is inferior.
  • patent documents 3 and 4 the viscosity index more than the viscosity index which PAO has by the mixing
  • an object of the present invention is to provide a lubricating oil composition for a continuously variable transmission having a low viscosity and a high viscosity index, good shear stability, and a long fatigue life.
  • the present invention provides the following lubricating oil composition for continuously variable transmissions.
  • a lubricating oil composition for a continuously variable transmission wherein (A) the sulfur content is 0.03% by mass or less, and the kinematic viscosity at 100 ° C. is 1.5 mm 2 / s to 3 mm 2 / s.
  • at least one of mineral oil and poly- ⁇ -olefin is 45% by mass to 65% by mass based on the total amount of the composition, and (B) the sulfur content is 0.03% by mass or less.
  • (C) 100 wherein at least one of mineral oil and poly- ⁇ -olefin having a viscosity of 5.5 mm 2 / s to 8 mm 2 / s is 10% by mass to 20% by mass based on the total amount of the composition.
  • the chlorate is blended in an amount of 8% by mass or more and 14% by mass or less based on the total amount of the composition, and the total amount of the component (C) and the component (D) is 19% by mass or more,
  • a lubricating oil composition for a continuously variable transmission wherein the viscosity is 5.5 mm 2 / s or more and 6.5 mm 2 / s or less and the kinematic viscosity at ⁇ 20 ° C. is 680 mm 2 / s or less.
  • the kinematic viscosity at 100 ° C. of the component (A) is 1.5 mm 2 / s to 2.5 mm 2 / s
  • the component (B) The kinematic viscosity at 100 ° C. is 5.5 mm 2 / s to 7.5 mm 2 / s
  • the mass average molecular weight of the component (D) is 10,000 to 30000
  • the kinematic viscosity at 100 ° C. is 5.
  • a lubricating oil composition for a continuously variable transmission wherein the lubricating oil composition is 8 mm 2 / s or more and 6.5 mm 2 / s or less.
  • component (B) has a kinematic viscosity at 100 ° C. of 5.5 mm 2 / s to 7.0 mm 2 / s, (D And a component having a mass average molecular weight of 15000 or more and 30000 or less, and a kinematic viscosity at ⁇ 20 ° C. of 660 mm 2 / s or less.
  • a lubricating oil composition for a continuously variable transmission wherein the lubricating oil composition for a continuously variable transmission is used in a belt type continuously variable transmission.
  • a lubricating oil composition for a continuously variable transmission having a low viscosity and a high viscosity index, good shear stability, and a long fatigue life.
  • the lubricating oil composition for continuously variable transmission of the present invention can be suitably used particularly for a belt type continuously variable transmission.
  • the lubricating oil composition of the present invention is characterized by blending the components (A) to (D) described above. Details will be described below.
  • component (A) In the continuously variable transmission lubricating oil composition of the present invention, as component (A), the sulfur content is 0.03% by mass or less, and the kinematic viscosity at 100 ° C. is 1.5 mm 2 / s or more and 3 mm 2 / s or less.
  • a mineral oil and a poly- ⁇ -olefin hereinafter also referred to as PAO
  • PAO poly- ⁇ -olefin
  • mineral oil used in component (A) for example, a lubricating oil fraction obtained by subjecting crude oil to atmospheric distillation and vacuum distillation is subjected to solvent removal, solvent extraction, hydrocracking, solvent dewaxing, catalytic dewaxing.
  • paraffinic and naphthenic compounds which are purified by appropriately combining purification treatment such as hydrorefining, sulfuric acid washing, or clay treatment, can be suitably used.
  • PAO for example, 1-octene oligomer, 1-decene oligomer and the like can be used.
  • mineral oils and PAOs those having a kinematic viscosity at 100 ° C. within the above range may be used alone, or two or more selected from these may be mixed and used in an arbitrary ratio. Good.
  • the component (B) has a sulfur content of 0.03% by mass or less, and a kinematic viscosity at 100 ° C. of 5.5 mm 2 / s to 8 mm 2 / s.
  • a mineral oil and a poly- ⁇ -olefin of 5.5 mm 2 / s to 7.5 mm 2 / s is blended in an amount of 10% by mass to 20% by mass based on the total amount of the composition. .
  • the mineral oil or poly- ⁇ -olefin blended in the component (B) can be the same as that blended in the component (A) described above.
  • [C component] CVT lubricating oil composition of the present invention (C) as component a kinematic viscosity at 100 ° C. is 30 mm 2 / s or more 400 mm 2 / s the following poly - ⁇ - olefin 5 wt% or more 12 wt% It is blended below.
  • the kinematic viscosity at 100 ° C. is less than 30 mm 2 / s, the viscosity index is lowered, and when it exceeds 400 mm 2 / s, the shear stability is lowered, which is not preferable.
