WO2009084485A1 - 蒸留酒の製造方法 - Google Patents
蒸留酒の製造方法 Download PDFInfo
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- WO2009084485A1 WO2009084485A1 PCT/JP2008/073219 JP2008073219W WO2009084485A1 WO 2009084485 A1 WO2009084485 A1 WO 2009084485A1 JP 2008073219 W JP2008073219 W JP 2008073219W WO 2009084485 A1 WO2009084485 A1 WO 2009084485A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- lactic acid
- shochu
- flavor
- acid bacteria
- distilled liquor
- Prior art date
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Classifications
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12H—PASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
- C12H6/00—Methods for increasing the alcohol content of fermented solutions or alcoholic beverages
- C12H6/02—Methods for increasing the alcohol content of fermented solutions or alcoholic beverages by distillation
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12G—WINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
- C12G3/00—Preparation of other alcoholic beverages
- C12G3/04—Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs
- C12G3/06—Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs with flavouring ingredients
Definitions
- the present invention relates to a method for producing distilled liquor and distilled liquor produced by the method.
- Lactic acid bacteria are abundant in traditional fermented foods and have been used for a long time in the food culture of each country. Among sake brewing, its effects are well known in Japan for the production of sake. Also, overseas, bourbon whiskey is known as a sour mash that is acidified by lactic acid bacteria during the production of wort raw materials, and in wine, malolactic fermentation by lactic acid bacteria during the post-fermentation period after alcohol production is complete, It is known that it contributes to acidity reduction and flavor enhancement. In Belgium, beer with a complex taste with a sour taste is also made by fermentation with wild yeast and lactic acid bacteria.
- Non-Patent Document 1 describes that lactic acid bacteria belonging to Lactobacillus pentosus and Lactobacillus plantarum have characteristics that allow them to grow in shochu moromi and can become rot-causing lactic acid bacteria. For this reason, in the production of shochu, the addition of lactic acid bacteria in the production process has not been sufficiently studied so far.
- Patent Document 1 Japanese Patent Application Laid-Open No. 2000-60531 refers to a method of utilizing lactic acid bacteria for enhancing shochu flavor.
- the lactic acid bacteria used in the Examples of Patent Document 1 are divided into two strains, Lactobacillus plantarum ATCC21028 (Examples 1 and 2) and Lactobacillus plantarum IFO12011 (Example 3). Not too much. The effects of using these two strains of lactic acid bacteria are evaluated only by a sensory test, and no quantitative evaluation such as analytical values of flavor components is shown.
- Non-patent Document 2 diethyl succinate which is a flavor component is quantified. It is described that diethyl succinate can be detected when malolactic fermentation occurs in fermentation moromi before distillation. However, since the amount of diethyl succinate detected is very small, it has not been reported how it affects quality. JP 2000-60531 A Momose et al., J. Brew. Soc. Japan., 92 (6), 452-457 (1997) Journal of Applied Microbiology, 2002, 92, 1005-1013
- An object is to provide a distilled spirit.
- diethyl succinate is a substance having a sweet scent, which itself has an influence on the flavor, and the taste and scent of distilled liquor not only depends on the amount of each component but also the overall quality of the liquor. Also thought it would change significantly. Based on this idea, the inventor not only increased the scent simply by increasing the diethyl succinate component, but also that the flavor of distilled liquor was enhanced overall by the production of other flavor components. I found it.
- diethyl succinate which is a flavor component of distilled liquor
- diethyl succinate which is a flavor component of distilled liquor
- the flavor enhancement of distilled liquor can be quantitatively evaluated.
- the casei group Lactobacillus casei , Lactobacillus paracasei , Lactobacillus rhamnosus
- Lactobacillus casei Lactobacillus paracasei
- the present invention has the following contents. 1.
- a method for producing distilled liquor comprising adding a lactic acid bacterium belonging to the Lactobacillus casei group to a raw material for distilled liquor. 2.
- the method according to 1 above wherein the lactic acid bacterium is added at the same time as or before or after the preparation of yeast in a distilled liquor material. 3.
- the method according to 1 or 2 above wherein the distilled liquor raw material is a shochu raw material. 4).
- a method for enhancing the flavor of distilled liquor comprising adding lactic acid bacteria belonging to the Lactobacillus casei group to the raw material of distilled liquor. 7).
- a method for enhancing the flavor of shochu comprising adding lactic acid bacteria belonging to the Lactobacillus casei group to the shochu raw material.
- the present invention adds a lactic acid bacterium belonging to the Lactobacillus casei group to a distilled liquor raw material prior to the distillation step to perform a lactic acid fermentation, thereby producing a distilled liquor having an excellent flavor without causing rot of moromi. Succeeded in getting.
- the distilled liquor in the present invention includes shochu, whiskey, vodka, gin, brandy, rum and the like.
