WO2000044120A1 - Synchronization of ofdm signals - Google Patents

Synchronization of ofdm signals Download PDF

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Publication number
WO2000044120A1
WO2000044120A1 PCT/US2000/001399 US0001399W WO0044120A1 WO 2000044120 A1 WO2000044120 A1 WO 2000044120A1 US 0001399 W US0001399 W US 0001399W WO 0044120 A1 WO0044120 A1 WO 0044120A1
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Prior art keywords
symbol
phases
subject matter
correlation
determining
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Ceased
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PCT/US2000/001399
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English (en)
French (fr)
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WO2000044120A8 (en
Inventor
Lawrence W. Yonge
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Atheros Powerline LLC
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Intellon Corp
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Priority to JP2000595449A priority Critical patent/JP4751986B2/ja
Priority to EP00909936A priority patent/EP1145470B1/en
Priority to AT00909936T priority patent/ATE487295T1/de
Priority to AU32113/00A priority patent/AU3211300A/en
Priority to CA002358931A priority patent/CA2358931C/en
Priority to DE60045186T priority patent/DE60045186D1/de
Publication of WO2000044120A1 publication Critical patent/WO2000044120A1/en
Publication of WO2000044120A8 publication Critical patent/WO2000044120A8/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

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Classifications

    • HELECTRICITY
    • H04ELECTRIC COMMUNICATION TECHNIQUE
    • H04LTRANSMISSION OF DIGITAL INFORMATION, e.g. TELEGRAPHIC COMMUNICATION
    • H04L27/00Modulated-carrier systems
    • H04L27/26Systems using multi-frequency codes
    • H04L27/2601Multicarrier modulation systems
    • H04L27/2647Arrangements specific to the receiver only
    • H04L27/2655Synchronisation arrangements
    • H04L27/2662Symbol synchronisation
    • HELECTRICITY
    • H04ELECTRIC COMMUNICATION TECHNIQUE
    • H04LTRANSMISSION OF DIGITAL INFORMATION, e.g. TELEGRAPHIC COMMUNICATION
    • H04L27/00Modulated-carrier systems
    • H04L27/26Systems using multi-frequency codes
    • H04L27/2601Multicarrier modulation systems
    • H04L27/2647Arrangements specific to the receiver only
    • H04L27/2655Synchronisation arrangements
    • H04L27/2668Details of algorithms
    • H04L27/2673Details of algorithms characterised by synchronisation parameters
    • H04L27/2676Blind, i.e. without using known symbols
    • H04L27/2679Decision-aided

