WO2009116264A1 - Son de céréale sec dégraissé contenant un ingrédient diététique adsorbé et concentré, concentré d'ingrédient diététique préparé à partir du son et son procédé de fabrication - Google Patents

Son de céréale sec dégraissé contenant un ingrédient diététique adsorbé et concentré, concentré d'ingrédient diététique préparé à partir du son et son procédé de fabrication Download PDF

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Publication number
WO2009116264A1
WO2009116264A1 PCT/JP2009/001169 JP2009001169W WO2009116264A1 WO 2009116264 A1 WO2009116264 A1 WO 2009116264A1 JP 2009001169 W JP2009001169 W JP 2009001169W WO 2009116264 A1 WO2009116264 A1 WO 2009116264A1
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WIPO (PCT)
Prior art keywords
polar
cereal meal
health
dried
producing
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PCT/JP2009/001169
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English (en)
Japanese (ja)
Inventor
潮秀樹
長阪玲子
大原和幸
寺島亜実
福森武
金本繁晴
若林敬士
前原裕之
Original Assignee
国立大学法人東京海洋大学
株式会社サタケ
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Publication of WO2009116264A1 publication Critical patent/WO2009116264A1/fr

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    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23K—FODDER
    • A23K50/00—Feeding-stuffs specially adapted for particular animals
    • A23K50/80—Feeding-stuffs specially adapted for particular animals for aquatic animals, e.g. fish, crustaceans or molluscs
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23K—FODDER
    • A23K20/00—Accessory food factors for animal feeding-stuffs
    • A23K20/10—Organic substances
    • A23K20/111—Aromatic compounds
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A23L33/105—Plant extracts, their artificial duplicates or their derivatives
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A23L33/15—Vitamins
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L7/00—Cereal-derived products; Malt products; Preparation or treatment thereof
    • A23L7/10—Cereal-derived products
    • A23L7/101—Addition of antibiotics, vitamins, amino-acids, or minerals
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L7/00—Cereal-derived products; Malt products; Preparation or treatment thereof
    • A23L7/10—Cereal-derived products
    • A23L7/115—Cereal fibre products, e.g. bran, husk
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
    • Y02A40/80—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in fisheries management
    • Y02A40/81—Aquaculture, e.g. of fish
    • Y02A40/818—Alternative feeds for fish, e.g. in aquacultures
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P60/00—Technologies relating to agriculture, livestock or agroalimentary industries
    • Y02P60/80—Food processing, e.g. use of renewable energies or variable speed drives in handling, conveying or stacking
    • Y02P60/87—Re-use of by-products of food processing for fodder production