  • the blending amount When the blending amount is less than 5% by mass, the viscosity of the finished lubricating oil composition is lowered, and when used for a continuously variable transmission, there is a possibility that the wear of machine parts may increase. If the blending amount exceeds 12% by mass, there is a case where the viscosity increases and the friction loss increases, which is not preferable.
  • the component (D) has a weight average molecular weight of 10,000 to 40,000, preferably a weight average molecular weight of 10,000 to 30,000, more preferably a weight average molecular weight of 15,000 to 30,000. 8 to 14% by mass of the following polymethacrylate (hereinafter also referred to as PMA) is blended.
  • PMA polymethacrylate
  • the mass average molecular weight is less than 10,000, the viscosity index decreases, which is not preferable. If the mass average molecular weight is more than 40,000, there may be a disadvantage that the shear stability is lowered.
  • the blending amount is less than 8% by mass on the basis of the total amount of the lubricating oil composition, the viscosity of the lubricating oil composition is lowered, and there is a possibility that the wear of machine parts may increase when used for a continuously variable transmission. .
  • the blending amount exceeds 12% by mass, the viscosity of the lubricating oil composition increases, and there may be a disadvantage that friction loss increases when used for a continuously variable transmission.
  • the total amount of component (C) and component (D) is preferably 19% by mass or more, more preferably 19% by mass or more and 40% by mass or less, based on the total amount of the composition.
  • the lubricating oil composition of the present invention has a viscosity that can be suitably used for a continuously variable transmission.
  • the lubricating oil composition of the present invention may further contain other additives such as detergents, ashless dispersants, antiwear agents, friction modifiers, anti-proofing agents as necessary, as long as the effects of the present invention are not impaired. You may mix
  • a preferable blending amount is about 0.01% by mass or more and 10% by mass or less based on the total amount of the composition.
  • the ashless dispersant include succinimides, boron-containing succinimides, benzylamines, boron-containing benzylamines, succinic esters, monovalent or divalent typified by fatty acids or succinic acid. Examples thereof include amides of carboxylic acids.
  • a preferable blending amount of the ashless dispersant is about 0.1% by mass or more and 20% by mass or less based on the total amount of the composition.
  • the antiwear agent examples include sulfur type antiwear agents such as thiophosphate metal salts (Zn, Pb, Sb, etc.) and thiocarbamic acid metal salts (Zn, etc.), phosphate esters (tricresyl phosphate), and the like. And phosphorus-based antiwear agents.
  • a preferable blending amount of the antiwear agent is about 0.05% by mass or more and 5% by mass or less based on the total amount of the composition.
  • the friction modifier examples include polyhydric alcohol partial esters such as neopentyl glycol monolaurate, trimethylolpropane monolaurate, and glycerin monooleate (oleic acid monoglyceride).
  • a preferable blending amount of the friction modifier is about 0.05% by mass or more and 4% by mass or less based on the composition.
  • the rust inhibitor examples include fatty acid, alkenyl succinic acid half ester, fatty acid soap, alkyl sulfonate, polyhydric alcohol fatty acid ester, fatty acid amide, oxidized paraffin, alkyl polyoxyethylene ether, and the like.
  • a preferable blending amount of the rust inhibitor is about 0.01% by mass or more and 3% by mass or less based on the total amount of the composition.
  • the metal deactivator examples include benzotriazole, benzotriazole derivatives, triazole, triazole derivatives, imidazole, imidazole derivatives, thiadiazole, and the like, and these are used alone or in combination of two or more.
  • a preferable blending amount of the metal deactivator is about 0.01% by mass or more and 5% by mass or less based on the total amount of the composition.
  • the antifoaming agent for example, a silicone compound, an ester compound, or the like is used alone or in combination of two or more.
  • a preferable blending amount of the antifoaming agent is about 0.05% by mass or more and 5% by mass or less based on the total amount of the composition.
  • the antioxidant hindered phenol-based or amine-based, zinc alkyldithiophosphate (ZnDTP) or the like is preferably used.
  • ZnDTP zinc alkyldithiophosphate
  • the phenol type bisphenol type and ester group-containing phenol type are particularly suitable.
  • As the amine system a dialkyldiphenylamine system or a naphthylamine system is suitable.
  • a preferable blending amount of the antioxidant is about 0.05% by mass or more and 7% by mass or less.
  • the lubricating oil composition for continuously variable transmissions of the present invention comprising the above components has a kinematic viscosity at 100 ° C. of 5.5 mm 2 / s to 6.5 mm 2 / s, preferably 5.8 mm 2 / s. s to 6.5 mm 2 / s, and the kinematic viscosity at ⁇ 20 ° C. is 680 mm 2 / s or less, preferably 660 mm 2 / s or less.
