US5258228A - Infrared slight energy radiation powder and synthetic fiber containing said radiation powder mixed therein and fiber articles comprising said fiber - Google Patents

Infrared slight energy radiation powder and synthetic fiber containing said radiation powder mixed therein and fiber articles comprising said fiber Download PDF

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Publication number
US5258228A
US5258228A US07/507,532 US50753290A US5258228A US 5258228 A US5258228 A US 5258228A US 50753290 A US50753290 A US 50753290A US 5258228 A US5258228 A US 5258228A
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infrared
fiber
radiation powder
slight energy
energy radiation
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US07/507,532
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English (en)
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Toshio Komuro
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K5/00—Heat-transfer, heat-exchange or heat-storage materials, e.g. refrigerants; Materials for the production of heat or cold by chemical reactions other than by combustion
    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F1/00—General methods for the manufacture of artificial filaments or the like
    • D01F1/02—Addition of substances to the spinning solution or to the melt
    • D01F1/10—Other agents for modifying properties
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2913—Rod, strand, filament or fiber
    • Y10T428/2918—Rod, strand, filament or fiber including free carbon or carbide or therewith [not as steel]
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2982—Particulate matter [e.g., sphere, flake, etc.]

Definitions

  • This invention relates to infrared slight energy radiation powder and synthetic fiber containing the radiation powder mixed therein and fiber articles comprising the synthetic fiber.
  • fiber articles in relation with the present invention is defined as to mean wide concept including garments such as clothes, underwear and socks; fabric apparel accessories such as handkerchieves and towels; bedding such as quilts and blankets; and wrapping articles.
  • Ceramics has been known as "functional material” which radiates infrared slight energy (referred often to far-infrared radiation). There has been a common understanding that ceramics acts on the object to change some physical property in radiating infrared slight energy. However, it still has not been apparent what kind of physical property can be changed in what kind of material of the object. Also, preferable components of ceramics as "functional material” has been unknown.
  • the infrared slight energy radiation in general heats the object directly with radiation heat like a solar beam without heating gas or liquid in between and the infrared slight energy radiation penetrates into inner part of the object like microwave heating used for a microwave oven without heating excessively the surface of the object. Therefore, the infrared slight energy radiation has been used mainly for heaters such as a stove, a cooking stove and a kotatsu, namely, a low, covered table with a heat source underneath.
  • the infrared slight energy radiation has also been utilized in a traditional method of cooking for sweet potatoes baked in pebbles. The potatoes are baked comfortably warm by the infrared slight energy radiation from the heated pebbles.
  • the infrared slight energy radiation has been known as useful for the heaters, however, it has become clear that the infrared slight energy radiation particularly serves for food maturity, food freshness-keeping, taste improvement, atmosphere ionizing and the like. The mechanism is not fully explained, however, the infrared slight energy is proved to be effective in food and living use besides the industrial use through the experiments conducted by the inventor of the present invention.
  • the development in other types of radiation power has been expected which would be able to radiate no less effective infrared slight energy than that of the previous invention.
  • the development in the effective use of the radiation powder has also been expected to be proposed.
  • this invention discloses substituting titanium for silica in the previous invention. Also, this invention discloses substituting palladium for platinum in the previous invention. Precisely, the feature of this invention is to provide infrared slight energy radiation powder comprising alumina and titanium with platinum or palladium added as additives, or, to provide infrared slight energy radiation powder comprising alumina and silica with palladium added as additives. Silica and titanium in this invention are both essential substances that without silica or titanium, the principal purpose of providing sufficient quantities of infrared slight energy radiation can not be achieved. This invention also discloses synthetic fiber containing the radiation powder dispersedly mixed therein.
  • the radiation powder comprising in accordance with the above-described components having fabricated into other forms or shapes for adapting to the objects provides high energy ratio in the wavelength range (more than wavelength 4 ⁇ m) and satisfactory radiant quantities both in relatively low temperature region (less than 700° K.) and in relatively high temperature region (700° ⁇ 1300° K.). Generally, with the coverage of 3 ⁇ 12 ⁇ m wavelength, the radiation powder is applicable to various purposes of use.
  • the radiation powder In applying the radiation powder into synthetic fiber, for example, nylon, in dispersed condition, infrared slight energy is radiated from whole of the fabric.
  • synthetic fiber for example, nylon
  • stockings or underwear made of the fiber are so warm that they have curative effects for cold-blooded nature and arthalgia caused by the cold.
  • Another meritorious purpose of the radiation powder is utilizing for wrapping articles which are effective for the wrapped food in maturity, keeping for a long time and freshness-retaining.
