WO2005007342A1 - 研磨装置 - Google Patents
研磨装置 Download PDFInfo
- Publication number
- WO2005007342A1 WO2005007342A1 PCT/JP2004/010364 JP2004010364W WO2005007342A1 WO 2005007342 A1 WO2005007342 A1 WO 2005007342A1 JP 2004010364 W JP2004010364 W JP 2004010364W WO 2005007342 A1 WO2005007342 A1 WO 2005007342A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- ring
- polishing
- retainer ring
- top ring
- polished
- Prior art date
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Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B24—GRINDING; POLISHING
- B24B—MACHINES, DEVICES, OR PROCESSES FOR GRINDING OR POLISHING; DRESSING OR CONDITIONING OF ABRADING SURFACES; FEEDING OF GRINDING, POLISHING, OR LAPPING AGENTS
- B24B37/00—Lapping machines or devices; Accessories
- B24B37/27—Work carriers
- B24B37/30—Work carriers for single side lapping of plane surfaces
- B24B37/32—Retaining rings
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B24—GRINDING; POLISHING
- B24B—MACHINES, DEVICES, OR PROCESSES FOR GRINDING OR POLISHING; DRESSING OR CONDITIONING OF ABRADING SURFACES; FEEDING OF GRINDING, POLISHING, OR LAPPING AGENTS
- B24B49/00—Measuring or gauging equipment for controlling the feed movement of the grinding tool or work; Arrangements of indicating or measuring equipment, e.g. for indicating the start of the grinding operation
- B24B49/16—Measuring or gauging equipment for controlling the feed movement of the grinding tool or work; Arrangements of indicating or measuring equipment, e.g. for indicating the start of the grinding operation taking regard of the load
Definitions
- the present invention relates to a polishing apparatus, and more particularly, to a polishing apparatus that holds an object to be polished such as a semiconductor wafer and presses the object against a polishing surface to polish the object.
- the thickness of the film at the stepped portion becomes thinner when the thin film is formed, or a short circuit occurs due to an open circuit due to disconnection of the wiring or an insulation failure between the wiring layers. Yield tends to decrease. In addition, even if it operates normally in the beginning, there is a problem of reliability when used for a long time. Furthermore, during the exposure in the lithography step, if the irradiation surface has irregularities, the lens focus of the exposure system will be partially out of focus, and if the irregularities on the surface of the semiconductor device increase, it becomes difficult to form a fine pattern itself. Problem arises.
- CMP chemical mechanical polishing
- a polishing liquid containing abrasive grains such as silica (SiO 2) is supplied onto a polishing surface such as a polishing pad while a substrate such as a semiconductor wafer is brought into sliding contact with the polishing surface. Polishing.
- This type of polishing apparatus includes a polishing table having a polishing surface composed of a polishing pad, and a top ring for holding a semiconductor wafer.
- a polishing table having a polishing surface composed of a polishing pad, and a top ring for holding a semiconductor wafer.
- the polishing pad Since the polishing pad has a characteristic, the pressing force applied to the outer peripheral edge of the semiconductor wafer being polished becomes uneven, so that only the outer peripheral edge of the semiconductor wafer is polished so much, that is, so-called “edge dripping” occurs. There are cases.
- the outer peripheral edge of the semiconductor wafer W is held by the retainer ring 600 and is located on the outer peripheral side of the semiconductor wafer W by the retainer ring 600.
- a top ring having a structure for pressing the polished surface 610 is also used. In this type of top ring, as shown in FIG.
- a retainer ring 600 is fixed to an outer peripheral portion of a disk-shaped housing (flange portion) 60, and is attached to a central portion of the housing 62.
- the pressing force of the connected top ring shaft 630 is pressed against the polishing surface 610.
- the portion pressing the object to be polished W tends to be complicated. Since the top ring has a complicated pressing function, the part where the retainer ring 600 is attached to the housing 62 is separated from the outer peripheral edge of the workpiece W in the circumferential direction, resulting in structural overhaul. State. The bending moment M caused by this overhang. As a result, as shown in FIG. 1, the retainer ring 600 is bent, and the surface pressure of the retainer ring 600 on the polished surface 6100 becomes uneven. If the retainer ring 600 undergoes uneven wear due to the passage of the polishing time, the polishing profile changes, which adversely affects the polishing stability.
- the retainer ring 600 attached to the top ring and holding the outer periphery of the object to be polished 600 has a function of holding the object to be polished W
- a function of uniformly pressing the surface 6 10 Disclosure of the invention
- the present invention has been made in view of the above problems, and a first object of the present invention is to provide a polishing apparatus capable of performing high-precision polishing by preventing or reducing uneven wear of a retainer ring during polishing. And
- the present invention can be carried on the polishing apparatus It is a third object of the present invention to provide a retainer ring capable of performing the dummy polishing on another dedicated device or a machine tool.
- a polishing surface a top ring for holding an object to be polished, and a top ring for pressing the top ring against the polishing surface
- a polishing apparatus provided with a shaft (the top ring includes a retainer ring for holding an outer peripheral edge of the object to be polished, a substantially disk-shaped housing connected to the top ring shaft, and the retainer ring; A sliding contact connecting portion that connects the retainer ring and the housing in a state in which the housing is in sliding contact with the housing;
- the sliding contact portion may be a free joint, preferably a pole joint, for slidingly contacting the retainer ring and the housing.
- a polishing apparatus including a polishing surface, a top ring for holding an object to be polished, and a top shaft for pressing the top ring against the polishing surface.
- the above-mentioned top ring is the above-mentioned polishing PT / JP2004 / 010364
- a retainer ring for holding an outer peripheral edge of the object, a substantially disk-shaped housing connected to the topping shaft, and a connection portion for connecting the retainer ring and the housing.
- the connecting portion is configured to have low bending stiffness while sufficiently securing horizontal and vertical stiffness.
- the rigidity of the connecting portion in the horizontal and vertical directions is increased, the load due to the top ring shaft can be reliably transmitted to the retainer ring. Further, since the bending rigidity of the connecting portion is reduced, the bending moment due to the load applied to the housing is absorbed by the connecting portion, and the bending moment acting on the retainer ring can be reduced. Therefore, it is possible to suppress the retainer ring from being tilted and reduce uneven wear of the bottom surface of the retainer ring.
- connection portion is disposed outside a center of a radial width of the retainer ring.
