WO2009072648A1 - 亜鉛又は亜鉛合金めっきに耐食性皮膜を形成させるための表面処理水溶液及び処理方法 - Google Patents

亜鉛又は亜鉛合金めっきに耐食性皮膜を形成させるための表面処理水溶液及び処理方法 Download PDF

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Publication number
WO2009072648A1
WO2009072648A1 PCT/JP2008/072257 JP2008072257W WO2009072648A1 WO 2009072648 A1 WO2009072648 A1 WO 2009072648A1 JP 2008072257 W JP2008072257 W JP 2008072257W WO 2009072648 A1 WO2009072648 A1 WO 2009072648A1
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WIPO (PCT)
Prior art keywords
zinc
coating film
alloy deposit
zinc alloy
aqueous solution
Prior art date
Application number
PCT/JP2008/072257
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English (en)
French (fr)
Inventor
Hitoshi Sakurai
Satoshi Yuasa
Keisuke Nonomura
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Dipsol Chemicals Co., Ltd.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by Dipsol Chemicals Co., Ltd. filed Critical Dipsol Chemicals Co., Ltd.
Priority to CN2008801263492A priority Critical patent/CN101939388B/zh
Priority to EP08857313.4A priority patent/EP2223975B1/en
Priority to US12/746,549 priority patent/US20100297454A1/en
Publication of WO2009072648A1 publication Critical patent/WO2009072648A1/ja
Priority to US14/591,049 priority patent/US20150125708A1/en

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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D1/00—Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances
    • C09D1/02—Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances alkali metal silicates
    • C09D1/04—Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances alkali metal silicates with organic additives
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
    • C04B28/24—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing alkyl, ammonium or metal silicates; containing silica sols
    • C04B28/26—Silicates of the alkali metals
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D163/00—Coating compositions based on epoxy resins; Coating compositions based on derivatives of epoxy resins
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/08—Anti-corrosive paints
    • C09D5/082—Anti-corrosive paints characterised by the anti-corrosive pigment
    • C09D5/084—Inorganic compounds
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
    • C23C22/60—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using alkaline aqueous solutions with pH greater than 8
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C22/05—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions
    • C23C22/68—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using aqueous solutions using aqueous solutions with pH between 6 and 8
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2103/00—Function or property of ingredients for mortars, concrete or artificial stone
    • C04B2103/0045—Polymers chosen for their physico-chemical characteristics
    • C04B2103/0046—Polymers chosen for their physico-chemical characteristics added as monomers or as oligomers
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/00474—Uses not provided for elsewhere in C04B2111/00
    • C04B2111/00482—Coating or impregnation materials
    • C04B2111/00525—Coating or impregnation materials for metallic surfaces
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2150/00—Compositions for coatings
    • C08G2150/90—Compositions for anticorrosive coatings
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C2222/00—Aspects relating to chemical surface treatment of metallic material by reaction of the surface with a reactive medium
    • C23C2222/20—Use of solutions containing silanes
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/31504—Composite [nonstructural laminate]
    • Y10T428/31652—Of asbestos
    • Y10T428/31663—As siloxane, silicone or silane

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Inorganic Chemistry (AREA)
  • Metallurgy (AREA)
  • Mechanical Engineering (AREA)
  • General Chemical & Material Sciences (AREA)
  • Ceramic Engineering (AREA)
  • Structural Engineering (AREA)
  • Chemical Treatment Of Metals (AREA)
  • Other Surface Treatments For Metallic Materials (AREA)
  • Paints Or Removers (AREA)
  • Application Of Or Painting With Fluid Materials (AREA)

Abstract

　本発明は、亜鉛又は亜鉛合金めっきに高耐食性の、垂れ染み・溜まり染みのない均一外観で、厚みの不均一不良を生じない、密着性の良好な皮膜を付与するためのクロムフリーの処理液及び処理方法を提供することを目的とする。本発明は、（ａ）アルカリ金属シリケート（Ｍ2Ｏ・ｎＳｉＯ2（式中、Ｍはアルカリ金属を示し、ｎはＳｉＯ2／Ｍ2Ｏモル比を示す））、（ｂ）水溶性又は水分散性シランカップリング剤及び（ｃ）水溶性又は水分散性グリシジルエーテル化合物を含有することを特徴とする亜鉛又は亜鉛合金めっき上に耐食性皮膜を形成させるための表面処理水溶液を提供する。また、本発明は、亜鉛又は亜鉛合金めっき表面を、前記表面処理水溶液に接触させることを含む、亜鉛又は亜鉛合金めっき上に高耐食性皮膜を形成させる表面処理方法を提供する。さらに、本発明の前記表面処理水溶液は、亜鉛又は亜鉛合金めっき上に形成された６価クロムフリー又は完全クロムフリーの化成処理皮膜表面に対しても施すことができる。すなわち、本発明は、亜鉛又は亜鉛合金めっき上に形成された化成処理皮膜表面を、前記表面処理水溶液に接触させることを含む、亜鉛又は亜鉛合金めっき上に高耐食性皮膜を形成させる表面処理方法をも提供する。また、本発明は、亜鉛又は亜鉛合金めっき表面、又は亜鉛または亜鉛合金めっき上に形成された化成処理皮膜表面に前記を接触させることにより形成された高耐食性皮膜を提供する。
PCT/JP2008/072257 2007-12-07 2008-12-08 亜鉛又は亜鉛合金めっきに耐食性皮膜を形成させるための表面処理水溶液及び処理方法 WO2009072648A1 (ja)

