WO2009072505A1 - 有機アルカリ金属化合物および有機遷移金属化合物の製造方法 - Google Patents

有機アルカリ金属化合物および有機遷移金属化合物の製造方法 Download PDF

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Publication number
WO2009072505A1
WO2009072505A1 PCT/JP2008/071908 JP2008071908W WO2009072505A1 WO 2009072505 A1 WO2009072505 A1 WO 2009072505A1 JP 2008071908 W JP2008071908 W JP 2008071908W WO 2009072505 A1 WO2009072505 A1 WO 2009072505A1
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WO
WIPO (PCT)
Prior art keywords
metal compound
alkali metal
atom
producing organic
general formula
Prior art date
Application number
PCT/JP2008/071908
Other languages
English (en)
French (fr)
Inventor
Atsushi Sakuma
Munehito Funaya
Original Assignee
Mitsui Chemicals, Inc.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mitsui Chemicals, Inc. filed Critical Mitsui Chemicals, Inc.
Priority to US12/745,868 priority Critical patent/US8409480B2/en
Priority to EP08856231.9A priority patent/EP2226326B1/en
Priority to JP2009544683A priority patent/JP5237966B2/ja
Priority to CA2707511A priority patent/CA2707511C/en
Priority to CN200880117423.4A priority patent/CN101874033B/zh
Publication of WO2009072505A1 publication Critical patent/WO2009072505A1/ja

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F1/00—Compounds containing elements of Groups 1 or 11 of the Periodic System
    • C07F1/02—Lithium compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F17/00—Metallocenes

Abstract

[課題]　高収率で有機アルカリ金属化合物が得られる製造方法、およびその化合物を用いた有機遷移金属化合物の製造方法を提供すること。 [解決手段]　下記一般式（１）で表される活性プロトン含有化合物と、アルカリ金属化合物との反応において、下記一般式（２）で表される化合物を添加することを特徴とする、有機アルカリ金属化合物の製造方法。 　ＲＨp　・・・（１） 〔一般式（１）中、Ｒは、炭化水素基またはアミノ基を示し、ハロゲン原子、ケイ素原子、酸素原子または窒素原子を含有してもよく、Ｈは活性プロトンを示し、ｐはアルカリ金属化合物との反応において引き抜かれる水素原子の数である。〕 〔一般式（２）中、Ｒa～Ｒcは、水素原子、炭化水素基、ヘテロ原子含有基、ケイ素含有基から選ばれる原子または基を示し、互いに同一でも異なっていてもよく、隣接した置換基は互いに結合して環を形成してもよい。〕
PCT/JP2008/071908 2007-12-04 2008-12-02 有機アルカリ金属化合物および有機遷移金属化合物の製造方法 WO2009072505A1 (ja)

Priority Applications (5)

Application Number Priority Date Filing Date Title
US12/745,868 US8409480B2 (en) 2007-12-04 2008-12-02 Process for preparing organic alkali metal compound and organic transition metal compound
EP08856231.9A EP2226326B1 (en) 2007-12-04 2008-12-02 Method for producing organic alkali metal compound and method for producing organic transition metal compound
JP2009544683A JP5237966B2 (ja) 2007-12-04 2008-12-02 有機アルカリ金属化合物および有機遷移金属化合物の製造方法
CA2707511A CA2707511C (en) 2007-12-04 2008-12-02 Processes for preparing organic alkali metal compound and organic transition metal compound
CN200880117423.4A CN101874033B (zh) 2007-12-04 2008-12-02 有机碱金属化合物和有机过渡金属化合物的制造方法

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2007313007 2007-12-04
JP2007-313007 2007-12-04

Publications (1)

Publication Number Publication Date
WO2009072505A1 true WO2009072505A1 (ja) 2009-06-11

Family

ID=40717683

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/JP2008/071908 WO2009072505A1 (ja) 2007-12-04 2008-12-02 有機アルカリ金属化合物および有機遷移金属化合物の製造方法

Country Status (9)

Country Link
US (1) US8409480B2 (ja)
EP (1) EP2226326B1 (ja)
JP (1) JP5237966B2 (ja)
KR (1) KR101269789B1 (ja)
CN (1) CN101874033B (ja)
CA (1) CA2707511C (ja)
RU (1) RU2445316C1 (ja)
TW (1) TWI435878B (ja)
WO (1) WO2009072505A1 (ja)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2014050816A1 (ja) 2012-09-25 2014-04-03 三井化学株式会社 遷移金属化合物、オレフィン重合用触媒およびオレフィン重合体の製造方法
WO2014050817A1 (ja) 2012-09-25 2014-04-03 三井化学株式会社 オレフィン重合体の製造方法およびオレフィン重合体
WO2014087924A1 (ja) * 2012-12-07 2014-06-12 株式会社クラレ 多官能性アニオン重合開始剤およびその製造方法