Definitions

  • the invention relates to broadband transmission of information. More specifically, the invention relates to time synchronization of a received OFDM signal with a reference.
  • Orthogonal Frequency Division Multiplexing is a spread spectrum technology wherein the available bandwidth is subdivided into a number of discrete channels or subcarriers that are overlapping and orthogonal to each other. Each channel has a well defined frequency. Data are transmitted in the form of symbols that encompass the subcarrier frequencies. The amplitude and/or phase of the subcarriers represents the encoded information. Before a received OFDM symbol can be decoded, frequency and time synchronization of the signal have to be determined. This process is referred to as synchronization.
  • Frequency synchronization In OFDM transmission across power lines, the frequencies are low and crystals that provide good frequency control and stability are readily available. Frequency synchronization, however, may become more difficult at higher frequencies, e.g., in radio transmission.
  • Time synchronization of the received OFDM signals is more difficult to achieve, in particular in the presence of narrow band interference in the OFDM channels.
  • OFDM signals are typically synchronized using a time domain correlator, i.e. a correlator operating in the time domain.
  • An OFDM transmitter and a corresponding OFDM receiver typically operate at identical and stable subcarrier frequencies, but the clock cycle defining the symbol times in the transmitter and receiver may be offset with respect to each other by a certain symbol time offset. Time synchronization between the transmitter and receiver clock cycles is accomplished by determining this offset.
  • the receiver monitors the OFDM transmission channels for a predetermined synchronization symbol. Once the offset is established, all subsequently received symbols are shifted by the amount of the so determined offset and thereby aligned.
  • the time domain correlator computes cross- correlation values between a stored temporal symbol pattern and a received temporal symbol by shifting the stored symbol pattern in small time steps relative to the received symbol until a maximum correlation value is found.
  • the subsequently received OFDM symbols are then shifted in time by the total time shift that produced the initial alignment between the received symbol and the stored or reference symbol.
  • This method requires computation of a large number of digitized values of the received symbol.
  • Correlation is also difficult to establish if the received signal is corrupted by narrowband interference.
  • a received symbol is incrementally time-shifted in small time steps over the time duration of the reference symbol.
  • the received symbol is Fourier-transformed (FFT) into the frequency domain.
  • FFT Fourier-transformed
  • a cross-correlation is carried out in the frequency domain, wherein a correlation maximum is obtained when the FFT operation is performed at exactly the correct time shift.
  • the invention features a frequency domain synchronization, in which the phases of the subcarriers are displaced relative to the phases of a reference until correlation is achieved, and temporal alignment is determined from the amount of phase displacement required to achieve correlation.
  • the invention features determining phases of a first received symbol for the orthogonal transmission channels; comparing the phases of the first symbol with phases of a reference to determine a correlation between the phases of the first symbol and the phases of the reference; displacing the phases of the first symbol relative to the phases of the reference by a phase displacement and repeating the comparing; choosing a phase displacement based on the correlation between the phases of the first symbol and the phases of the reference; and determining the temporal alignment from the chosen phase displacement.
  • Embodiments of the invention may include one or more of the following features.
  • the predetermined phase shift may depend on the frequency of the transmission channel and may preferably be proportional to the frequency of the transmission channel.
  • the phases of the reference may be stored in a memory.
  • the reference may be a symbol that was received prior to receiving the first symbol. Transmission channels which exhibit temporal variations exceeding a predefined fluctuation value may be excluded from the phase comparison.
  • the correlation result may be formed by computing absolute differences between the phases of the first symbol and the reference for the orthogonal channels and adding the absolute differences to obtain an error signal.
  • the temporal alignment computed for the first symbol may be used to synchronize at least one symbol following the first symbol.
  • the chosen phase displacement may be that which maximizes the correlation between the phases of the first symbol and the phases of the reference.
  • the received phases may be computed by applying a window function.
  • the window function may be a rectangular window or an apodizing window function, such as a Gaussian, Hanning, Hamming, Blackman and Kaiser-Bessel window.
  • the window function may be applied to the first symbol either before or after the spectral content of the first symbol is determined.
  • FIG. 1 is a temporal OFDM symbol
  • FIG. 2 illustrates symbolically a frequency distribution of OFDM channels
  • FIG. 3 is a sequence of OFDM symbols with superimposed random noise
  • FIG. 4 is the OFDM symbol sequence of FIG. 3 with a superimposed jammer
  • FIG. 5 is the output signal of a time domain correlator of the symbol sequence of FIG. 3;
  • FIGS. 6 and 7 are output signals of the time domain correlator of the symbol sequence of FIG. 4 at different jammer signal levels
  • FIG. 8 is the output signal of the phase correlator of the invention with the symbol sequence of FIG. 3 and a rectangular window;
  • FIGS. 9 is the output signal of the phase correlator of the invention with the symbol sequence of FIG. 4 and a rectangular window;
  • FIGS. 10 is the Fourier transform of the OFDM waveform of FIG. 4 with a rectangular window