Definitions

  • the present invention relates to a dried defatted cereal meal obtained by adsorbing and concentrating a polar health function ingredient such as ⁇ -oryzanol, tocopherol, polyphenols, etc., a concentrate of the health function ingredient prepared from the koji;
  • a polar health function ingredient such as ⁇ -oryzanol, tocopherol, polyphenols, etc.
  • a material for polar health function ingredient-containing foods, medicines, quasi-drugs, cosmetics, animal feeds, or aquatic feeds composed of a dried defatted cereal meal or a concentrate of health function ingredients; It relates to the manufacturing method.
  • rice bran which is a raw material for vegetable oils such as rice oil
  • useful health functional ingredients such as ⁇ -oryzanol, tocopherol, and polyphenol.
  • ⁇ -oryzanol growth promoting action, gonadal stimulating action, vitamin E-like action, anti-stress action, decholesterol action, anti-hyperlipidemia and other pharmacological actions, antioxidant action, ultraviolet absorption action, tyrosinase activity suppression
  • Physiologically active actions such as action and skin temperature raising action are known.
  • lipid metabolism improving effect for tocopherol, lipid metabolism improving effect, membrane stabilizing effect, endocrine stimulating effect, sexual function improving effect, immune enhancing effect, wound repair effect, radiation damage protective effect, anti-aging effect, etc. are related to polyphenols such as catechins Is known to have physiological activities such as antibacterial activity, antioxidant activity, anti-cariogenic activity, antiviral activity, antiallergic activity, ⁇ -amylase inhibitory activity, blood pressure increase inhibitory effect, blood cholesterol lowering effect and the like.
  • Physiologically active substances such as ⁇ oryzanol are abundantly contained in rice bran and the like. However, in the conventional methods for producing rice oil and the like, these physiologically active substances are left in the cooking oil and purified. It was difficult to use these physiologically active substances when using edible oil. That is, conventionally, as a method for refining rice oil or the like, an alkali refining method and a distillation deoxidation method are known. In the alkali refining method, oil collection; degumming; dewaxing; alkaline deoxidation; decolorization; deodorization.
  • Japanese Patent Laid-Open No. 6-340889 discloses a method for producing rice oil in which oryzanols are concentrated by removing fatty acids contained therein by steam distillation under vacuum when refining rice bran crude oil.
  • Japanese Patent Laid-Open No. 2000-119682 discloses that when extracting oil from rice bran, the rice bran is previously treated with an enzyme such as amylase, cellulase, hemicellulase, protease, and extracted with a hydrocarbon-based organic solvent.
  • JP-A-2002-238455 discloses a method for producing a bioactive rice bran oil containing 1.8% by weight oryzanol or sterol by extracting a crude oil from a rice bran raw material, and degumming and dewaxing the crude oil.
  • the crude oil is distilled in a vacuum state at a distillation temperature of 210 to 250 ° C., and further subjected to alkali treatment for deoxidation, or crude oil degumming
  • the crude oil is deodorized by distillation at 250 ° C. or less under reduced pressure, and ⁇ -Oryzanol and Tokov Nord, a method for producing a rice oil containing sterols and the like are disclosed.
  • JP 2002-293793 A and JP 2004-300034 A disclose that a saponified soap stock which has been saponified by adding an alkali such as sodium hydroxide to rice bran oil soap stock and dehydrated with ethyl acetate and acetone.
  • Japanese Patent Application Laid-Open No. 2007-124917 discloses a rice oil produced from rice bran for a method for obtaining an oryzanol-enriched fraction by extraction with such an organic solvent, and further obtaining an oryzanol-enriched fraction by column chromatography. Is used to produce rice oil containing a high concentration of oryzanol by alkaline extraction or treatment with an enzyme such as lipase.
  • cereal meal such as rice bran
  • cereal meal such as rice bran
  • oil plant seeds such as soybeans, rapeseed, cottonseed, rice bran or oily plant residues extracted from fats and oils.
  • Japanese Patent Application Laid-Open No. 9-182562 an animal liquefied fatty substance containing cholesterol is contacted with oil plant seeds such as soybeans, rapeseed, cottonseed, rice bran or oily plant residues extracted from fats and oils.
  • oil plant seeds such as soybeans, rapeseed, cottonseed, rice bran or oily plant residues extracted from fats and oils.
  • 2004-329019 discloses a method of preparing a glycerin-adsorbed feed by mixing glycerin adsorbing carrier such as defatted lees and perlite with glycerin and adsorbing glycerin on the glycerin adsorbing carrier. Yes.
  • cereal meal such as rice bran is used for adsorbing health functional substances such as ⁇ -oryzanol and used for purification and concentration of the component.
  • An object of the present invention is to easily use a health function component having a polarity from a raw material containing the component in order to effectively use a polar health function component composed of ⁇ oryzanol, tocopherol, polyphenols and the like.
  • a polar health function component composed of ⁇ oryzanol, tocopherol, polyphenols and the like.
  • the materials containing the health functional ingredients that have been refined and acquired by effective means An object of the present invention is to provide a method for producing a material that can be effectively used, and a material containing a health functional ingredient produced by the method.
  • the present inventor intensively examines a method for purifying, concentrating, and separating the health functional ingredient in order to effectively use the polar health functional ingredient composed of ⁇ -oryzanol, tocopherol, polyphenols and the like contained in rice bran and the like.
  • dry defatted cereal meal such as dry defatted rice bran can specifically adsorb relatively high-polarity health functional ingredients such as ⁇ -oryzanol, tocopherol, polyphenols, etc., and concentrate the health functional ingredients in the cereal meal.
  • Using the properties of the dried defatted cereal meal selectively and effectively the health functional ingredients from raw materials containing polar health functional ingredients such as ⁇ -oryzanol, tocopherol, polyphenols, etc.