- the connection part By arranging the connection part outside the center of the retainer ring in the radial direction, the load of the top ring shaft is applied to the outside of the center of the retainer ring in the radial direction. A bending moment is generated. The bending moment cancels the bending moment due to the load applied to the housing, and the bending moment acting on the retaining ring can be further reduced. Therefore, uneven wear on the bottom surface of the retainer ring can be more effectively reduced.
- the connecting portion may have a constricted cross-sectional shape at a central portion in the vertical direction.
- a polishing apparatus including a polishing surface, a top ring for holding an object to be polished, and a top ring shaft for pressing the top ring against the polishing surface.
- the above-mentioned top ring is the above-mentioned polishing T JP2004 / 010364
- the rigidity of the housing is increased so that the inclination of the bottom surface of the retainer ring with respect to the polishing surface is reduced.
- high rigidity can be obtained by forming the housing from a material having high strength and rigidity such as metal and ceramics and increasing the thickness thereof. In this way, by increasing the rigidity of the housing, even if a load is applied to the central part of the housing by the top ring shaft, the bending moment is less likely to act on the retaining ring, reducing uneven wear of the retaining ring. be able to.
- a polishing apparatus for polishing an object to be polished such as a semiconductor wafer to a flat and mirror surface.
- the polishing apparatus includes a polishing surface and a top ring that slides while pressing an object to be polished against the polishing surface.
- the top ring includes a retainer ring that holds an outer peripheral edge of the polishing target.
- the retainer ring has a first ring portion made of resin, a second ring portion made of metal or ceramic, and the first ring portion and the second ring portion can be detachably attached in two layers in a vertical direction. And a fastener to be fastened.
- the reliability of the fastening between the first ring portion and the second ring portion can be improved. Also, by replacing only the first ring portion that is worn, the retainer ring can be regenerated, and the cost of parts consumption can be reduced. Also, when the retainer ring is fastened to the lower surface of the outer peripheral portion of the housing with a detachable fastener, the tightening stress can be received by the second ring portion made of a highly rigid metal or ceramic, Deformation of the retainer ring is suppressed, enabling dummy polishing 00 value 0364
- the first ring portion preferably contacts the polishing surface. Further, the first ring portion preferably contains particles that act as abrasive grains when shaved. In this case, since the particles shaved off the first ring portion of the retainer ring act as abrasive grains, the abrasive grains are supplied from the retainer ring only by supplying pure water to the polished surface, for example.
- the retainer ring further includes a fitting portion that fits the first ring portion and the second ring portion. According to such a configuration, assembling of the retainer ring becomes easy, and the reliability of fastening of the first ring portion and the second ring portion is further improved.
- the retainer ring is configured to be reproducible only by replacing the first ring portion. Since the retainer ring can be regenerated only by replacing the first ring portion, the cost of consumables can be reduced and the environmental load can be reduced.
- the fastener is a porto.
- the first ring portion and the second ring portion can be easily assembled and disassembled.
- a retainer ring for holding an outer peripheral surface of an object to be polished held on a substrate holding surface of a top ring.
- the retainer ring includes a first ring portion made of resin, a second ring portion made of metal or ceramic, and the first ring portion and the second ring portion being detachably attached in two layers in a vertical direction. And a fastener for fastening as much as possible.
- the first ring portion is flattened and polished.
- the first fastener and the second fastener can be detachably connected to each other.
- the first ring portion After forming the retainer ring having a two-layer structure in the vertical direction, the first ring portion can be flattened and polished. Therefore, there is no need to perform dummy polishing on a polishing apparatus as in the related art.
- FIG. 1 is a schematic diagram showing a conventional top ring.
- FIG. 2 is a schematic diagram illustrating the overall configuration of the polishing apparatus according to the first embodiment of the present invention.
- FIG. 3 is a vertical cross-sectional view of an entire cross section of the top ring in the polishing apparatus of FIG.
- FIG. 4 is a longitudinal sectional view of another cut surface of the top ring in the polishing apparatus of FIG.
- FIG. 5 is a plan view showing a sliding contact portion (housing) of the top ring of FIG.
- FIG. 6 is a longitudinal sectional view showing a modification of the top ring in FIG.
- FIG. 7 is a longitudinal sectional view showing a top ring according to the second embodiment of the present invention.
- FIG. 8 is a diagram schematically showing the top ring of FIG.
- FIG. 9 is a longitudinal sectional view showing a top ring according to the third embodiment of the present invention.
- FIG. 10A is a longitudinal sectional view showing a mounting portion of the retainer ring of the top ring shown in FIG.
- FIG. 10B is a diagram showing a surface pressure distribution in the retaining ring of FIG. 10A.
- Fig. 11 shows an example of the port arrangement in the retainer ring shown in Fig. 9. 0364
- FIG. 9 is a plan view shown.
- FIG. 12 is a plan view showing another example of the arrangement of the bolts in the retainer ring shown in FIG.
- FIG. 13A is a longitudinal sectional view showing a mounting portion of a conventional top ring retainer ring.
- FIG. 13B is a diagram showing a surface pressure distribution in the retainer ring of FIG. 13A.
- FIG. 14 is a longitudinal sectional view showing a top ring according to the fourth embodiment of the present invention.
- FIG. 15 is a cross-sectional view showing a modification of the top ring of FIG.
- FIG. 16 is a cross-sectional view showing a modification of the topping of FIG.
- FIG. 17A is an enlarged cross-sectional view of a main part of the top ring according to the fifth embodiment of the present invention.
- FIG. 17B is an enlarged sectional view of a main part of the top ring according to the sixth embodiment of the present invention.
- FIG. 18A and FIG. 18B are enlarged cross-sectional views showing a modification of the retainer ring of the top ring of FIG.
- FIG. 19 is an enlarged sectional view showing a modification of the retainer ring of the top ring of FIG.
- FIG. 20 is a graph showing the surface pressure distribution along the radial direction of the bottom surface of the retaining ring shown in FIG. 17B.
- FIG. 2 is a schematic diagram illustrating the overall configuration of the polishing apparatus according to the first embodiment of the present invention.
- a polishing table 100 having a polishing pad 101 attached to its upper surface is provided below the top ring 1.
- a polishing liquid supply nozzle 102 is provided above the polishing table 100.From the polishing liquid supply nozzle 102, a polishing pad 101 on the polishing table 100 is placed. Polishing liquid Q is supplied.