  • the kinematic viscosity at 100 ° C. is less than 5.5 mm 2 / s, when used in a continuously variable transmission, the wearability of machine parts increases, and the reliability and durability of the machine decrease.
  • the lubricating oil composition for continuously variable transmission satisfies the above-described components, blending amount, and viscosity, so that it has low viscosity and high viscosity index, and has good shear stability.
  • the fatigue life of machine parts can be kept long.
  • Examples 1 to 5 A composition for a continuously variable transmission was prepared with the composition shown in Table 1.
  • the kinematic viscosity at 100 ° C. and ⁇ 20 ° C., the BF viscosity at ⁇ 40 ° C., the viscosity after shearing, and the rolling four-ball fatigue life were as follows: It measured by the method shown in.
  • the components described in Table 1 are as follows.
  • Mineral oil-1 Mineral oil mineral oil having a sulfur content of 0.03% by mass or less and a kinematic viscosity at 100 ° C. of 2.2 mm 2 / s and a kinematic viscosity at 40 ° C.
  • PAO-1 having a kinematic viscosity at 100 ° C. of 6.5 mm 2 / s and a kinematic viscosity at 40 ° C. of 37 mm 2 / s: PAO having a kinematic viscosity at 100 ° C. of 1.8 mm 2 / s
  • PAO-2 PAO having a kinematic viscosity at 100 ° C. of 3.9 mm 2 / s
  • PAO-3 PAO having a kinematic viscosity at 100 ° C.
  • PAO-4 PAO with a kinematic viscosity at 100 ° C. of 100 mm 2 / s
  • PMA-1 Polymethacrylate PMA-2 having a weight average molecular weight of 20000: Additive for polymethacrylate CVT oil having a weight average molecular weight of 50,000: detergent (Ca sulfonate, etc.), dispersant (succinimide, etc.), extreme pressure additive and A package containing antiwear agents (sulfides, phosphate compounds, phosphorus sulfide compounds, etc.), antifoaming agents, copper deactivators, etc.
  • Rolling 4-ball fatigue life A rolling four-ball test was used to measure the time at which pitching occurred. The measurement conditions were a SUJ-2 3/4 inch ball, a load of 6.9 GPa, a rotation speed of 2200 rpm, and an oil temperature of 90 ° C.
  • the lubricating oil composition of the present invention since the lubricating oil composition of the present invention has a low viscosity and a high viscosity index and high low temperature fluidity, it has less friction loss when used for a continuously variable transmission compared to a commercially available product. This indicates that the cold startability is good, that is, fuel consumption can be reduced. In addition, in the kinematic viscosity after shearing and the rolling four-ball fatigue life test, the values corresponding to the commercially available products are maintained. Therefore, the lubricating oil composition of the present invention has a low viscosity and a high viscosity index, good shear stability, and a long fatigue life.
  • Comparative Examples 1 to 4 including commercial products, no low viscosity, high viscosity index, low temperature fluidity, shear stability, and fatigue life are seen compared to the Examples. .
  • Comparative Example 1 has a high kinematic viscosity at ⁇ 20 ° C. and a short fatigue life.
  • Comparative Example 2 has a low kinematic viscosity after shearing and a short fatigue life.
  • Comparative Example 3 has a large BF viscosity and is inferior in low-temperature fluidity. Since Comparative Example 4 has a low kinematic viscosity at 100 ° C., the kinematic viscosity after shearing is also low, a suitable value cannot be maintained, and the fatigue life is shortened.
  • the present invention can be used as a lubricating oil for a transmission, and can be suitably used particularly for a belt type continuously variable transmission of an automobile.

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  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • Engineering & Computer Science (AREA)
  • Lubricants (AREA)
PCT/JP2010/070914 2010-02-17 2010-11-24 無段変速機用潤滑油組成物 Ceased WO2011102037A1 (ja)

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CN201080064070.3A CN102770516B (zh) 2010-02-17 2010-11-24 无级变速器用润滑油组合物
EP10846168.2A EP2537914B1 (en) 2010-02-17 2010-11-24 Lubricant composition for continuously variable transmission
US13/579,636 US9725672B2 (en) 2010-02-17 2010-11-24 Method for lubricating a continuously variable transmission, and a continuously variable transmission
KR1020127024013A KR101777892B1 (ko) 2010-02-17 2010-11-24 무단 변속기용 윤활유 조성물

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EP2537914A4 (en) 2013-12-11
US20120316092A1 (en) 2012-12-13
KR101777892B1 (ko) 2017-09-12
CN102770516A (zh) 2012-11-07
CN102770516B (zh) 2014-04-02
EP2537914A1 (en) 2012-12-26
JP2011168677A (ja) 2011-09-01
KR20130001245A (ko) 2013-01-03
US9725672B2 (en) 2017-08-08
JP5646859B2 (ja) 2014-12-24
EP2537914B1 (en) 2018-03-28

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