  • the present invention was completed.
  • the present invention performs an adsorption treatment on an extract extracted from an organic solvent from a raw material containing polar health functional ingredients such as ⁇ -oryzanol, tocopherol, and polyphenols, using dried defatted cereal meal as an adsorption carrier.
  • it comprises a method for producing a dried defatted cereal meal with adsorbed and concentrated polar health function components such as ⁇ -oryzanol, tocopherol and polyphenol.
  • the extract used as a raw material in the present invention which is extracted with an organic solvent and contains polar health functional components such as ⁇ -oryzanol, tocopherol, and polyphenols, is preferably an extract extracted from rice bran or kombu Can be mentioned.
  • the dried defatted cereal meal used as a carrier for adsorbing and concentrating polar health functional components such as ⁇ -oryzanol, tocopherol, polyphenol, etc. is preferably dried defatted rice bran or dried defatted wheat bran (dried defatted wheat bran).
  • the dried defatted cereal meal is obtained by washing the cereal meal with a low-polar organic solvent and a high-polar organic solvent, and modifying the defatted cereal meal to be an adsorption carrier that adsorbs a highly polar chemical substance.
  • a dried product can be used.
  • examples of the low polarity organic solvent used in such washing treatment include a low polarity organic solvent composed of n-hexane or chloroform
  • examples of the high polarity organic solvent include high polarity composed of acetone, methanol, or ethanol. Mention may be made of organic solvents.
  • the defatted cereal meal that has been modified to be an adsorption carrier that adsorbs a highly polar chemical substance is dried at 50 to 100 ° C. for 12 to 24 hours. Can do.
  • the adsorption / concentration treatment of the health functional component performed using the dried defatted cereal meal as an adsorption carrier is performed using a nonpolar organic solvent.
  • a particularly preferred nonpolar organic solvent in such a case is n-hexane.
  • a polar elution / separation solvent is used from dried defatted cereal meals adsorbed and concentrated with polar health function components such as ⁇ -oryzanol, tocopherol, and polyphenols produced by the method of the present invention.
  • polar health function components such as ⁇ -oryzanol, tocopherol, and polyphenols produced by the method of the present invention.
  • a concentrate in which polar health function components such as ⁇ -oryzanol, tocopherol, and polyphenols are concentrated can be produced.
  • a mixed solvent of n-hexane / ethanol can be mentioned.
  • a process for eluting and separating polar health function components such as ⁇ oryzanol, tocopherol, and polyphenols from a dried defatted cereal meal with adsorbed and concentrated health function components using a separation solvent It is preferable to carry out under alkaline conditions.
  • the dried defatted cereal meal or adsorbed and concentrated polar health function components such as ⁇ -oryzanol, tocopherol, and polyphenols produced by the production method of the present invention, or concentrates of the health function components are used in various applications. Especially, it can be used without restriction as a material for health functional ingredient-containing foods and drinks, pharmaceuticals, quasi drugs, cosmetics, animal feeds, or marine feeds.
  • the present invention is characterized in that [1] an extract extracted with an organic solvent from a raw material containing a health component with polarity is subjected to an adsorption treatment using dried defatted cereal meal as an adsorption carrier.
  • a method for producing dried defatted cereal meal with adsorbed and concentrated polar health function ingredients, and [2] one or more health, wherein the polar health function ingredients are selected from ⁇ -oryzanol, tocopherol, and polyphenols A method for producing a dried defatted cereal meal with adsorbed and concentrated polar functional health ingredients as described in [1] above, which is a functional ingredient, and [3] selected from ⁇ oryzanol, tocopherol, and polyphenols
  • An extract extracted from a raw material containing one or more health functional ingredients with an organic solvent is an extract extracted from rice bran or kombu.
  • [2] A method for producing a dried defatted cereal meal with adsorbed and concentrated polar health functional ingredients as described in [2] above, and [4] a dried defatted cereal meal with dried defatted rice bran or dried defatted wheat bran.
  • a method for producing a dried defatted cereal meal with adsorbed and concentrated polar health function components according to any one of the above [1] to [3], or [5] a dried defatted cereal meal The above-mentioned [1], wherein the cocoon is washed with a low-polar organic solvent and a high-polar organic solvent, and the defatted cereal cocoon modified to be an adsorption carrier that adsorbs a highly polar chemical substance is dried.
  • the present invention also provides [6] dried defatted cereal meal, wherein the cereal meal is washed with a low polarity organic solvent composed of n-hexane or chloroform and a high polarity organic solvent composed of acetone, methanol, or ethanol,
  • the method for producing a dried defatted cereal meal with adsorbed and concentrated polar health function components according to the above [5], wherein the defatted cereal meal modified to be an adsorbing carrier is dried [7]
  • the dried defatted cereal meal is a product obtained by drying the defatted cereal meal at 50 to 100 ° C.
  • the present invention provides [11] a polar health function component from a defatted cereal meal with adsorbed and concentrated polar health function component according to any one of [1] to [10] above.
  • a method for producing a concentrate of a polar health functional ingredient characterized by elution and separation using a separation solvent, and [12] a polar health functional ingredient selected from ⁇ -oryzanol, tocopherol, and polyphenols [11] The method for producing a polar health functional ingredient concentrate as described in [11] above, wherein [11] is a polar elution / separation solvent, A method for producing a polar health function ingredient concentrate according to [11] or [12], wherein an ethanol mixed solvent is used, and [14] a polar health function ingredient is adsorbed and concentrated.