- the method of the present invention is particularly effective for producing shochu and whiskey, but is not limited thereto, and can be widely applied to the above-mentioned spirits.
- Lactic acid bacteria that can be used in the present invention are lactic acid bacteria belonging to the Lactobacillus casei group.
- the Lactobacillus casei group is a general term for Lactobacillus casei and its very closely related Lactobacillus paracasei and Lactobacillus rhamnosus lactic acid bacteria.
- the lactic acid bacteria used in the present invention can grow in distilled liquor raw materials, for example, shochu raw materials, particularly in moromi, for example, have resistance to acidic conditions of pH 3.5 or lower, and have an ethanol concentration above a certain level. For example, lactic acid bacteria showing sensitivity to 15% by weight or more of ethanol are preferable.
- the lactic acid bacteria of the present invention can secure a desired number of bacteria even in moromi, so that a desired flavor can be imparted to shochu.
- the growth of lactic acid bacteria is suppressed by ethanol at a certain concentration or higher, excessive growth of lactic acid bacteria can be prevented in the shochu raw material, particularly in moromi, and the production of shochu off-flavor can be suppressed.
- the shochu off-flavor substance refers to a substance that imparts a strange odor, altered odor, bad odor, etc. to the shochu, and examples thereof include diacetyl, acetaldehyde, and acetic acid.
- the distilled liquor raw material is a generic term for raw materials of distilled liquor in the process prior to the distillation process, such as a carbon source, a saccharide obtained by saccharifying the carbon source, moromi obtained by alcohol fermentation of the saccharide.
- a carbon source such as a carbon source, a saccharide obtained by saccharifying the carbon source, moromi obtained by alcohol fermentation of the saccharide.
- any sugar and starch may be used as the carbon source and sugar, but preferably grains such as rice, wheat, whey, corn, corn, millet, acne, and potatoes.
- Starchy materials such as buckwheat, or those obtained by pulverizing and steaming these.
- As a method for saccharifying the carbon source in the raw material that is, starch, addition of koji mold or enzyme agent is used, but koji using koji mold is preferably used.
- koji mold koji molds belonging to the genus Aspergillus , Rhizopus, etc. are used.
- the saccharifying enzyme an enzyme produced by Aspergillus or an enzyme agent such as ⁇ -amylase or glucoamylase is used.
- saccharification may be performed under any conventional conditions as long as the carbon source can be converted into a saccharide by koji mold, saccharifying enzyme, or the like. For example, when gonococcus is added to cause saccharification, gonococcus is usually seeded at 30-45 ° C. for 35-60 hours after seeding the gonococcus.
- the lactic acid bacterium is added before the distillation step, and preferably the lactic acid bacterium is added at any time if the ethanol concentration in the shochu raw material is lower than a certain concentration, for example, lower than 15% by weight. Although it may be added to the distilled liquor raw material, it is preferably added at the same time as or before or after the yeast is charged into the distilled liquor raw material.
- shochu making water and yeast are added to a carbon source or a sugar added with an enzyme agent or koji, and moromi is prepared by alcohol fermentation.
- sugar preparation obtained by saccharifying the carbon source for example, yeast is added to the koji, and the remaining carbon source is added as the fermentation progresses. Is called.
- the stage charging is based on parallel dual fermentation in which saccharification of the carbon source and alcohol fermentation proceed simultaneously.
- yeast for example, association shochu yeast, association sake yeast, awamori yeast, etc., any yeast used for shochu production can be used.
- Alcohol fermentation is usually carried out at 20 to 35 ° C. for 7 to 22 days after yeast is charged. After alcoholic fermentation is complete, the obtained moromi is concentrated directly or by pressure filtration, centrifugation to separate the fermentation residue, yeast cells, etc., and the resulting liquid is distilled to concentrate the ethanol. In the form of the original sake. The raw liquor is adjusted as it is, or mixed, diluted, added with alcohol, etc., and further filtered, aged, etc. as necessary to obtain a shochu form.
- Example Enhancement of Flavor of Shochu The primary fermentation raw material (750 g dry koji, 1.25 L feed water) was inoculated with dried yeast for shochu (Kyokai No. 3) and fermented at 25 ° C. for 6 days to obtain primary moromi.
- Each of the resulting precipitates containing lactic acid bacteria was added to 600 ml of primary moromi.
- 800 g of steamed barley and 1 L of charged water were added as a secondary raw material (hanging wheat) and fermented at 25 ° C. for 10 days to obtain secondary moromi.
- a secondary moromi produced without adding a precipitate containing lactic acid bacteria was used as a comparison.