Priority Applications (4)

Application Number Priority Date Filing Date Title
CN2008801263492A CN101939388B (zh) 2007-12-07 2008-12-08 用于在锌或锌合金镀层上形成耐腐蚀性覆膜的表面处理水溶液及处理方法
EP08857313.4A EP2223975B1 (en) 2007-12-07 2008-12-08 Surface-treating aqueous solution and treatment methods for forming corrosion-resistant coating film over zinc or zinc alloy deposit
US12/746,549 US20100297454A1 (en) 2007-12-07 2008-12-08 Surface-Treating Aqueous Solution and Treatment Methods for Forming Corrosion-Resistant Coating Film Over Zinc or Zinc Alloy Deposit
US14/591,049 US20150125708A1 (en) 2007-12-07 2015-01-07 Surface-treating aqueous solution and treatment methods for forming corrosion-resistant coating film over zinc or zinc alloy deposit

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2007-317156 2007-12-07
JP2007317156A JP5322000B2 (ja) 2007-12-07 2007-12-07 亜鉛又は亜鉛合金めっきに耐食性皮膜を形成させるための表面処理水溶液及び処理方法

Related Child Applications (2)

Application Number Title Priority Date Filing Date
US12/746,549 A-371-Of-International US20100297454A1 (en) 2007-12-07 2008-12-08 Surface-Treating Aqueous Solution and Treatment Methods for Forming Corrosion-Resistant Coating Film Over Zinc or Zinc Alloy Deposit
US14/591,049 Division US20150125708A1 (en) 2007-12-07 2015-01-07 Surface-treating aqueous solution and treatment methods for forming corrosion-resistant coating film over zinc or zinc alloy deposit

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WO2009072648A1 true WO2009072648A1 (ja) 2009-06-11

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US (2) US20100297454A1 (ja)
EP (1) EP2223975B1 (ja)
JP (1) JP5322000B2 (ja)
KR (1) KR101212335B1 (ja)
CN (1) CN101939388B (ja)
WO (1) WO2009072648A1 (ja)

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US20130295292A1 (en) * 2010-10-27 2013-11-07 Chemetall Gmbh Aqueous composition for pretreating a metal surface before applying another coating or for treating said surface

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CN102912345B (zh) * 2012-10-29 2014-10-22 南京信息工程大学 一种铝合金表面防腐方法
CN102965657A (zh) * 2012-11-22 2013-03-13 象山华鹰塑料工程有限公司 一种用于锌合金表面耐腐蚀膜的表面处理液
CN103045086B (zh) * 2012-12-18 2016-03-02 安徽六方重联机械股份有限公司 一种金属表面硅烷处理剂及其制备方法
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CN103059723A (zh) * 2012-12-18 2013-04-24 安徽六方重联机械股份有限公司 一种耐剥离的金属表面硅烷处理剂及其制备方法
CN103031056B (zh) * 2012-12-18 2016-02-24 安徽六方重联机械股份有限公司 一种含有水性纳米氧化锌料的金属表面硅烷处理剂及其制备方法
JP6090693B2 (ja) * 2012-12-28 2017-03-08 福田金属箔粉工業株式会社 表面処理銅箔及び当該表面処理銅箔を用いたプリント配線板
CN103254764A (zh) * 2013-04-08 2013-08-21 马鞍山拓锐金属表面技术有限公司 一种抗剥离的金属表面硅烷处理剂及其制备方法
CN104059411B (zh) * 2013-05-03 2016-02-24 攀钢集团攀枝花钢铁研究院有限公司 制备镀层保护剂的方法和由该方法制备的镀层保护剂及其用途以及热镀金属材料
CN104059409B (zh) * 2013-05-03 2016-02-17 攀钢集团攀枝花钢铁研究院有限公司 一种表面转化层形成剂及其制备方法和用途以及热镀金属材料
EP3040385A4 (en) 2013-08-28 2017-03-29 Dipsol Chemicals Co., Ltd. Friction modifier for top coating agent for trivalent chromium chemical conversion coating film or chromium-free chemical conversion coating film, and top coating agent including same
CN103468127B (zh) * 2013-09-12 2016-03-02 昆山瑞仕莱斯高新材料科技有限公司 用于表面处理的水性封闭剂及其制作方法
CN104099007B (zh) * 2014-06-19 2016-07-06 锐展(铜陵)科技有限公司 一种多镁基铝合金表面处理剂
KR101728027B1 (ko) * 2015-12-24 2017-04-18 주식회사 포스코 전기강판 접착 코팅 조성물, 접착 코팅층이 형성된 전기강판, 전기강판 제품, 및 이의 제조 방법
JP6757220B2 (ja) * 2016-09-27 2020-09-16 日本パーカライジング株式会社 金属材料用表面処理剤及びその製造方法、並びに、表面処理被膜付き金属材料及びその製造方法
WO2023140062A1 (ja) * 2022-01-21 2023-07-27 ナミックス株式会社 金属部材

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EP2223975A4 (en) 2011-03-02
CN101939388B (zh) 2013-03-13
CN101939388A (zh) 2011-01-05
KR101212335B1 (ko) 2012-12-13
US20100297454A1 (en) 2010-11-25
JP2009138132A (ja) 2009-06-25
JP5322000B2 (ja) 2013-10-23
US20150125708A1 (en) 2015-05-07
EP2223975A1 (en) 2010-09-01
KR20100087208A (ko) 2010-08-03

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