  • any one of [11] to [13] above, wherein the treatment for eluting / separating a polar health functional ingredient from the dried defatted cereal meal using an elution / separation solvent is performed under alkaline conditions.
  • the polar health function component produced by the method for producing a polar health function component concentrate and [15] the method for producing a dried defatted cereal meal according to any one of [1] to [10] above is adsorbed.
  • a health functional ingredient-containing food or drink comprising a concentrated dried defatted cereal meal or a polar health functional ingredient concentrate produced by the method for producing a concentrate according to any one of [11] to [14] above It consists of materials for pharmaceuticals, pharmaceuticals, quasi-drugs, cosmetics, animal feeds, or marine feeds.
  • FIG. 3 is a photograph showing the results of separation of ⁇ -oryzanol using a mixed solvent of n-hexane and ethanol in an adsorption / separation elution test of health functional ingredients using dry defatted rice bran in an example of the present invention. It is a photograph showing the separation result of ⁇ -oryzanol by n-hexane / ethanol mixed solvent (100: 1, v / v) in the adsorption / separation elution test of health functional ingredients using dry defatted rice bran in the examples of the present invention. .
  • In the Example of this invention it is a figure which shows the condition of the elution and isolation
  • the present invention by subjecting an extract extracted from an organic solvent from a raw material containing polar health functional ingredients such as ⁇ -oryzanol, tocopherol, and polyphenols, by adsorption treatment using dried defatted cereal meal as an adsorption carrier, It consists of a method for producing a dried defatted cereal meal with adsorbed and concentrated polar health function components such as ⁇ oryzanol, tocopherol, and polyphenols.
  • an extract extracted from the plant material with an organic solvent is used as a raw material.
  • the organic solvent used for extracting the extract containing the health functional ingredient from plant materials include lower alcohols such as methanol, ethanol and propanol, ethers such as acetone, ethyl acetate and diethyl ether, and n-hexane.
  • n-hexane is particularly preferred in view of subsequent adsorption / concentration treatment with dried defatted cereal meal.
  • the defatted cereal meal used as a carrier for adsorbing and concentrating health functional ingredients includes defatted rice bran, wheat straw (wheat bran), onion, barley meal, rye meal, buckwheat meal, high meal, and pigeon meal.
  • defatted cereal meals include defatted rice meal and defatted wheat meal (wheat bran).
  • the dry defatted cereal meal used in the present invention was obtained by washing the cereal meal with a low-polar organic solvent and a high-polar organic solvent and drying the defatted cereal meal modified so as to be an adsorption carrier that adsorbs a highly polar chemical. It is preferable.
  • the treatment is performed by washing the cereal meal with a low polarity organic solvent composed of hexane or chloroform and a high polarity organic solvent composed of acetone, methanol or ethanol.
  • the dry defatted cereal meal is prepared by drying the defatted cereal meal at 50-100 ° C. for 12-24 hours.
  • the adsorption treatment in which dried defatted cereal meal is used as an adsorption carrier is performed using a nonpolar organic solvent in which health function components are dissolved.
  • the nonpolar organic solvent is particularly preferably n-hexane from the viewpoint of non-adsorption on the carrier.
  • adsorbing and concentrating the health functional component using the dried defatted cereal meal can be performed by immersing the dried defatted cereal meal in a solvent in which the health functional ingredient is dissolved. It is carried out by passing a solvent in which the health function component is dissolved using a column packed with a cereal bran adsorption carrier.
  • the dried defatted cereal meal obtained by adsorbing and concentrating the health functional ingredient can be used for various applications as a health functional ingredient-containing material.
  • a health functional ingredient concentrate can be produced.
  • the elution / separation solvent for the health function component a polar elution / separation solvent is used, and as the elution / separation solvent, an n-hexane / ethanol mixed solvent is used as a particularly preferred elution / separation solvent.
  • the dried defatted cereal meal or concentrate obtained by adsorbing and concentrating the health function component in the present invention is used as a health function component-containing material, such as for foods and drinks or pharmaceutical foods with a health function, such as tablets, paints, and drinks. It is used for various uses such as pharmaceuticals, quasi-drugs, cosmetics such as emulsions, creams and lotions, animal feeds such as livestock and pets, and marine feeds for marine animals.
  • defatted rice bran can be used as a ⁇ -oryzanol-enhanced carrier.
  • the amount of adsorption increased compared to the case where the adsorption test was performed with ⁇ oryzanol alone, because the amount of ⁇ oryzanol dissolved in n-hexane increased due to the presence of other components such as triglyceride in rice bran oil. Expected to have increased.
  • the present invention is a material obtained by adsorbing and concentrating the health function components from raw materials containing the components, or the health function Provides a simple and inexpensive method that can be applied practically and with effective means to obtain a concentrate of the health function component that has been eluted and separated from the material that has adsorbed and concentrated the component. To do.
  • the material obtained by adsorbing and concentrating the health function ingredient produced in the present invention, and the concentrate of the health function ingredient eluted and separated from the material are made from dry defatted cereal meal as a carrier.
  • it has properties that are highly adaptable to various uses, and is used to manufacture products with health functions in a wide range of applications such as food and drink, pharmaceuticals, cosmetics, quasi-drugs, animal feed, and marine feed. Provide materials that can be used effectively.