  • FIG. 1 is a graph of energy radiant quantities versus wavelength showing radiation features of infrared slight energy in relatively low temperature region radiated from a sheet made of the radiation powder in accordance with an example of this invention
  • FIG. 2 is a graph corresponding to FIG. 1 in relatively high temperature region
  • FIG. 3 is a graph showing a comparison between the size of a water molecular cluster of water having infrared slight energy radiation and without having the radiation.
  • the present invention is to provide the infrared slight energy radiation powder, an example of which comprises chiefly alumina and titanium with platinum added as additives.
  • a grain size being less than 1 ⁇ is mixed with 55 ⁇ 70 wt % of powdered titanium, a grain size of which may be similar to that of alumina.
  • colloidal platinum a grain size of which is roughly 7 ⁇ 40 ⁇ is added to serve for oxygen and hydrogen absorption, namely, colloid activation.
  • silicon nitride a grain size being less than 0.34 ⁇ may be added to the basic constituent described above. Silicon nitride activates hydrogen in regulating hydrogen ion migration to a determined direction. Addition of 2.3 wt % of silicon nitride is preferable.
  • the radiation powder can be in a state of powder, or fabricated into a high molecular pellet or a sheet.
  • the radiation powder in relation with the example is mixed into synthetic fiber such as nylon, vinylon, ester, acrylic and urethane in dispersed condition.
  • synthetic fiber such as nylon, vinylon, ester, acrylic and urethane in dispersed condition.
  • the following fiber articles are made of the synthetic fiber.
  • the infrared slight energy radiation from the fiber composing panty hoses or underwear penetrates into human body to improve the circulation of the blood so that those clothes are warm and retain heat.
  • the fabric is not necessarily made of 100% fiber in relation with this invention but the desired effects can be obtained by the fabric mixed-span with ordinary fiber.
  • the fiber containing the radiation powder dispersedly mixed in it may be used for the specific parts of the body, such as knees and elbows to obtain curative effects for cold-blooded nature or arthralgia caused by the cold.
  • the fiber contributes to the health in a way that the infrared slight energy from the fiber absorbed deeply into the body activates water molecules in the cells.
  • the activated water molecules further activate the cells of the body to function for metabolism in discharging egesta in the cells.
  • Improved circulation of the blood and body fluid carrying oxygen and nutrition to all over the body results in healthy condition of the cells.
  • the bedding such as quilts, blankets and pillows made of the fiber in relation with the present invention not only retains heat and improves the circulation of the blood but also deodorizes and keeps soft and dry feeling due to the infrared slight energy radiation from itself.
  • the examination has been carried out on the temperature distribution of the three cases, a quilt made of the fiber in relation with the present invention, a feather quilt and a woolen quilt, in 30 minutes after start using.
  • the quilt made of the fiber in relation with the present invention has shown better results than the feather quilt or the woolen quilt which are substantially heat-retaining.
  • Non woven fabric for wrapping articles is made of the fiber mixedly containing the radiation powder in relation with the present invention.
  • the wrapping articles considerably keep freshness of the wrapped perishable food. That is, the fresh meat and fish comprises more than 70% water, so that the water molecules of which are activated, as a matter of course the cells of the meat and the fish are kept in a fresh condition.
  • the infrared slight energy radiation from the fiber resonants with the water molecules in the cells of the meat or fish. Consequently, the water molecule cluster including hydrogen ion and hydroxide ion is reduced in size fastening the ionic bonds to improve oxygen activation in the cells and to decrease water liberation from the surface of the meat and fish for effecting inhibition of aerobic bacteria propagation and browning of the food.
  • FIG. 3 shows the comparison made by NMR spectrum (nuclear magnetic resonance spectrum) in the size of water molecule clusters between water content of a fish wrapped in a wrapping article made of non woven fabric in relation with this invention and water content of a fish wrapped in a wrapping article made of the conventional non woven fabric. It has been apparent from the result that A showing the size of a water molecule cluster of water having infrared slight energy radiation is smaller than B showing the same without having infrared slight energy radiation. This shows that the water molecule cluster has been broken to be smaller by the human action of radiating infrared slight energy. Reduction of the water molecule cluster in size means that activated water molecules function as to re-include dissolved oxygen in the cluster, changing the structure of water, which results in inhibition of bacteria propagation.
  • the infrared slight energy radiation powder in relation with the present invention is preferable as a material functioning for radiating infrared slight energy.
  • the radiation powder can be in a state of powder or fabricated into a pellet, a sheet or in any shapes in response to the form, construction or material of the object.
  • the radiation powder has a various use in prospect as it can provide sufficient quantities of infrared slight energy radiation having wide wavelength range.
  • the synthetic fiber with the radiation powder mixed therein is preferable for clothes and bedding because of the effectiveness of infrared slight energy radiation from the fiber for heat-retaining and improving the health. Wrapping articles made by the synthetic fiber in relation with this invention keep freshness of the wrapped food and have antibacterial effects.