- polishing pads there are various polishing pads available on the factory.
- SUBA800Surfinxxx-5, Surfin0000 is a nonwoven fabric obtained by hardening fibers with a resin resin
- IC100 is a rigid foamed resin (single layer). is there.
- Foamed polyurethane is porous and has many fine dents or holes on its surface.
- the top ring 1 is connected to the top ring shaft 11 via a universal joint 10, and the top ring shaft 11 is a top ring air cylinder 1 fixed to the top ring head 110. 1 Connected to 1.
- the top ring 1 includes a substantially disk-shaped housing 2 (flange portion) connected to the lower end of the top ring shaft 11, and a retaining ring 3 arranged on the outer periphery of the housing 2.
- the air cylinder 1 1 1 for the top ring is connected to the pressure adjusting section 1 20 via the regulator R 1.
- the pressure adjusting section 120 supplies a pressurized fluid such as pressurized air from a compressed air source, or a pump or the like. 2004/010364
- the pressure is adjusted by evacuation according to 1 1.
- the pressure adjusting section 120 can adjust the air pressure of the pressurized air supplied to the topping air cylinder 111 through the regulator R 1.
- the top ring air cylinder 1 1 1 is moved up and down by the top ring air cylinder 1 1 1 to move up and down the entire top ring 1, and at the same time, polish the retainer ring 3 attached to the housing 2 with a predetermined pressing force. It can be pressed to 0.
- the top ring shaft 11 is connected to the rotary cylinder 112 via a key (not shown).
- the rotary cylinder 112 has an evening pulley 113 on its outer periphery.
- the top ring head 110 is fixed with a top ring module 1 1 4 and the timing plate 1 13 is a timing belt. It is connected to the evening pulley 1 16 provided in 4. Therefore, by rotating the top ring motor 1 14, the rotating cylinder 1 1 2 and the top ring shaft 1 1 1 are rotated via the timing pulley 1 16, the evening timing belt 1 15, and the timing pulley 1 13.
- -Top ring 1 rotates.
- the top ring head 110 is supported by a top ring head shaft 117 rotatably supported by a frame (not shown).
- FIG. 3 is a vertical cross-sectional view of the entire top ring 1 in Fig. 2
- Fig. 4 is a vertical cross-sectional view of another cut surface of the top ring 1 in Fig. 2
- Fig. 5 is a housing 2 of the top ring 1 in Fig. 3.
- the retainer ring 3 includes a substantially cylindrical upper member 3 a and a substantially cylindrical lower member 3 b, and a lower portion of the lower member 3 b It protrudes inward.
- a ball joint 4 as a free joint for slidingly contacting the retainer ring 3 and the housing 2 is provided above the upper member 3a of the retainer ring 3 in a circle of the retainer ring 3. It is provided at a plurality of locations in the circumferential direction.
- the pole joint 4 is interposed between a spherical concave portion 2 a formed on the lower surface of the housing 2 and a spherical concave portion 3 c formed on an upper part of the upper member 3 of the retainer ring 3.
- connection ports 5 are provided at a plurality of positions in the circumferential direction.
- the housing 2 is provided with a spring receiver 2b corresponding to the connection port 5, and the coil spring 6 is interposed between the connection port 5 and the spring receiver 2b.
- the pole joint 4, the connection port 5, the spring receiver 2b, and the coil spring 6 form a sliding contact connecting portion that connects the retainer ring 3 and the housing 2 in a state of sliding contact with each other.
- the pawl joint 4 slides the retainer ring 3 and the housing 2 is described.
- any structure that slides the retainer ring 3 and the housing 2 is used. May be used.
- the top ring shaft 11 is disposed above the central portion of the housing 2, and the housing 2 and the top ring shaft 11 are connected by the universal joint 10.
- the universal joint 10 includes a spherical bearing mechanism that enables the housing 2 and the top ring shaft 11 to be able to tilt with respect to each other, and a rotation transmission mechanism that transmits the rotation of the top ring shaft 11 to the housing 2. The pressing force and the rotational force are transmitted while allowing the top ring shaft 11 to tilt from the housing 2 to each other.
- the spherical bearing mechanism has a spherical surface formed in the center of the lower surface of the top ring shaft 11.
- connection port 7 is attached near the top ring shaft 11 of the housing 2, and a connection port 7 is provided between the connection port 7 and a spring receiver 1 1b provided on the top ring shaft 11. Is provided with a coil spring 8. With such a structure, the housing 2 is held so as to be tiltable with respect to the top ring shaft 11.
- the rotation transmission mechanism includes an engagement pin 9 fixed near the top ring shaft 11 of the housing 2 and an engagement hole 11 c formed in the top ring shaft 11. Even if the housing 2 is tilted, the engaging pin 9 can be moved up and down in the engaging hole 11c, so that the engaging pin 9 engages with the engaging hole 11c by shifting the contact point.
- the rotation transmission mechanism surely transmits the rotation torque of the top ring shaft 11 to the housing 2.
- An elastic pad 20 abutting on the semiconductor wafer W held by the top ring 1, an annular holder ring 21, and an elastic pad 20 And a substantially disk-shaped chucking plate 22 for supporting the same.
- the outer periphery of the elastic pad 20 is sandwiched between the holder ring 21 and the chucking plate 22 fixed to the lower end of the holder ring 21, and the lower surface of the chucking plate 22 is attached to the elastic pad 20. Covering.
- a pressure chamber 30 is formed between the elastic pad 20 and the chucking plate 22.
- the elastic pad 20 is made of ethylene propylene rubber (EPDM), polyurethane rubber, silicon rubber, etc. It is made of rubber material with excellent durability.
- An opening 22 a is formed at the center of the chucking plate 22.
- the opening 22 a communicates with the fluid path 40 including a tube, a connector, and the like, and is disposed on the fluid path 40. It is connected to the pressure regulator 120 via R2. That is, the pressure chamber 30 between the elastic pad 20 and the chucking plate 22 is connected to the pressure adjusting unit 120 via the regulator R 2 arranged on the fluid path 40. .
- a pressure sheet 23 made of an elastic film is stretched between the holder ring 21 and the housing 2.
- One end of the pressure sheet 23 is sandwiched by a pressure sheet support 2 d attached to the lower surface of the housing 2, and the other end is formed between the upper end 21 a of the holder ring 21 and the stopper 21 b. It is sandwiched between.