Abstract

La présente invention concerne un procédé par lequel un ingrédient diététique polaire, tel que le γ-oryzanol, le tocophérol ou les polyphénols, peut être purifié et obtenu par un procédé en pratique disponible, approprié et efficace. L'invention concerne également un matériau contenant un ingrédient diététique qui est produit par le procédé décrit ci-dessus et peut être utilisé efficacement. Un matériau contenant un ingrédient diététique polaire, tel que le γ-oryzanol, le tocophérol ou les polyphénols, est extrait avec un solvant organique et l'extrait obtenu est soumis à un traitement d'adsorption à l'aide d'un son de céréale sec dégraissé à titre de charge d'adsorption. Ainsi, un son de céréale sec dégraissé comprenant l'ingrédient diététique polaire, tel que le γ-oryzanol, le tocophérol ou les polyphénols, qui y est adsorbé et concentré, est produit. Le son de céréale sec dégraissé, dans lequel l'ingrédient diététique polaire est adsorbé et concentré, ou un concentré de l'ingrédient diététique produit par le procédé décrit ci-dessus est applicable pour de nombreux objectifs, sans aucune restriction d'utilisation en tant que matériau.
PCT/JP2009/001169 2008-03-21 2009-03-17 Son de céréale sec dégraissé contenant un ingrédient diététique adsorbé et concentré, concentré d'ingrédient diététique préparé à partir du son et son procédé de fabrication WO2009116264A1 (fr)

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JP2008-073390 2008-03-21
JP2008073390A JP5463526B2 (ja) 2008-03-21 2008-03-21 健康機能成分を吸着・濃縮した乾燥脱脂穀類糠、該糠から調製した健康機能成分の濃縮物、及びそれらの製造方法

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JP2013158320A (ja) * 2012-02-07 2013-08-19 Nisshin Pet Food Kk ペッドフード
JP2017212906A (ja) * 2016-05-31 2017-12-07 株式会社岡安商店 オリザノール卵
JP2022508666A (ja) * 2019-11-22 2022-01-19 フーナン・ファチェン・バイオテック・インコーポレイテッド オリザノール含有ソープストックを原料としてオリザノールを製造する方法

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WO2011115910A1 (fr) * 2010-03-15 2011-09-22 Rutgers, The State University Of New Jersey Méthodes d'obtention de produits naturels à partir de liquides comestibles et leurs méthodes d'application
JP2015086153A (ja) * 2013-10-29 2015-05-07 株式会社ファンケル Ｖｌｄｌ分泌抑制剤
KR20230149566A (ko) * 2022-04-20 2023-10-27 한국 한의학 연구원 고량강 추출물을 유효성분으로 포함하는 아토피 피부염의 예방, 개선 또는 치료용 조성물

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