- the resulting precipitate containing lactic acid bacteria was inoculated to the primary fermentation raw material (750 g dry koji, 1.25 L feed water) simultaneously with dried yeast for shochu (Association No. 3). Fermentation was performed at 25 ° C. for 6 days to obtain primary moromi. Next, for 600 ml of primary moromi, there are two preparations when 600 g of wheat straw is used as a secondary raw material (whole straw) and when 800 g of steamed wheat and 1 liter of charged water are added (hanging wheat). The method was used to ferment at 25 ° C. for 10 days to obtain secondary moromi.
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- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Bioinformatics & Cheminformatics (AREA)
- General Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Life Sciences & Earth Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Food Science & Technology (AREA)
- Alcoholic Beverages (AREA)
Abstract
Description
1.蒸留酒原料にラクトバチルス・カゼイグループに属する乳酸菌を添加することを特徴とする蒸留酒の製造方法。
2.前記乳酸菌を、蒸留酒原料に酵母を仕込むと同時又は仕込み前後に添加する上記1に記載の方法。
3.前記蒸留酒原料が焼酎原料である上記1又は2に記載の方法。
4.上記1又は2に記載の方法で製造された蒸留酒。
5.上記3に記載の方法で製造された焼酎。
6.蒸留酒原料にラクトバチルス・カゼイグループに属する乳酸菌を添加することを特徴とする蒸留酒の香味増強方法。
7.焼酎原料にラクトバチルス・カゼイグループに属する乳酸菌を添加することを特徴とする焼酎の香味増強方法。
本発明に使用できる乳酸菌は、ラクトバチルス・カゼイグループに属する乳酸菌である。本発明における、ラクトバチルス・カゼイ(Lactobacillus casei)グループとは、ラクトバチルス・カゼイ及びその極めて近縁のラクトバチルス・パラカゼイ(Lactobacillus paracasei)及びラクトバチルス・ラムノサス(Lactobacillus rhamnosus)の乳酸菌を総称する。本発明に用いられる乳酸菌は、蒸留酒原料、例えば、焼酎原料中、特にモロミ中において増殖が可能である、例えば、pH3.5以下の酸性条件に耐性を有し、かつ、一定以上のエタノール濃度、例えば、15重量%以上のエタノールに感受性を示す乳酸菌が好ましい。このような特性により、本発明の乳酸菌はモロミ中においても所望の菌数が確保できるため、焼酎に所望の香味を付与することができる。また、乳酸菌は、一定以上の濃度のエタノールにより増殖が抑制されるので、焼酎原料中、特にモロミ中において乳酸菌の過剰増殖を防ぐことができ、かつ焼酎オフフレーバーの生成等を抑制することができる。焼酎オフフレーバー物質とは、焼酎に異臭、変質臭、悪変臭等を付与する物質をいい、例えばダイアセチル、アセトアルデヒド、酢酸等があげられる。
(蒸留酒原料)
本発明において、蒸留酒原料とは炭素源、炭素源を糖化して得られる糖質、糖質をアルコール発酵して得られるモロミ等、蒸留工程以前の工程にある蒸留酒の原材料を総称していう。焼酎を例にとれば、炭素源及び糖質としては、いかなる糖質および澱粉質を用いてもよいが、好ましくは米、麦、あわ、トウモロコシ、こうりゃん、ひえ、きび等の穀類、イモ類、そば等の澱粉質、またはこれらを粉砕、蒸煮したものを用いる。原料中の炭素源すなわち澱粉質を糖化する方法としては、麹菌や酵素剤の添加が用いられるが、好ましくは麹菌を用いた麹が用いられる。
(乳酸菌の添加時期及び蒸留酒の製造)
本発明における乳酸菌の添加時期は、蒸留工程以前であり、かつ好ましくは焼酎原料中のエタノール濃度が、一定濃度より低い時期、例えば、15重量%より低い時期であれば、いずれの時期において乳酸菌を蒸留酒原料に添加してもよいが、蒸留酒原料に酵母を仕込むと同時に又はその前後に添加することが好ましい。
[実施例 焼酎の香味増強]
一次発酵原料(750g乾燥麹、1.25L仕込み水)に焼酎用乾燥酵母(協会3号)を接種し、25℃で6日間発酵させ、一次モロミを得た。
10mlのMRS液体培地でL. plantarum JCM1149株を前培養した。OD660=5の培養液6mlを遠心分離(3,000rpm、10分)し、上澄み液を捨て、乳酸菌を含む沈殿を得た。
Claims (7)
- 蒸留酒原料にラクトバチルス・カゼイグループに属する乳酸菌を添加することを特徴とする蒸留酒の製造方法。
- 前記乳酸菌を、蒸留酒原料に酵母を仕込むと同時又は仕込み前後に添加する請求項1に記載の方法。
- 前記蒸留酒原料が焼酎原料である請求項1又は2に記載の方法。
- 請求項1又は2に記載の方法で製造された蒸留酒。
- 請求項3に記載の方法で製造された焼酎。
- 蒸留酒原料にラクトバチルス・カゼイグループに属する乳酸菌を添加することを特徴とする蒸留酒の香味増強方法。
- 焼酎原料にラクトバチルス・カゼイグループに属する乳酸菌を添加することを特徴とする焼酎の香味増強方法。
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JP2007338815A JP2009153506A (ja) | 2007-12-28 | 2007-12-28 | 蒸留酒の製造方法 |
JP2007-338815 | 2007-12-28 |
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JP (1) | JP2009153506A (ja) |