- a pressure chamber 31 is formed inside the housing 2 by the housing 2, the chucking plate 22, the holder ring 21, and the pressure sheet 23.
- the pressure chamber 31 communicates with a fluid path 41 composed of a tube, a connector, and the like, and the pressure chamber 31 is connected to the pressure chamber 31 via a regulator R 3 arranged on the fluid path 41.
- the pressure sheet 23 is formed of a rubber material having excellent strength and durability, such as ethylene propylene rubber (EPDM), polyurethane rubber, and silicone rubber.
- the pressure chambers 30 between the chucking plate 22 and the elastic pad 20 and the pressure chamber 31 above the chucking plate 22 have the pressure chambers 30 and 31 respectively.
- a pressurized fluid such as pressurized air or the like can be supplied through the fluid paths 40 and 41 connected to each other, or the pressure can be adjusted to atmospheric pressure or vacuum. That is, as shown in Fig. 2, the pressure chambers 30 and 31 are supplied to the respective pressure chambers by the regulators R2 and R3 arranged on the flow paths 40 and 41 of the pressure chambers 31 and 31, respectively. The pressure of the pressurized fluid can be adjusted. this 0364
- the pressure inside each of the pressure chambers 30 and 31 can be controlled independently or can be set to atmospheric pressure or vacuum.
- the chucking plate 22 has an inner suction portion 24 and an outer suction portion 25 protruding downward, provided outside the opening 22a.
- the inner suction portion 24 has a communication hole 24a communicating with the fluid passage 42 composed of a tube, a connector, and the like, and the inner suction portion 40 is disposed on the fluid passage 42.
- the outer suction part 25 is connected to the fluid path 43 composed of a tube, a connector, etc. Is formed, and the outer adsorbing portion 25 is connected to the pressure adjusting portion 120 via a regulator R 5 arranged on the fluid passage 43.
- a negative pressure is formed at the open ends of the communication holes 24 a, 25 a of the suction portions 24, 25 by the pressure adjustment portion 120, and the semiconductor wafer W is suctioned to the suction portions 24, 25.
- An elastic sheet made of a thin rubber sheet or the like is adhered to the lower end surfaces of the suction sections 24 and 25, and the suction sections 24 and 25 are adapted to flexibly hold the semiconductor wafer W by suction. ing.
- a cleaning liquid passage 26 is formed in the upper member 3 a of the retainer ring 3.
- the cleaning liquid passage 26 communicates with a small gap between the outer peripheral surface of the elastic pad 20 and the lower member 3 b of the retainer ring 3.
- the cleaning liquid (pure water) is supplied to the gap through the cleaning liquid path 26.
- the entire top ring 1 is positioned at the transfer position of the semiconductor wafer, and the communication holes 24 a and 25 a of the suction portions 24 and 25 are fluidized. Connect to pressure regulator 120 via lines 42 and 43.
- the semiconductor wafer W is vacuum-sucked on the lower end surfaces of the suction portions 24, 25 by the suction action of the communication holes 24a, 25a.
- the top ring 1 is moved while the conductor wafer W is being sucked, and the entire top ring 1 is positioned above a polishing table 100 having a polishing surface (polishing pad 101).
- the outer peripheral edge of the semiconductor wafer W is held by the retainer ring 3 so that the semiconductor wafer W does not protrude from the top ring 1.
- the suction portions 24 and 25 release the suction of the semiconductor wafer W, hold the semiconductor wafer W on the lower surface of the top ring 1, and also operate the top ring air cylinder 11 connected to the top shaft 11. 1 is operated to press the retainer ring 3 fixed to the lower end of the top ring 1 against the polishing surface of the polishing table 100 with a predetermined pressing force. In this state, a pressurized fluid of a predetermined pressure is supplied to the pressure chamber 30 to press the semiconductor wafer W against the polishing surface of the polishing table 100 '.
- the polishing liquid Q is supplied from the polishing liquid supply nozzle 102 in advance, so that the polishing liquid Q is retained on the polishing pad 101, and the polishing surface (lower surface) of the semiconductor wafer W and the polishing pad 101 are The polishing is performed in a state where the polishing liquid Q is present during the polishing.
- the chucking plate 22 When the pressurized fluid is supplied to the pressure chamber 30, the chucking plate 22 receives an upward force. Therefore, in the present embodiment, the pressure fluid is supplied to the pressure chamber 31 via the fluid passage 41. This prevents the chucking plate 22 from being lifted upward by the force from the pressure chamber 31.
- the semiconductor wafer W is polished by the force of the retainer ring 3 being pressed against the polishing pad 101 by the top ring air cylinder 111 and the pressurized air supplied to the pressure chamber 30.
- the semiconductor wafer W is polished by appropriately adjusting the force applied to 1.
- the semiconductor wafer W is vacuum-sucked again to the lower end surfaces of the suction portions 24 and 25.
- the pressure chamber 30 that presses the semiconductor wafer W against the polishing surface 30
- the lower end surfaces of the suction portions 24 and 25 are brought into contact with the semiconductor wafer W.
- the pressure in the pressure chamber 31 is released to the atmospheric pressure or the pressure is reduced to a negative pressure. This is because if the pressure in the pressure chamber 31 is kept high, only the portion of the semiconductor wafer W that is in contact with the suction portion 40 is strongly pressed against the polished surface. .
- the entire top ring 1 is positioned at the transfer position of the semiconductor wafer, and the communication holes 24 a and 24 a of the suction portions 24 and 25 are moved.
- a fluid for example, a mixture of compressed air or a mixture of nitrogen and pure water
- the retainer ring 3 and the housing 2 are brought into sliding contact with the ball joint 4. Therefore, even if a load is applied to the center of the housing 2 by the top ring shaft 1 1, the housing 2 and the retainer ring 3 slide, so only the vertical component of the load is transmitted to the retainer ring 3, and the bending moment No longer works. As a result, the retainer ring 3 is not tilted by the bending moment, and uneven wear on the bottom surface of the retainer ring 3 can be prevented.
- the housing 2 can be made of metal or ceramics having strength and strength.
- the polishing pad is formed from a material having high rigidity and the thickness thereof is further increased to form a housing 2 having high rigidity.
- the housing 2 is made highly rigid, the bending moment will be reduced even if a load is applied to the center of the housing 2 by the top ring shaft 1 1. It hardly acts on the ring 3 and can prevent uneven wear of the retainer ring 3.