  • FIGS. 11 is the Fourier transform of the OFDM waveform of FIG. 4 with a
  • FIGS. 12 and 13 are correlation and autocorrelation peaks of the phase correlator of the invention with the symbol sequence of FIG. 4 and a Hanning window;
  • FIGS. 14 is a schematic diagram of the phase correlator module of the invention.
  • FIG. 15 is a block diagram of the phase correlator circuit of FIG. 14.
  • FIGS. 16 A and 16B is a flowchart of the phase correlation process.
  • Each symbol has a predetermined time duration or symbol time T s .
  • Each symbol is comprised of N sinusoidal waveforms that are orthogonal to each other and form the OFDM channels or subcarriers.
  • Each subcarrier has a frequency fj and a phase ⁇ , measured from the beginning of the symbol.
  • Orthogonality of the subcarriers requires that a whole number of periods of each waveform are contained within the symbol time T s .
  • the phases ⁇ j of the waveforms can be set arbitrarily without affecting the orthogonality of the waveforms.
  • the OFDM subcarriers occupy a frequency range between frequencies fi and fN referred to as OFDM bandwidth.
  • Each subcarrier frequency fj has a uniform frequency spacing ⁇ f from the adjacent subcarrier frequency f, ⁇ ] .
  • ⁇ f is inversely proportional to the symbol time T s .
  • the amplitude Aj, i.e., the signal power, in each channel is selected to be uniform.
  • the phases of the 84 subcarriers are selected to be random and independent of each other. However, any other set of phases may be selected without affecting the scope of the invention.
  • the symbol is sampled during the symbol time T s at 256 sample points at a clock rate of 40 MHz.
  • the unmodulated amplitudes Aj of each of the 84 OFDM channels are identical.
  • OFDM channels may experience interference noise.
  • noise can arise from two sources: Random noise wherein the noise energy is randomly distributed in both the time and frequency domain; and narrowband noise generated, for example, by a jammer emitting a narrowband signal at one or several frequencies that are localized within the frequency range of the OFDM channels.
  • the first symbol 32 is a "dummy" symbol having a zero signal amplitude.
  • the first symbol 32 is followed by waveform 34 including four consecutive symbols 10 of FIG. 1.
  • the fifth symbol 36 has also the form of symbol 10, except that the phases of all subcarriers are inverted.
  • the last symbol 38 is another "dummy" symbol with zero signal amplitude.
  • the jammer- to-signal amplitude ratio is 31.7 dB, i.e., the jammer amplitude is 500 times stronger than the signal amplitude in each of the N OFDM channels.
  • the jammer completely masks the OFDM symbols 34, 36 of waveform 30.
  • symbol data may be extracted from received OFDM waveforms having superimposed noise with a conventional time-based correlator, if the signal-to noise ratio exceeds a certain value. This is particularly true for random noise.
  • a correlator operating in the time domain performs a correlation between two symbols.
  • Correlation can, for example, be established between the OFDM symbol 10 and a predetermined reference symbol stored in a memory.
  • correlation can be established between a received OFDM symbol 10 and another OFDM symbol 10 received at an earlier time.
  • the correlator multiplies the sample points, if necessary after adjusting their amplitude, with 256 corresponding reference sample points that may be stored in a memory of the time domain correlator.
  • the sample is then successively time- shifted by a time shift corresponding to the time difference between two or more sample points and another correlation is computed.
  • the correlator produces a peak output value when the symbol is temporally aligned with the reference.
  • a time domain correlator correlates the waveform 30 with a reference corresponding to symbol 10.
  • the waveform 30 includes superimposed random noise with a signal-to-noise ratio of 4.1 dB.
  • the output signal 50 of the time domain correlator exhibits five distinct correlation peaks 52, 54 located at the sample points 256, 512, 768, 1024 and 1280, respectively. Note that the correlation peak 54 is inverted with respect to the four preceding correlation peaks 52 because the phase of the fifth symbol 36 is inverted relative to the phase of the preceding symbols 34.
  • the correlation peaks coincide with the beginning of sampling period which indicates that the symbols 34 are temporally aligned with the reference 10.
  • the jammer waveform 40 of FIG. 4 is applied to the signal input of the time domain correlator which then performs the same correlation as in FIG. 5.
  • the jammer- to-signal amplitude ratio is 23.77 dB.
  • the time domain correlator output signal 60 exhibits a peak 62 at sample point 768 and another peak 64 at sample point 1280. None of the other expected peaks are discernable.
  • the peaks 62, 64 may not be reliable since none of the other expected peaks are discernable.
  • no correlation peaks are visible when the jammer-to-signal amplitude ratio increases to 31.73 dB.
  • a time domain correlator may therefore not be able to reliably synchronize OFDM symbols even at moderate jammer signal levels.
  • the received OFDM symbols can still be synchronized in the presence of much stronger jammer by correlation in the frequency domain.
  • a temporal shift between two symbols corresponds to a phase shift of the OFDM subcarriers.
  • the phase shifts are typically proportional to the subcarrier frequencies (modulo 2 ⁇ ). Consequently, instead of synchronizing the OFDM symbols in the time domain, the OFDM symbols can be synchronized in the frequency domain by correlating the phases of the subcarriers with the phases of a reference symbol. Alternatively or in addition, autocorrelation can be performed by correlating the phases of a received symbol with those of an earlier received symbol.
  • Phase correlation has several advantages: it is more robust than time domain correlation since it is significantly less affected by amplitude variations; phase correlation may also require less computations and less complex hardware.
  • the temporal waveform S, n is received by phase correlator module 150.
