WO2009060815A1 - トリフルオロメタンスルホニルフルオリドの製造方法 - Google Patents

トリフルオロメタンスルホニルフルオリドの製造方法 Download PDF

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Publication number
WO2009060815A1
WO2009060815A1 PCT/JP2008/070016 JP2008070016W WO2009060815A1 WO 2009060815 A1 WO2009060815 A1 WO 2009060815A1 JP 2008070016 W JP2008070016 W JP 2008070016W WO 2009060815 A1 WO2009060815 A1 WO 2009060815A1
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WO
WIPO (PCT)
Prior art keywords
fluoride
preparation
trifluoromethanesulfonyl
metal fluoride
trifluoromethanesulfonyl fluoride
Prior art date
Application number
PCT/JP2008/070016
Other languages
English (en)
French (fr)
Inventor
Shigenori Sakai
Takayoshi Morinaka
Tsutomu Nanmyo
Takashi Kume
Original Assignee
Central Glass Company, Limited
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Central Glass Company, Limited filed Critical Central Glass Company, Limited
Priority to EP08846952.3A priority Critical patent/EP2216325B1/en
Priority to CN2008801141902A priority patent/CN101842348B/zh
Publication of WO2009060815A1 publication Critical patent/WO2009060815A1/ja

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Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/02Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof
    • C07C303/22Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof from sulfonic acids, by reactions not involving the formation of sulfo or halosulfonyl groups; from sulfonic halides by reactions not involving the formation of halosulfonyl groups

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

トリフルオロメタンスルホニルクロリド(CF3SO2Cl)と金属フッ化物を、水の存在下、反応させることにより、トリフルオロメタンスルホニルフルオリド(CF3SO2F)を製造する方法にあたり、水の量を金属フッ化物100質量%に対し0.6質量%~10.0質量%の範囲で行うことを特徴とする、トリフルオロメタンスルホニルフルオリドの製造方法が開示されている。この製造方法は、従来の製造法に比べ、短工程で、高収率かつ高純度でトリフルオロメタンスルホニルフルオリドを製造できる。
PCT/JP2008/070016 2007-11-06 2008-11-04 トリフルオロメタンスルホニルフルオリドの製造方法 WO2009060815A1 (ja)

Priority Applications (2)

Application Number Priority Date Filing Date Title
EP08846952.3A EP2216325B1 (en) 2007-11-06 2008-11-04 Process for preparation of trifluoromethanesulfonyl fluoride
CN2008801141902A CN101842348B (zh) 2007-11-06 2008-11-04 三氟甲磺酰氟的制造方法

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
JP2007-287969 2007-11-06
JP2007287969 2007-11-06
JP2008-280872 2008-10-31
JP2008280872A JP5347431B2 (ja) 2007-11-06 2008-10-31 トリフルオロメタンスルホニルフルオリドの製造方法

Publications (1)

Publication Number Publication Date
WO2009060815A1 true WO2009060815A1 (ja) 2009-05-14

Family

ID=40625706

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/JP2008/070016 WO2009060815A1 (ja) 2007-11-06 2008-11-04 トリフルオロメタンスルホニルフルオリドの製造方法

Country Status (4)

Country Link
EP (1) EP2216325B1 (ja)
JP (1) JP5347431B2 (ja)
CN (1) CN101842348B (ja)
WO (1) WO2009060815A1 (ja)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2014016130A1 (fr) 2012-07-23 2014-01-30 Rhodia Operations Procédé de préparation d'un composé sulfonimide et de ses sels
JP2015057379A (ja) * 2013-08-09 2015-03-26 ダイキン工業株式会社 フッ化メタンの製造方法

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5169880B2 (ja) * 2009-01-29 2013-03-27 セントラル硝子株式会社 トリフルオロメタンスルホニルフルオリドの精製方法
CN105198683B (zh) * 2015-09-24 2017-03-29 信阳师范学院 一种磺酰氟类化合物的制备方法
CN105669501A (zh) * 2016-02-25 2016-06-15 湖北恒新化工有限公司 一种2-萘磺酰氟的制备方法
CN111183114A (zh) * 2017-10-11 2020-05-19 大金工业株式会社 氟磺酸锂的制造方法
CN109824551A (zh) * 2019-04-04 2019-05-31 武汉大学 一种由三氟甲基磺酰氯制备三氟甲基磺酰氟的方法
CN112724047B (zh) * 2020-12-15 2023-10-17 中船(邯郸)派瑞特种气体股份有限公司 一种制备三氟甲磺酰氟的装置及方法
CN112760672B (zh) * 2020-12-15 2022-04-08 中船(邯郸)派瑞特种气体股份有限公司 一种甲基磺酰氯电化学制备三氟甲基磺酰氟的方法
CN112742337B (zh) * 2020-12-29 2023-06-02 中船(邯郸)派瑞特种气体股份有限公司 一种连续反应制备甲基磺酰氟的装置和方法

Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2732398A (en) 1953-01-29 1956-01-24 cafiicfzsojk
JPS51125322A (en) 1975-03-21 1976-11-01 Bayer Ag Process for manufacturing sulfonic acid fluoride
JPH0672987A (ja) 1992-08-25 1994-03-15 Nippon Bayeragrochem Kk メタンスルホニルフルオライド誘導体の製造方法
JPH06263715A (ja) * 1993-01-18 1994-09-20 Central Glass Co Ltd 高純度メタンスルホニルフロライドの製造法
JP2000264871A (ja) 1999-03-16 2000-09-26 Central Glass Co Ltd トリフルオロメタンスルホニルクロリドの製造方法
JP2003206272A (ja) 2001-12-28 2003-07-22 Kanto Denka Kogyo Co Ltd 含フッ素アルカンスルホニルフルオリドの製造方法
JP3444477B2 (ja) 1998-12-28 2003-09-08 セントラル硝子株式会社 トリフルオロメタンスルホニルクロリドの製造方法
JP3456634B2 (ja) 1998-12-28 2003-10-14 セントラル硝子株式会社 トリフルオロメタンスルホニルクロリドの製造方法
WO2004096759A1 (ja) 2003-04-25 2004-11-11 Showa Denko K.K. パーフルオロアルカンスルホニルフルオライドの製造方法

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5540818A (en) * 1993-01-18 1996-07-30 Central Glass Co., Ltd. Process for the production of high purity methanesulphonyl fluoride at an improved yield
JP2008255100A (ja) * 2007-03-09 2008-10-23 Central Glass Co Ltd トリフルオロメタンスルホニルフルオリドの製造方法

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2732398A (en) 1953-01-29 1956-01-24 cafiicfzsojk
JPS51125322A (en) 1975-03-21 1976-11-01 Bayer Ag Process for manufacturing sulfonic acid fluoride
JPH0672987A (ja) 1992-08-25 1994-03-15 Nippon Bayeragrochem Kk メタンスルホニルフルオライド誘導体の製造方法
JPH06263715A (ja) * 1993-01-18 1994-09-20 Central Glass Co Ltd 高純度メタンスルホニルフロライドの製造法
JP3444477B2 (ja) 1998-12-28 2003-09-08 セントラル硝子株式会社 トリフルオロメタンスルホニルクロリドの製造方法
JP3456634B2 (ja) 1998-12-28 2003-10-14 セントラル硝子株式会社 トリフルオロメタンスルホニルクロリドの製造方法
JP2000264871A (ja) 1999-03-16 2000-09-26 Central Glass Co Ltd トリフルオロメタンスルホニルクロリドの製造方法
JP2003206272A (ja) 2001-12-28 2003-07-22 Kanto Denka Kogyo Co Ltd 含フッ素アルカンスルホニルフルオリドの製造方法
WO2004096759A1 (ja) 2003-04-25 2004-11-11 Showa Denko K.K. パーフルオロアルカンスルホニルフルオライドの製造方法

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
O. A. RADCHENKO; A. YA. IL'CHENKO; L. M. YAGUPOL'SKII, ZH. ORG. KHIM., vol. 15, 1981, pages 500 - 503
See also references of EP2216325A4 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2014016130A1 (fr) 2012-07-23 2014-01-30 Rhodia Operations Procédé de préparation d'un composé sulfonimide et de ses sels
JP2015057379A (ja) * 2013-08-09 2015-03-26 ダイキン工業株式会社 フッ化メタンの製造方法

Also Published As

Publication number Publication date
EP2216325A1 (en) 2010-08-11
EP2216325A4 (en) 2012-02-15
JP5347431B2 (ja) 2013-11-20
CN101842348A (zh) 2010-09-22
CN101842348B (zh) 2013-06-05
JP2009132695A (ja) 2009-06-18
EP2216325B1 (en) 2015-01-14

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