- the bending moment generated in the retainer ring 3 by the above-described indirect connection portion can be made zero. Therefore, it is not necessary to prevent the occurrence of bending moment by increasing the rigidity of the housing 2, and as shown in FIG. 6, the housing 2 can be made thinner and lighter to improve maintainability. .
- FIG. 7 is a longitudinal sectional view showing a top ring according to the second embodiment of the present invention.
- a connection portion 50 is provided instead of the sliding connection portion in the first embodiment.
- the connecting portion 50 connects the upper member 3a of the retainer ring 3 and the housing 2, and is configured to have low bending stiffness while securing sufficient horizontal and vertical stiffness. I have.
- the width of the central portion in the vertical direction is made smaller than the width of the upper and lower portions to form a constricted cross-sectional shape, so that the rigidity in the horizontal and vertical directions is sufficiently secured and the bending rigidity is reduced. ing.
- the rigidity of the connecting portion 50 in the horizontal and vertical directions is increased, the load by the topping shaft 11 can be reliably transmitted to the retaining ring 3. Also, since the bending rigidity of the connecting portion 50 is reduced, the bending moment due to the load applied to the center of the housing 2 Is absorbed by the connecting portion 5.0, and the bending moment acting on the retainer ring 3 can be reduced. Therefore, it is possible to suppress the retainer ring 3 from being tilted and reduce uneven wear of the bottom surface of the retainer ring 3.
- the housing 2, the connecting portion 50, and the upper member 3a of the retainer ring 3 are integrally formed, but the present invention is not limited to this.
- the bending moment acting on the retainer ring 3 can be reduced by the connection portion 50 having a low bending rigidity.
- the bending moment acting on the retainer ring 3 can be further reduced by arranging it outside the center of the ring. That is, by disposing the connecting portion 50 outside the center of the radial width of the retainer ring 3, as shown in FIG. 8, the top ring shaft 1 is located outside the center of the radial width of the retainer ring 3. Since the load 1 is applied, a bending moment Mi is generated at the center of the width of the retainer ring 3.
- the bending mode one instrument M moment M 2 bending due to the load applied to the central portion of the housing 2 is canceled, it is possible to further reduce the bending mode one instrument acts on the retainer ring 3. Therefore, uneven wear on the bottom surface of the retainer ring 3 can be more effectively reduced.
- one end of the pressure sheet 23 in the present embodiment is held between the upper member 3a of the retainer ring 3 and the pressure sheet support 3d provided radially inside the upper member 3a.
- it may be fixed to the housing 2 side.
- FIG. 9 is a longitudinal sectional view showing the top ring 301 in the third embodiment of the present invention.
- the top ring 301 is housed And a retainer ring 303 attached to the lower end of the outer peripheral edge of the housing 302.
- the housing 302 is formed of a material having high strength and rigidity such as metal and ceramics.
- the housing 302 includes a cylindrical container-shaped housing main body 302 a, and an annular pressure sheet supporting part 302 b fitted inside the cylindrical part of the housing main body 302 a. ing.
- a retainer ring 303 is fixed to a lower end of the housing main body 302 a of the housing 302 by a port 308.
- a top ring shaft 311 is provided above the center of the housing main body 3 02 a of the housing 302, and the housing 302 and the topping shaft 3 1 1 are connected to the universal joint 3. They are linked by 10.
- the universal joint portion 310 includes a spherical bearing mechanism that enables the housing 302 and the topping shaft 311 to be tilted relative to each other, and a rotation that transmits the rotation of the top ring shaft 311 to the housing 302.
- a transmission mechanism is provided so that the pressing force and the rotational force can be transmitted from the top ring shaft 311 to the housing 302 while allowing them to tilt each other.
- the spherical bearing mechanism includes a spherical concave portion 311a formed at the center of the lower surface of the top ring shaft 311 and a spherical concave portion 30 formed at the center of the upper surface of the housing main body 302a. 2c and a bearing pole 312 made of a hard material such as ceramics interposed between the recesses 311a and 302c.
- the rotation transmission mechanism is composed of a drive pin (not shown) fixed to the top ring shaft 311 and a driven pin (not shown) fixed to the housing main body 302a. .
- the driven pin and the driving pin can move up and down relatively, and the contact pins are shifted from each other to engage with each other, and the rotation transmitting mechanism rotates the top ring shaft 3 1 1 to rotate.
- a semiconductor wafer W as an object to be polished held by the top ring 301.
- Elastic pad 304 to be in contact with, annular holder ring 300, annular elastic pad support members 309 and 313 for supporting elastic pad 304, and elastic pad support
- a generally disk-shaped chucking plate 306 supporting the members 309 and 313 is accommodated.
- the elastic pad 304 has its outer peripheral portion sandwiched between the chucking plate 303 and the elastic pad supporting members 309, 3I3, and the elastic pad supporting members 309, 31 3 covers the lower surface.
- a pressure sheet 307 made of an elastic film is stretched between the holder ring 305 and the housing 302.
- One end of the pressure sheet 300 is connected to the housing body portion 302 a of the housing 302 and the pressure sheet support portion 300.
- a pressure chamber 314 is formed inside the housing 302 by the base plate 302, the chucking plate 306, the holder ring 305, and the pressure sheet 307.
- a fluid passage 315 such as a pipe is opened in the pressure chamber 314, and the fluid passage 315 is connected to a compressed air source via a switching valve (not shown).
- the lower end of the chucking plate 310 is opened with the end of a fluid passage 316, 319 such as a pipe, and the fluid passage 316, 319 is provided with a switching valve or a regulator not shown.
- fluid passages 317 and 318 such as pipes are opened on the lower surface of the elastic pad support members 309 and 313, and the fluid passages 317 and 318 are provided with switching valves (not shown). It is connected to a vacuum source and a compressed air source via a regire.
- the semiconductor wafer W is suction-held on the lower surfaces of the elastic pad supporting members 309 and 313. .
- the semiconductor wafer W sucked and held on the lower surface of the housing 302 is pressed against the polishing surface (the upper surface of the polishing pad) 3221 of the polishing table 320 which rotates.
- the semiconductor wafer W is polished by the relative motion between the semiconductor wafer W and the polishing surface 3221.