KR (1) | KR20100106320A (ja) |
CN (1) | CN101889073A (ja) |
TW (1) | TW200951216A (ja) |
WO (1) | WO2009084485A1 (ja) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN111235002A (zh) * | 2020-01-19 | 2020-06-05 | 江南大学 | 一种黑枣果醋及其制备方法 |
Families Citing this family (10)
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JP2012055236A (ja) | 2010-09-09 | 2012-03-22 | Suntory Holdings Ltd | 焼酎の製造方法 |
JP5754903B2 (ja) * | 2010-09-09 | 2015-07-29 | サントリーホールディングス株式会社 | 新規焼酎の製造方法 |
CN103562372A (zh) * | 2011-06-03 | 2014-02-05 | 三得利控股株式会社 | 混合蒸馏酒及其制造方法 |
CN102994318B (zh) * | 2012-12-30 | 2013-12-18 | 杜林� | 一种应用乳酸菌发酵生产黄酒的方法 |
CN104593189A (zh) * | 2014-12-02 | 2015-05-06 | 天津科技大学 | 新型固态发酵生产浓香型白酒的方法 |
CN104450399B (zh) * | 2014-12-05 | 2016-06-15 | 天津科技大学 | 一种液态发酵生产米香型白酒的方法 |
CN108179085B (zh) * | 2018-02-27 | 2021-07-20 | 会稽山绍兴酒股份有限公司 | 一种加快黄酒产陈酒香陈酒味的方法 |
CN108441377A (zh) * | 2018-05-21 | 2018-08-24 | 安徽省领航动物保健品有限责任公司 | 一种发酵型领航三肽酒的制作方法 |
CN114672383B (zh) * | 2022-04-15 | 2024-07-16 | 海天醋业(广东)有限公司 | 黄酒及其陈酿方法 |
KR20240126651A (ko) | 2023-02-14 | 2024-08-21 | 김주영 | 술지게미와 유산균을 활용한 증류주 제조 방법 |
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JPH01257460A (ja) * | 1987-12-28 | 1989-10-13 | Calpis Food Ind Co Ltd:The | 豊醇風味の乳酒の製造方法 |
JP2000060531A (ja) * | 1998-08-12 | 2000-02-29 | Kyowa Hakko Kogyo Co Ltd | 焼酎の製造方法 |
JP2003169659A (ja) * | 2001-09-26 | 2003-06-17 | Takara Holdings Inc | アルコール含有飲料及びその製造方法 |
-
2007
- 2007-12-28 JP JP2007338815A patent/JP2009153506A/ja active Pending
-
2008
- 2008-12-19 CN CN200880119797XA patent/CN101889073A/zh active Pending
- 2008-12-19 KR KR1020107011623A patent/KR20100106320A/ko not_active Application Discontinuation
- 2008-12-19 WO PCT/JP2008/073219 patent/WO2009084485A1/ja active Application Filing
- 2008-12-23 TW TW097150261A patent/TW200951216A/zh unknown
Patent Citations (3)
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JPH01257460A (ja) * | 1987-12-28 | 1989-10-13 | Calpis Food Ind Co Ltd:The | 豊醇風味の乳酒の製造方法 |
JP2000060531A (ja) * | 1998-08-12 | 2000-02-29 | Kyowa Hakko Kogyo Co Ltd | 焼酎の製造方法 |
JP2003169659A (ja) * | 2001-09-26 | 2003-06-17 | Takara Holdings Inc | アルコール含有飲料及びその製造方法 |
Non-Patent Citations (1)
Title |
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TANABE K. ET AL.: "Kansho Shochu Jozo ni Okeru Shubo, Moromi Chu no Nyusankin ni Tsuite", KADAI NOGAKUJUTSU HOKOKU, 1982, pages 69 - 77 * |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111235002A (zh) * | 2020-01-19 | 2020-06-05 | 江南大学 | 一种黑枣果醋及其制备方法 |
CN111235002B (zh) * | 2020-01-19 | 2022-11-11 | 江南大学 | 一种黑枣果醋及其制备方法 |
Also Published As
Publication number | Publication date |
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CN101889073A (zh) | 2010-11-17 |
TW200951216A (en) | 2009-12-16 |
JP2009153506A (ja) | 2009-07-16 |
KR20100106320A (ko) | 2010-10-01 |
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