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  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Manufacturing & Machinery (AREA)
  • General Chemical & Material Sciences (AREA)
  • Textile Engineering (AREA)
  • Physics & Mathematics (AREA)
  • Combustion & Propulsion (AREA)
  • Thermal Sciences (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Artificial Filaments (AREA)
  • Chemical Or Physical Treatment Of Fibers (AREA)
  • Multicomponent Fibers (AREA)
  • Radiation-Therapy Devices (AREA)
US07/507,532 1989-12-20 1990-04-11 Infrared slight energy radiation powder and synthetic fiber containing said radiation powder mixed therein and fiber articles comprising said fiber Expired - Lifetime US5258228A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP1-328396 1989-12-20
JP1328396A JPH03190990A (ja) 1989-12-20 1989-12-20 赤外線微弱エネルギー放射用の粉末及びそれを混入した合成繊維

Publications (1)

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US5258228A true US5258228A (en) 1993-11-02

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US (1) US5258228A (cs)
EP (1) EP0462275B1 (cs)
JP (1) JPH03190990A (cs)
KR (1) KR960000473B1 (cs)
AT (1) ATE126822T1 (cs)
AU (1) AU5173590A (cs)
CA (1) CA2046875C (cs)
DE (1) DE69021874T2 (cs)
ES (1) ES2075896T3 (cs)
HK (1) HK74496A (cs)
WO (1) WO1991009088A1 (cs)

Cited By (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5779950A (en) * 1996-12-02 1998-07-14 Kang; Dong Soon Method of making a synthetic fiber containing infrared energy powder
US20040202899A1 (en) * 2002-06-05 2004-10-14 Toshio Komuro Antithrombogenic platiniferous ceramic composition and article containing the same
US20040213995A1 (en) * 2000-07-04 2004-10-28 Yoshihiro Hirata Healthy fiber products
US20040225049A1 (en) * 2000-05-19 2004-11-11 Toshio Komuro Composition for far infrared irradiation with excellent antistatic property and fiber and textile product both containing the same
US20050109158A1 (en) * 2003-11-25 2005-05-26 The Boeing Company Method for preparing ultra-fine, submicron grain titanium and titanium-alloy articles and articles prepared thereby
US20080134406A1 (en) * 2006-12-06 2008-06-12 Su-Huei Shih Health care fitness underwear
US20080312066A1 (en) * 2007-06-12 2008-12-18 Min-Chu Lin Message energy memory ceramics
US20090280107A1 (en) * 1997-10-23 2009-11-12 Nelsestuen Gary L Modified vitamin k-dependent polypeptides
WO2013170543A1 (zh) * 2012-05-14 2013-11-21 Mao Yingjun 一种升温蓄热的纤维及其制备方法和纺织品
USD766597S1 (en) 2014-06-27 2016-09-20 Multiple Energies Technologies Llc Apparel with bioceramic surface ornamentation
US9476146B2 (en) 2014-09-11 2016-10-25 Clopay Plastic Products Company, Inc. Polymeric materials providing improved infrared emissivity
US9833509B2 (en) 2014-05-05 2017-12-05 Multiple Energy Technologies Llc Bioceramic compositions and biomodulatory uses thereof
US10252945B2 (en) 2012-09-26 2019-04-09 Multiple Energy Technologies Llc Bioceramic compositions