- the lower surface of the pressure chamber 3 14 and the chucking plate 30 6 and the semiconductor wafer W are connected via the fluid passages 3 15 ′ 3 16, 3 17, 3 18 and 3 19. Compressed air is sent between them, and the pressure is adjusted to adjust the polishing table of semiconductor W 3
- the pressing force against the polished surface 3 21 of 20 is adjusted.
- FIG. 10A is a longitudinal sectional view showing a mounting portion of the retainer ring 303 of the top ring 301
- FIG. 10B is a view showing a surface pressure distribution in the retainer ring 303.
- the retainer ring 303 is formed of a first ring portion 331, made of resin, and a metal having substantially the same planar shape as the first ring portion 331, Or second ring part 3 made of ceramic
- first ring portion 331 is fastened to the lower surface of the second ring portion 332 with a port 33.
- annular groove 332a is formed on the lower surface of the second ring portion 332, and an annular groove fitted on the groove 332a is formed on the upper surface of the first ring portion 331.
- a projection 331a is formed. That is, the retainer ring 303 has a fitting portion that fits the first ring portion 3311 and the second ring portion 3332. This makes it easy to assemble the first ring portion 331, with the second ring portion 332, and furthermore, the two are more firmly fastened. Such a fitting portion may not be provided. Alternatively, the first ring portion 3311 and the second ring portion 3332 may be fixed using pins instead of the fitting portions. Yes.
- the resin material of the first ring part 331 of the retainer ring 303 is polyetheretherketone (PEEK), polyphenylene sulfide (PPS), and a wholly aromatic polyimid, a super heat-resistant plastic. Resin and polycarbonate resin.
- PEEK polyetheretherketone
- PPS polyphenylene sulfide
- a wholly aromatic polyimid a super heat-resistant plastic.
- Resin and polycarbonate resin it is preferable that the first ring portion 331, which comes into contact with the polished surface 321, contains particles that act as abrasive grains when shaved or particles that do not damage the semiconductor wafer.
- a metal such as titanium or stainless steel, or a ceramic such as alumina is used so that heat transfer from the first ring portion 331 is improved.
- the material of the port 33 that fastens the first ring portion 33 1 and the second ring portion 33 32 includes the resin material of the first ring portion 33 1 and the second ring portion 33 A metal with a coefficient of thermal expansion close to that of metal 2 (titanium, stainless steel) or ceramic is preferred.
- Porto 3 33 A material having a high heat transfer coefficient is used for Porto 3 33. Further, as shown in FIG. 11, even when a plurality of ports 3333 are provided at a predetermined pitch on the circumference and the first ring portion 3311 and the second ring portion 3332 are fastened. Good. Alternatively, as shown in FIG. 12, a plurality of ports 33 may be provided at a predetermined pitch on two circumferences.
- FIG. 13A is a longitudinal sectional view showing a mounting portion of the conventional top ring 401 for retaining the retainer ring 4 40, for comparing the operation and effect thereof with the retainer ring 303 having the configuration shown in FIG. 10A. It is.
- FIG. 13A is a longitudinal sectional view showing a mounting portion of the conventional top ring 401 for retaining the retainer ring 4 40, for comparing the operation and effect thereof with the retainer ring 303 having the configuration shown in FIG. 10A. It is.
- FIG. 13B is a view showing a surface pressure distribution in the retainer ring 44.
- the retainer ring 440 is integrally formed of a resin material, and is fixed to the lower surface of the outer periphery of the housing 302 by bolts.
- the retainer ring 440 integrally formed of such a resin material is deformed by the fastening force of the por 1 attached to the housing 302, so that a new retainer ring 440 is provided for the housing 302. After attaching 0, it is necessary to perform dummy polishing to remove surface irregularities due to this deformation, and this dummy polishing contributes to increase the downtime of the apparatus.
- a ring part made of stainless steel (or titanium or ceramic) and a ring part made of resin may be bonded with an adhesive to form a two-layer structure.
- Such a two-layered retainer ring is discarded together with the retainer ring due to abrasion of the resin ring portion, so that the cost of consumables and the environmental load are large.
- the reliability of the adhesive is low due to aging of the adhesive and peeling due to insufficient adhesive strength.
- the retainer ring 303 is fastened to the first ring portion 3311 and the second ring portion 3332 by a port 3333, and the retainer ring 303 is vertically Because of the layer structure, the first ring part 3 3 1 and the second ring The fastening of the part 332 is highly reliable, and the retainer ring 303 can be regenerated by replacing only the worn first ring part 331.
- an annular groove 332a is formed on the lower surface of the second ring portion 3332, and an annular protrusion fitted to the groove 3332a is formed on the upper surface of the first ring portion 331.
- the assembly of the retainer ring 30.3 becomes easy, and the first ring portion 331 and the second ring portion 332 are connected.
- the reliability of fastening is further improved.
- the retainer ring 303 can be regenerated only by replacing the first ring portion 331, the cost of consumables can be reduced and the environmental load can be reduced.
- the retainer ring 303 is assembled by assembling the retainer ring 303 with the first ring part 331 on the lower surface of the second ring part 3332 and tightening with the port 3333.
- the tightening stress of the port 308 is more rigid than that of the first ring portion 331.
- the large second ring portion 3332 is received, and deformation of the retainer ring 303 is suppressed. Therefore, it is possible to shorten the time (downtime) required for polishing and polishing for eliminating irregularities on the surface of the retainer ring 303.
- the first ring portion 331 and the second ring portion 332 that constitute the retainer ring 303 are fastened by the port 3333.
- the means for fastening the part 331 and the second ring part 332 is not limited to this, and various detachable fasteners can be used.
- a step having a small outside diameter is provided on one of the ring portions 331, 332, and a concave portion having a large inside diameter is provided on the other ring portion 332, 331, and the small outside portion is provided.
- a male screw groove is provided on the outer peripheral surface of the step portion having a large diameter
- a female screw groove is provided on the inner peripheral surface of the concave portion having a large inner diameter.
- the first ring portion 331 and the second ring portion 332 may be fastened to each other by screwing the grooves. It is also possible to use other mechanical fasteners.
- the retainer ring blocks the polishing slurry supplied from the outside of the retainer ring, so that the polishing object existing inside the retainer ring cannot be polished. It may be difficult to supply sufficient polishing slurry. For this reason, a method is conceivable in which a slit is formed on the bottom surface of the retainer ring, and polishing slurry is supplied to the polishing target placed inside the retainer ring through the slit.