  • the waveform S, n is filtered by a window filter 152 which can be placed either before a FFT module 153, as illustrated in FIG. 14, or after the FFT module 153 (not shown).
  • the FFT module 153 then transforms the filtered waveform to extract the information encoded on the OFDM subcarriers.
  • Window filter 152 operates on the temporal waveform and multiplies the received waveform S, n preferably with an apodizing filter function, e.g., a Hanning window.
  • a window filter placed after the FFT module 153 operates on the OFDM subcarriers in the frequency domain.
  • a convolution in the frequency domain is equivalent to multiplication in the time domain.
  • convolution is more computationally intensive than multiplication, and so time domain multiplication is employed.
  • time domain multiplication is employed.
  • the "windowed" amplitude in the frequency domain can be obtained by relatively simple convolution computation.
  • an accurate approximation can be achieved by subtracting for each subcarrier f, one half of the sum of the amplitudes at the two adjacent carriers, i.e., Vi (f, + ⁇ + f, +2 ).
  • Converter 154 converts the Fourier-transformed (FFT) data to polar coordinates representing the amplitudes A, and the phases ⁇ , of the received symbol at the N subcarrier frequencies fi, ... , f ⁇
  • the phases ⁇ may be stored in memory 155 for computing autocorrelation values for comparison with a symbol received at a later time.
  • phase correlator 157 For computing phase correlation between a received symbol and a reference, phase correlator 157 compares the phases ⁇ , of the received symbol with known reference phases ⁇ , ref that are stored in memory 156. Phase correlator 157 adds the absolute values of the difference between the phases ⁇ , and ⁇ , ref at the frequencies f, to produce a sum ⁇
  • are computed for each increment in the phase shifts and stored in a memory 169 (FIG. 15). The respective sum ⁇
  • a second converter 158 computes from the sum ⁇
  • phase correlator compares the phases ⁇ , of the received symbol with the phases ⁇ , prec of the preceding symbol that are stored in memory 155, and computes the respective sum ⁇
  • phase correlation in the frequency domain with a rectangular window is still superior to conventional time domain correlation.
  • a rectangular window is applied before the FFT unit 153.
  • each temporal sample point of input waveform Sj n is multiplied with the respective value of the window function at the sample point.
  • the window function R(t) of the rectangular window can be written as:
  • the received waveform 30 (i.e., the received signal contains only superimposed random noise) is "processed", i.e., filtered, with the rectangular window of Eq. (1).
  • the phase correlator circuit 160 distinctly resolves the five correlation peaks 82, 84 and their temporal position corresponds exactly to that of the correlation peaks 52, 54 obtained with the time domain correlator of FIG. 5. This result demonstrates that the phase correlator performs at least as well as the time domain correlator in the presence of random noise.
  • the input waveform 40 (the received signal contains both the random noise and the jammer with a jammer-to-signal amplitude ratio of 27.3 dB) is processed with the rectangular window of Eq. (1).
  • the output 90 of the phase correlator of the invention resolves five correlation peaks 92, 94. Although the peaks are significantly weaker than those of FIG. 8, correlation can still be established. This result compares favorably with the correlation signal of FIG. 6 obtained with the time domain correlator which showed essentially no correlation at a significantly lower jammer power of 23.8 dB. Correlation with the phase correlator of the invention can be improved even further by replacing the rectangular window with an apodizing function, or apodizing window.
  • FIGS. 10 and 11 show the benefit provided by an apodizing function over best be understood with reference to the Fourier-transforms of signal waveform 40.
  • processing the signal waveform 40 with the rectangular window of Eq. (1) produces a broad peak 102.
  • the interfering jammer signal extends to both sides 104, 106 of the jammer's center frequency f j , affecting a large percentage of the OFDM subcarriers.
  • the affected OFDM subcarriers may have to be excluded from the phase correlation for improved performance and also from the OFDM bandwidth.
  • the Hanning window and depending on the jammer- to-signal amplitude ratio the jammer essentially affects only a limited number of subcarriers having frequencies adjacent to the jammer frequency fj.
  • the jammer amplitude at the more distant frequencies is reduced by more than 26 dB from its peak amplitude 112.
  • the Hanning window most OFDM channels, with exception of the small number of channels immediately adjacent to the jammer frequency, are clearly resolved.
  • processing the signal waveform 40 with the Hanning window confines interference from the jammer to only several of the OFDM channels.
  • the phase correlator employing the Hanning window therefore provides significantly improved resolution and performance over the embodiment using the rectangular window, as will now be discussed.
  • an "apodizing" function i.e., a function that has smoother “edges” than the rectangular window
  • window filter 152 FIG. 14
  • Apodizing functions of this type are commonly employed in signal processing applications; examples are Hanning, Hamming and Blackman and Kaiser-Bessel windows.
  • a Hanning window can be represented by the following function:
  • n is the n th sample point out of a total of ⁇ sample point of the sampled received temporal waveform.
  • a Hamming window can be written as:
  • the input waveform 40 with a jammer-to-signal amplitude ratio of 27.3 dB is processed in window filter 152 with the Hanning window of Eq. (2).
  • Phase correlator 157 clearly resolves five correlation peaks 122, 124, 126.
  • a comparison between the peak signal amplitudes 122, 124, 126 obtained with the Hanning window and the amplitudes 92, 94 (FIG. 9) obtained with the rectangular window demonstrates the advantages of using an apodizing filter function.