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JP2585167B2 (ja) * 1992-07-16 1997-02-26 スワニー株式会社 金属を含有した繊維からなる肌着
JP2585166B2 (ja) * 1992-07-16 1997-02-26 スワニー株式会社 金属を含有した繊維からなる靴下
KR0155608B1 (ko) * 1995-07-14 1998-12-01 박홍기 원적외선 방사성 폴리에스테르 섬유의 제조방법
CN1049941C (zh) * 1996-12-10 2000-03-01 珠海经济特区天年高科技国际企业公司 含有无机氧化物复合粉体的医用无纺布
FR2763965B1 (fr) * 1997-05-28 1999-07-30 Seok Mi Soo Produit fibreux a base d'elvan
US7074499B2 (en) 2002-03-22 2006-07-11 Holofiber, Llc Polymeric fiber composition and method
JP4489439B2 (ja) * 2002-03-22 2010-06-23 ホロファイバー エルエルシー ポリマー繊維組成物および方法
KR100734310B1 (ko) 2006-02-03 2007-07-02 삼성전자주식회사 영상 신호 처리 장치의 동기 검출기 및 그 동기 검출기를포함하는 동기 선택 장치
CA2712513A1 (en) * 2007-01-31 2008-08-07 Innovision Headwear Inc. Optically active headgear
DK2072666T3 (da) 2007-09-28 2012-03-05 Venex Co Ltd Fiber indeholdende nanodimensioneret diamant og platinnanokolloid og sengetøjsprodukt omfattende fiberen
JP5467700B2 (ja) * 2010-12-24 2014-04-09 株式会社バイオフェイス東京研究所 プラチナシールド技術を用いた家電製品
ES2492215B1 (es) 2013-02-06 2015-06-29 Jesús CANDEL FABREGAS Polvo cerámico fotocatalítico y de emisión infrarroja, aplicable a fibras textiles y procedimiento de obtención de dicho polvo
JP7121949B2 (ja) * 2018-11-19 2022-08-19 株式会社セラフト ナノプラチナ粒子含有樹脂繊維
JP7362955B1 (ja) * 2023-03-15 2023-10-17 俊夫 小室 焼成体
CN118407273B (zh) * 2024-07-01 2024-09-10 安徽同和晶体新材料股份有限公司 一种高纯氧化铝纤维纸的制备方法

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US3607343A (en) * 1965-10-04 1971-09-21 Metco Inc Flame spray powders and process with alumina having titanium dioxide bonded to the surface thereof
US3715265A (en) * 1969-09-03 1973-02-06 Mc Donnell Douglas Corp Composite thermal insulation
JPS5686952A (en) * 1979-12-18 1981-07-15 Mitsubishi Petrochem Co Ltd Insulating sheet for agriculture
US4377618A (en) * 1980-07-23 1983-03-22 Matsushita Electric Industrial Company, Limited Infrared radiator
US4686791A (en) * 1983-11-12 1987-08-18 Kyowa Chemical Industry Co., Ltd. Agricultural film structure
US4746638A (en) * 1985-09-27 1988-05-24 Kureha Chemical Industry Co., Ltd. Alumina-titania composite powder and process for preparing the same
JPS6424837A (en) * 1987-07-21 1989-01-26 Keiichi Yamamoto Elastic foam
US4999243A (en) * 1986-12-15 1991-03-12 Nobushige Maeda Far infra-red radiant composite fiber
US5032376A (en) * 1988-09-30 1991-07-16 Maschinenfabrik Andritz Actiengesellschaft Method for producing aluminum titanate

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JPS62184088A (ja) * 1986-02-07 1987-08-12 Zenzo Nakagiri 遠赤外線放射用の粉末
JPS6365951A (ja) * 1986-09-08 1988-03-24 Nippon Shokubai Kagaku Kogyo Co Ltd 燃焼用触媒体の製造方法
JPH064506B2 (ja) * 1987-05-06 1994-01-19 英男 太田 遠赤外線放射セラミックス
JPH0197254A (ja) * 1987-10-07 1989-04-14 Kanamori Kk 遠赤外線放射不織布シート・堅綿

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3607343A (en) * 1965-10-04 1971-09-21 Metco Inc Flame spray powders and process with alumina having titanium dioxide bonded to the surface thereof
US3715265A (en) * 1969-09-03 1973-02-06 Mc Donnell Douglas Corp Composite thermal insulation
JPS5686952A (en) * 1979-12-18 1981-07-15 Mitsubishi Petrochem Co Ltd Insulating sheet for agriculture
US4377618A (en) * 1980-07-23 1983-03-22 Matsushita Electric Industrial Company, Limited Infrared radiator
US4686791A (en) * 1983-11-12 1987-08-18 Kyowa Chemical Industry Co., Ltd. Agricultural film structure
US4746638A (en) * 1985-09-27 1988-05-24 Kureha Chemical Industry Co., Ltd. Alumina-titania composite powder and process for preparing the same
US4999243A (en) * 1986-12-15 1991-03-12 Nobushige Maeda Far infra-red radiant composite fiber
JPS6424837A (en) * 1987-07-21 1989-01-26 Keiichi Yamamoto Elastic foam
US5032376A (en) * 1988-09-30 1991-07-16 Maschinenfabrik Andritz Actiengesellschaft Method for producing aluminum titanate