- a slit is formed on the sliding surface of the retainer ring, the polishing characteristics will vary in the circumferential direction between a portion having the slit and a portion having no slit. The retainer ring in the following embodiment can prevent such an adverse effect.
- FIG. 14 is a longitudinal sectional view showing a top ring 510 according to the fourth embodiment of the present invention.
- the top ring 510 holds the semiconductor wafer W to be polished, and slides while pressing against the polishing surface of the polishing pad 5222 to advance chemical mechanical polishing. Things. That is, the top ring 5 10 includes a retainer ring 5 12 on the lower surface of the housing 5 11, and holds the outer peripheral edge of the semiconductor wafer W on the inner peripheral surface of the retainer ring 5 12.
- a plate 515 is disposed inside the housing 511 via an elastic ring 514 so as to be movable vertically, and is surrounded by the plate 515 and the housing 511.
- the pressing force against the polished surface of the semiconductor wafer W is adjusted. Therefore, the semiconductor wafer W is held by the top ring 510 and pressed while the polishing pad fixed on the polishing table 521 is pressed. When the polishing slurry slides on the polishing surface of the metal 522 and the polishing slurry is supplied to the polishing surface, chemical mechanical polishing proceeds.
- the retainer ring 512 has a notch 512a extending inward in the radial direction on the outer peripheral surface thereof.
- the retainer ring 512 is made of, for example, a plastic resin, and a notch 512a having a width of about 0.5 mm to lmm (in the height direction of the retainer ring 512) has an entire circumference in this embodiment. Is formed along. It is preferable that the (radial) depth of the notch 5 1 2 a be set to about / of the (radial) width of the retainer ring 5 1 2.
- the width and depth of the notch 5 1 2a are of course determined as appropriate according to the dimensions, material, and the like of the entire retainer ring.
- the notch 5 12 a does not necessarily need to be formed over the entire circumference, but may be formed partially.
- the notch 5 12 a is preferably filled with an elastic body 5 19 such as rubber by a mold or the like.
- an elastic body 5 19 such as rubber by a mold or the like.
- the notch 5 1 2 a may be formed at the boundary between the retainer ring 5 1 2 and the bottom surface of the housing 5 1 1 as shown in FIG. 16 ⁇ that is, the retainer ring 5 1 A non-contact portion (notch) 512a is provided on the outer peripheral side of the joint portion between the 2 and the housing 511.
- the rigidity in the vertical direction can be reduced toward the outer peripheral side of the retainer ring 5 12, and the surface pressure of the polished surface on the bottom surface of the retainer ring 5 12 can be reduced as it moves toward the outer peripheral side.
- the polishing slurry can be easily sunk into the inner peripheral side of the retainer ring 512 as described above.
- the non-contact portion 512a provided between the bottom surface of the housing 511 and the upper surface of the retainer ring 512 shown in Fig. 16 may be filled with an elastic body such as rubber. .
- an elastic body such as rubber.
- FIG. 17A shows a part of the top ring 510 according to the fifth embodiment of the present invention.
- an extension portion 5 12 c extending to the outer peripheral side is arranged at the bottom of the cylindrical retainer ring 5 12. Since the extension 5 1 2 c is thinner than the thicker portion of the retainer ring 5 1 2, the rigidity in the vertical direction with respect to the bottom surface of the retainer ring 5 1 2 Can be reduced.
- FIG. 17B shows a part of the top ring 5 10 in the sixth embodiment of the present invention.
- This topping 5 10 is located just above the extension 5 12 c. Put it? ) As shown in FIG.
- the extension 5 12 c of FIGS. 17A and 17B is, for example, about 1 mm to 2 mm in thickness and about 5 mm in length in the radial direction 5 12 c. Is preferred.
- the width is about 0.5 mm to lmm and the length (in the radial direction) of the retainer ring is It is preferably of the order of 2 Z 3 of the width (in the radial direction).
- these dimensions should be changed as appropriate according to the overall dimensions, material, and the like of the retaining ring 512.
- the extension portion 512c and the notch 5122a do not necessarily need to be formed along the entire circumference, but may be provided partially.
- FIGS. 18A and 18B are examples in which the retainer ring 5 12 shown in FIG. 14 is made of a plurality of materials.
- the material of the ring part 512f that is in contact with the polished surface 522 is made of corrosion-resistant material, and the retainer that is in contact with the housing 511.
- the material of the part 512 d may be made of stainless steel.
- FIG. 18A an intermediate medium 512e may be provided on the bonding surface of the ring portion 512f and the retainer portion 512d.
- FIG. 18B the ring portion 512f and the retainer portion 512d can be directly bonded.
- FIG. 19 shows a modification of the retainer ring 5 12 shown in FIG.
- the material of the portion 512 h with reduced rigidity is easier to cut than the material of the portion 512 g whose rigidity is not reduced.
- the part with reduced rigidity 512 h is composed of PPS
- the part without reduced rigidity 51 g is composed of PEEK, and they are joined together.
- the pressure of the low rigidity portion 5 12 h is also reduced, so that the scraping rate of the retainer ring 5 12 itself is lower than that of the portion 5 12 g whose rigidity is not reduced.
- the step due to the difference in the amount of shaving changes the surface pressure distribution of the retainer ring 5 12. If the initial surface pressure distribution cannot be obtained, the amount of slurry supplied to the semiconductor wafer will change. Therefore, the difference in the amount of shaving can be suppressed by using a material having low rigidity 512h that is easily shaved.
- the rigidity of the portion where the shaved portion cannot be shaved is further reduced. That is, by optimizing the position height and depth of the notch 512a, it is possible to suppress a change in the surface pressure distribution even if the amount of shaving is different for the same material.
- a portion having high rigidity is cut first, and a high surface pressure distribution is applied to a portion that cannot be cut. Therefore, by appropriately designing the size of the notch 5 1 2a, a uniform distribution of the shaving amount can be obtained.
- FIG. 20 is a graph showing a surface pressure distribution in the retainer ring 512 shown in FIG. 17B.
- the surface pressure distribution is the highest, and at the outer peripheral surface R i of the retainer ring 512, the surface pressure distribution is reduced due to the interaction between the notch 512a and the extension 512c.
- extension 5 1 2 In the outer circumferential surface R 2 of c, the surface pressure is further reduced.