  • a time domain correlator did not produce reliable correlation at all (FIG. 6).
  • the input waveform 40 with a jammer-to-signal amplitude ratio of 31.3 dB is processed in window filter 152 with the Hanning window of Eq. (2).
  • the output peaks 132, 134, 136 in both correlation and autocorrelation are resolved, albeit with a smaller signal-to-noise ratio than that of the peaks of FIG. 12.
  • FIGS. 12 and 13 connect the autocorrelation peak signal values.
  • Autocorrelation represents correlation between a signal and the immediately preceding signal. No autocorrelation peak is observed at peak positions 122 of FIG. 12 and 132 of FIG. 13 since the first symbol 32 (FIG. 3) is a "dummy" symbol with zero amplitude.
  • the autocorrelation peaks of FIG. 12 are actually stronger than the correlation peaks with the reference signal.
  • One explanation for this result is that two received symbols are likely to contain the same artifacts caused, e.g., by inter-symbol interference, and therefore correlate better with each other than with the reference that does not contain those artifacts.
  • the presence of symbols on OFDM transmission channels may first be established by autocorrelation. Only after the symbols have been found, are the symbols synchronized relative to the reference.
  • apodizing window function such as the Hamming, Blackman and Kaiser-Bessel windows (not shown), produce phase correlator output peaks that are essentially identical to those obtained with the Hanning window.
  • phase correlator module 150 includes an window filter 152 and a FFT module 153 to transform the temporal symbol waveform into the frequency domain.
  • First converter 154 converts the output of the FFT module 153 to respective amplitude values A and phase values ⁇ j at each of the OFDM subcarrier frequencies f.
  • Phase correlator 157 compares the phases ⁇ j to known reference phases ⁇ j ref that may be stored in a memory 156, or to the phases ⁇ j of a symbol that was received earlier. The phases ⁇ , of the earlier received symbol may be stored in a memory
  • Phase correlator 157 then either compares the phases to produce an autocorrelation value or aligns the phases with the reference phases, as discussed above.
  • a corresponding time shift ⁇ T S which represents the temporal shift between the received symbols and the reference, is computed from the aligned phases and used for synchronization.
  • the phase correlator 157 includes a subtractor 162 that receives from the first converter 154 a respective symbol phase ⁇ ,.
  • Each subtractor 156 also receives a respective reference phase ⁇ , ref stored in memory 165.
  • a second input of the multiplexer 164 receives from memory device 156 respective phase shift constants ⁇ , that may be different for each subcarrier i.
  • the multiplexer 164 transfers either ⁇ , or ⁇ , to a respective adder 165.
  • Absolute value circuit 167 computes the absolute value
  • Adder 168 adds the output values produced by the N absolute value circuits 167 to form a first correlation value Ci which is stored in a first output register 169.
  • select line SEL enables each multiplexer 164 to transfer a respective phase shift constant ⁇ , to each of the adders 165 which then adds the respective phase shift constant ⁇ , to the previous (old) difference value ⁇ , old stored in register 166 to form a new difference value ⁇ , new .
  • Additions are always modulo(2 ⁇ ), with the result between - ⁇ and + ⁇ .
  • Absolute value circuit 167 then computes new absolute values
  • this process also repeats 256 times until the total phase shift ⁇ ( ⁇ ,) produced by adding the phase shift constants ⁇ , spans the symbol time T s .
  • the maximum (or minimum) value of all correlation values d, C 2 , ..., C max is determined and used to compute the time shift ⁇ T S between the symbol and the reference for synchronization.
  • the received symbol waveform is processed by applying a window function which can be a rectangular window or an apodizing window function, e.g., a Hanning window, step 212 and
  • the processed waveform is then Fourier-transformed, step 214.
  • the window function 212' can be applied following the Fourier transform 214'.
  • the frequency coordinates are converted to polar coordinates, step 216, to obtain the amplitudes A, and, more particularly, the phases ⁇ , of the symbol waveform at the OFDM subcarrier frequencies f,.
  • the phases ⁇ may be stored in a memory for subsequent autocorrelation of the received symbols, step 218.
  • phase shift constants ⁇ at each subcarrier frequency f, are fetched from memory, step 226.
  • the difference ⁇ , ⁇ , rei - ⁇ , is computed at the frequencies f household step 230.
  • are computed, step 232, and summed over all frequencies to form sum ⁇
  • is stored as a correlator output value in the next available output memory location, step 234.
  • a predetermined frequency-dependent phase shift ⁇ , is then added to each difference ⁇ , to form a new phase differences ⁇ , ⁇ ew ⁇ , old + ⁇ impart step 236.
  • step 2308 If the accumulated phase shift, i.e., the sum ⁇ ( ⁇ ,), corresponds to a time shift that is essentially equal to the the symbol time T s , step 238, then the process determines a largest or smallest value of the values stored in the memory locations 169 (FIG. 15) and computes a corresponding time shift ⁇ T S of the symbol relative to reference to synchronize the received symbols, step 244. If the accumulated phase shift is less than the symbol time T s , then the process returns from step 238 to step 230 and new differences
  • phase correlator 157 advantageously performs only additions and can readily be implemented in hardware with a reasonable number of gates, with the number depending on the number of subcarriers and waveform sample points.
  • phase correlator does not require expensive hardware and is extremely fast and it shares the same FFT processor implemented for OFDM modulation and demodulation.
  • the number of computations is proportional to the number of subcarrier frequencies.
  • the computation of the phase angles is also independent of the amplitudes Aj so that phase correlation can be performed before automatic gain control (AGC).
  • AGC automatic gain control