Cited By (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5779950A (en) * 1996-12-02 1998-07-14 Kang; Dong Soon Method of making a synthetic fiber containing infrared energy powder
US20090280107A1 (en) * 1997-10-23 2009-11-12 Nelsestuen Gary L Modified vitamin k-dependent polypeptides
US20040225049A1 (en) * 2000-05-19 2004-11-11 Toshio Komuro Composition for far infrared irradiation with excellent antistatic property and fiber and textile product both containing the same
US7201945B2 (en) * 2000-07-04 2007-04-10 Phild Co., Ltd. Healthy fiber products
US20040213995A1 (en) * 2000-07-04 2004-10-28 Yoshihiro Hirata Healthy fiber products
US20060275348A1 (en) * 2002-06-05 2006-12-07 Toshio Komuro Method for preventing or treating thrombosis
US8104482B2 (en) 2002-06-05 2012-01-31 Toshio Komuro Method for treating a thrombosis
US20040202899A1 (en) * 2002-06-05 2004-10-14 Toshio Komuro Antithrombogenic platiniferous ceramic composition and article containing the same
US20050109158A1 (en) * 2003-11-25 2005-05-26 The Boeing Company Method for preparing ultra-fine, submicron grain titanium and titanium-alloy articles and articles prepared thereby
US7241328B2 (en) * 2003-11-25 2007-07-10 The Boeing Company Method for preparing ultra-fine, submicron grain titanium and titanium-alloy articles and articles prepared thereby
US20080089802A1 (en) * 2003-11-25 2008-04-17 Keener Steven G Method for preparing ultra-fine, submicron grain titanium and titanium-alloy articles and articles prepared thereby
US7785530B2 (en) 2003-11-25 2010-08-31 The Boeing Company Method for preparing ultra-fine, submicron grain titanium and titanium-alloy articles and articles prepared thereby
US20080134406A1 (en) * 2006-12-06 2008-06-12 Su-Huei Shih Health care fitness underwear
US20080312066A1 (en) * 2007-06-12 2008-12-18 Min-Chu Lin Message energy memory ceramics
US8182825B2 (en) * 2007-06-12 2012-05-22 Min-Chu Lin Message energy memory ceramics
WO2013170543A1 (zh) * 2012-05-14 2013-11-21 Mao Yingjun 一种升温蓄热的纤维及其制备方法和纺织品
US10252945B2 (en) 2012-09-26 2019-04-09 Multiple Energy Technologies Llc Bioceramic compositions
US12234191B2 (en) 2012-09-26 2025-02-25 Multiple Energy Technologies Llc Bioceramic compositions
US9833509B2 (en) 2014-05-05 2017-12-05 Multiple Energy Technologies Llc Bioceramic compositions and biomodulatory uses thereof
US9962441B2 (en) 2014-05-05 2018-05-08 Multiple Energy Technologies Llc Bioceramic compositions and biomodulatory uses thereof
USD766597S1 (en) 2014-06-27 2016-09-20 Multiple Energies Technologies Llc Apparel with bioceramic surface ornamentation
US9476146B2 (en) 2014-09-11 2016-10-25 Clopay Plastic Products Company, Inc. Polymeric materials providing improved infrared emissivity

Also Published As

Publication number Publication date
CA2046875A1 (en) 1991-06-21
DE69021874T2 (de) 1996-02-15
EP0462275B1 (en) 1995-08-23
EP0462275A4 (en) 1992-01-02
DE69021874D1 (de) 1995-09-28
KR960000473B1 (ko) 1996-01-08
KR910011696A (ko) 1991-08-07
AU5173590A (en) 1991-07-18
ATE126822T1 (de) 1995-09-15
CA2046875C (en) 2000-01-11
HK74496A (en) 1996-05-03
WO1991009088A1 (fr) 1991-06-27
ES2075896T3 (es) 1995-10-16
JPH03190990A (ja) 1991-08-20
EP0462275A1 (en) 1991-12-27
JPH0545637B2 (cs) 1993-07-09

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