- the semiconductor wafer W to be polished and the retainer ring 512 are polished between the top ring 510 that rotates and the polishing surface 522 of the polishing pad 522 that rotates or rotates and revolves.
- the polishing slurry can sink into the space between the bottom surface of the polishing pad 5 and the polishing surface of the polishing pad 5 22 to easily supply the polishing slurry to the inside of the retainer ring 512.
- the polishing slurry can be uniformly supplied to the entire surface of the semiconductor wafer W to be polished, and uniform polishing characteristics can be obtained.
- the polishing slurry is transferred from the back surface of the polishing pad 52 to the upper surface of the polishing pad 52 (the polishing surface) through at least one opening provided in the polishing pad 52 at least at a portion where the semiconductor wafer W contacts. ),
- the retainer ring 512 provided with the notch 512a is used from the surface to be polished of the semiconductor wafer W to the outer periphery of the retainer ring 512 by the operation of the retainer ring 512 as described above. Since the finished polishing slurry is discharged well, a new polishing slurry can always be uniformly supplied to the surface to be polished of the semiconductor wafer W, so that uniform polishing characteristics can be obtained.
- Such a method of supplying the polishing slurry is suitable when the polishing pad revolves (with a radius e) or when the top ring 510 passes through the center of the polishing pad 522 which rotates.
- the sliding surface of the retainer ring has a size and a size that does not cancel the surface pressure gradient effect of the retainer ring 512 due to the notch 5 12a.
- a slit having a shape may be provided to further promote uniform slurry supply to the surface to be polished.
- the polishing slurry can be easily and uniformly supplied into the retainer ring that holds the outer peripheral edge of the polishing target.
- a polishing apparatus capable of obtaining good polishing characteristics over the entire surface of the object to be polished.
- the pulling can be applied to the object that holds the outer peripheral edge of the object to be polished and slides on the polished surface. It is not limited to what rotates.
- the present invention can be applied to, for example, a structure in which a top ring holds an object to be polished and performs a reciprocating motion with respect to a polishing surface.
- the present invention is not limited to the polishing apparatus having the polishing table.
- the present invention can be applied to any polishing apparatus that polishes the object to be polished by the relative motion between the object to be polished and the polished surface by pressing the object to be polished held by the top ring against the surface to be polished. Can be applied.
- the present invention can be suitably used for a polishing apparatus that holds an object to be polished such as a semiconductor wafer and presses the object to be polished, and polishes the object to be polished.
Landscapes
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Finish Polishing, Edge Sharpening, And Grinding By Specific Grinding Devices (AREA)
- Mechanical Treatment Of Semiconductor (AREA)
- Grinding-Machine Dressing And Accessory Apparatuses (AREA)
Description
Claims
Priority Applications (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US10/562,877 US20060128286A1 (en) | 2003-07-16 | 2004-07-14 | Polishing apparatus |
US11/797,721 US20070212988A1 (en) | 2003-07-16 | 2007-05-07 | Polishing apparatus |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2003275406A JP2005034959A (ja) | 2003-07-16 | 2003-07-16 | 研磨装置及びリテーナリング |
JP2003-275406 | 2003-07-16 |
Related Child Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US11/797,721 Division US20070212988A1 (en) | 2003-07-16 | 2007-05-07 | Polishing apparatus |
Publications (1)
Publication Number | Publication Date |
---|---|
WO2005007342A1 true WO2005007342A1 (ja) | 2005-01-27 |
Family
ID=34074551
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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PCT/JP2004/010364 WO2005007342A1 (ja) | 2003-07-16 | 2004-07-14 | 研磨装置 |
Country Status (4)
Country | Link |
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US (2) | US20060128286A1 (ja) |
JP (1) | JP2005034959A (ja) |
TW (1) | TWI283617B (ja) |
WO (1) | WO2005007342A1 (ja) |
Cited By (1)
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TWI819035B (zh) * | 2018-07-31 | 2023-10-21 | 日商荏原製作所股份有限公司 | 具備球面軸承之連結機構、球面軸承之軸承半徑決定方法、及基板研磨裝置 |
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JP2008023603A (ja) * | 2006-07-18 | 2008-02-07 | Nippon Seimitsu Denshi Co Ltd | 2層構造のリテーナリング |
JP2008093810A (ja) * | 2006-10-16 | 2008-04-24 | Shin Etsu Handotai Co Ltd | リテーナリング及び研磨ヘッド並びに研磨装置 |
JP2008229790A (ja) * | 2007-03-22 | 2008-10-02 | Nec Electronics Corp | リテーナリングおよび研磨装置 |
JP5464820B2 (ja) | 2007-10-29 | 2014-04-09 | 株式会社荏原製作所 | 研磨装置 |
KR101055002B1 (ko) * | 2008-12-11 | 2011-08-05 | 한상효 | 씨엠피장치용 리테이너링 |
JP5505713B2 (ja) * | 2010-04-26 | 2014-05-28 | 株式会社Sumco | 研磨液分配装置及びこれを備えた研磨装置 |
TWI674171B (zh) * | 2012-01-31 | 2019-10-11 | 日商荏原製作所股份有限公司 | 基板保持裝置、研磨裝置、及研磨方法 |
JP6403981B2 (ja) * | 2013-11-13 | 2018-10-10 | 株式会社荏原製作所 | 基板保持装置、研磨装置、研磨方法、およびリテーナリング |
US9597771B2 (en) * | 2013-12-19 | 2017-03-21 | Taiwan Semiconductor Manufacturing Co., Ltd. | Carrier head having retainer ring, polishing system including the carrier head and method of using the polishing system |
KR102173323B1 (ko) * | 2014-06-23 | 2020-11-04 | 삼성전자주식회사 | 캐리어 헤드, 화학적 기계식 연마 장치 및 웨이퍼 연마 방법 |
JP6449194B2 (ja) * | 2015-05-25 | 2019-01-09 | 株式会社荏原製作所 | 研磨装置、研磨ヘッド、およびリテーナリング |
CN113829233B (zh) * | 2021-08-21 | 2023-07-18 | 浙江晶盛机电股份有限公司 | 一种抛光载体 |
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Also Published As
Publication number | Publication date |
---|---|
TW200514649A (en) | 2005-05-01 |
US20060128286A1 (en) | 2006-06-15 |
US20070212988A1 (en) | 2007-09-13 |
JP2005034959A (ja) | 2005-02-10 |
TWI283617B (en) | 2007-07-11 |
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