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  • Engineering & Computer Science (AREA)
  • Computer Networks & Wireless Communication (AREA)
  • Signal Processing (AREA)
  • Synchronisation In Digital Transmission Systems (AREA)
  • Mobile Radio Communication Systems (AREA)
PCT/US2000/001399 1999-01-20 2000-01-20 Synchronization of ofdm signals Ceased WO2000044120A1 (en)

Priority Applications (6)

Application Number Priority Date Filing Date Title
JP2000595449A JP4751986B2 (ja) 1999-01-20 2000-01-20 Ofdm信号の同期化
EP00909936A EP1145470B1 (en) 1999-01-20 2000-01-20 Synchronization of ofdm signals
AT00909936T ATE487295T1 (de) 1999-01-20 2000-01-20 Synchronisation von ofdm signalen
AU32113/00A AU3211300A (en) 1999-01-20 2000-01-20 Synchronization of ofdm signals
CA002358931A CA2358931C (en) 1999-01-20 2000-01-20 Synchronization of ofdm signals
DE60045186T DE60045186D1 (de) 1999-01-20 2000-01-20 Synchronisation von ofdm signalen

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US09/234,289 1999-01-20
US09/234,289 US6111919A (en) 1999-01-20 1999-01-20 Synchronization of OFDM signals

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WO2000044120A1 true WO2000044120A1 (en) 2000-07-27
WO2000044120A8 WO2000044120A8 (en) 2001-06-21

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US (1) US6111919A (enExample)
EP (1) EP1145470B1 (enExample)
JP (1) JP4751986B2 (enExample)
AT (1) ATE487295T1 (enExample)
AU (1) AU3211300A (enExample)
CA (1) CA2358931C (enExample)
DE (1) DE60045186D1 (enExample)
WO (1) WO2000044120A1 (enExample)

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ATE487295T1 (de) 2010-11-15
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