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4006187A (en) * 1971-10-06 1977-02-01 Lithium Corporation Of America Preparation of aryllithium compounds by metalation
EP0661300A1 (de) * 1993-12-21 1995-07-05 Hoechst Aktiengesellschaft Verfahren zur Herstellung von Polyolefinen
JPH08208733A (ja) 1995-01-31 1996-08-13 Mitsubishi Chem Corp オレフィン重合用触媒
JPH1112290A (ja) 1997-06-24 1999-01-19 Mitsubishi Chem Corp 架橋メタロセンの製造方法
JP2001011087A (ja) 1999-07-02 2001-01-16 Japan Polychem Corp メタロセン生成物混合物からのメタロセン化合物の精製方法
JP3176092B2 (ja) 1991-08-26 2001-06-11 三井化学株式会社 新規遷移金属化合物及びそれを用いたポリオレフィンの製造方法
JP3320619B2 (ja) 1996-10-02 2002-09-03 三井化学株式会社 新規メタロセン化合物とそれを用いたオレフィンまたはジエンの重合方法
JP3713405B2 (ja) 1999-07-02 2005-11-09 三菱化学株式会社 架橋ジルコノセン化合物の製造方法

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US3663585A (en) * 1964-04-13 1972-05-16 Exxon Research Engineering Co Process for lithiating ferrocene
FR2313389A1 (fr) * 1975-06-06 1976-12-31 Anvar Nouveaux amorceurs de polymerisation organolithiens bi-fonctionnels et leurs applications, en particulier pour l'obtention d'elastomeres thermoplastiques
ES2093166T3 (es) * 1991-11-30 1996-12-16 Hoechst Ag Metalocenos con derivados de indenilo condensados con benzo como ligandos, procedimiento para su preparacion y su utilizacion como catalizadores.

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4006187A (en) * 1971-10-06 1977-02-01 Lithium Corporation Of America Preparation of aryllithium compounds by metalation
JP3176092B2 (ja) 1991-08-26 2001-06-11 三井化学株式会社 新規遷移金属化合物及びそれを用いたポリオレフィンの製造方法
EP0661300A1 (de) * 1993-12-21 1995-07-05 Hoechst Aktiengesellschaft Verfahren zur Herstellung von Polyolefinen
JPH08208733A (ja) 1995-01-31 1996-08-13 Mitsubishi Chem Corp オレフィン重合用触媒
JP3320619B2 (ja) 1996-10-02 2002-09-03 三井化学株式会社 新規メタロセン化合物とそれを用いたオレフィンまたはジエンの重合方法
JPH1112290A (ja) 1997-06-24 1999-01-19 Mitsubishi Chem Corp 架橋メタロセンの製造方法
JP2001011087A (ja) 1999-07-02 2001-01-16 Japan Polychem Corp メタロセン生成物混合物からのメタロセン化合物の精製方法
JP3713405B2 (ja) 1999-07-02 2005-11-09 三菱化学株式会社 架橋ジルコノセン化合物の製造方法

Non-Patent Citations (4)

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Title
ORGANOMETALLICS, vol. 26, 2007, pages 417 - 424
PURE & APPL. CHEM., vol. 60, 1988, pages 1627 - 1634
READY, THOMAS E. ET AL.: "Alkyl-substituted indenyl titanium precursors for syndiospecific Ziegler-Natta polymerization of styrene", JOURNAL OF ORGANOMETALLIC CHEMISTRY, vol. 519, no. 1-2, 1996, pages 21 - 28, XP008137358 *
See also references of EP2226326A4 *

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2014050816A1 (ja) 2012-09-25 2014-04-03 三井化学株式会社 遷移金属化合物、オレフィン重合用触媒およびオレフィン重合体の製造方法
WO2014050817A1 (ja) 2012-09-25 2014-04-03 三井化学株式会社 オレフィン重合体の製造方法およびオレフィン重合体
US9458257B2 (en) 2012-09-25 2016-10-04 Mitsui Chemicals, Inc. Process for producing olefin polymer and olefin polymer
US9458261B2 (en) 2012-09-25 2016-10-04 Mitsui Chemicals, Inc. Transition metal compound, olefin polymerization catalyst, and olefin polymer production process
US9796799B2 (en) 2012-09-25 2017-10-24 Mitsui Chemicals, Inc. Transition metal compound, olefin polymerization catalyst, and olefin polymer production process
US9896526B2 (en) 2012-09-25 2018-02-20 Mitsui Chemicals, Inc. Process for producing olefin polymer and olefin polymer
US10336838B2 (en) 2012-09-25 2019-07-02 Mitsui Chemicals, Inc. Process for producing olefin polymer and olefin polymer
US10336837B2 (en) 2012-09-25 2019-07-02 Mitsui Chemicals, Inc. Process for producing olefin polymer and olefin polymer
WO2014087924A1 (ja) * 2012-12-07 2014-06-12 株式会社クラレ 多官能性アニオン重合開始剤およびその製造方法

Also Published As

Publication number Publication date
EP2226326A4 (en) 2012-02-15
US8409480B2 (en) 2013-04-02
TWI435878B (zh) 2014-05-01
EP2226326B1 (en) 2016-02-17
US20120049391A1 (en) 2012-03-01
KR101269789B1 (ko) 2013-05-30
JPWO2009072505A1 (ja) 2011-04-21
RU2010126548A (ru) 2012-01-10
CN101874033A (zh) 2010-10-27
JP5237966B2 (ja) 2013-07-17
KR20100087404A (ko) 2010-08-04
TW200936597A (en) 2009-09-01
EP2226326A1 (en) 2010-09-08
CA2707511A1 (en) 2009-06-11
CA2707511C (en) 2013-04-02
CN101874033B (zh) 2016-05-11
RU2445316C1 (ru) 2012-03-20

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