TWI310397B - - Google Patents
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- TWI310397B TWI310397B TW92115283A TW92115283A TWI310397B TW I310397 B TWI310397 B TW I310397B TW 92115283 A TW92115283 A TW 92115283A TW 92115283 A TW92115283 A TW 92115283A TW I310397 B TWI310397 B TW I310397B
- Authority
- TW
- Taiwan
- Prior art keywords
- coated
- zinc oxide
- cerium oxide
- powder
- film
- Prior art date
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- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims description 377
- 229910000420 cerium oxide Inorganic materials 0.000 claims description 241
- BMMGVYCKOGBVEV-UHFFFAOYSA-N oxo(oxoceriooxy)cerium Chemical compound [Ce]=O.O=[Ce]=O BMMGVYCKOGBVEV-UHFFFAOYSA-N 0.000 claims description 241
- 239000011787 zinc oxide Substances 0.000 claims description 151
- 239000000203 mixture Substances 0.000 claims description 121
- 238000000034 method Methods 0.000 claims description 92
- 239000002245 particle Substances 0.000 claims description 85
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 69
- 229920000620 organic polymer Polymers 0.000 claims description 69
- 239000000843 powder Substances 0.000 claims description 53
- 239000010419 fine particle Substances 0.000 claims description 49
- -1 fatty acid salts Chemical class 0.000 claims description 48
- 230000001699 photocatalysis Effects 0.000 claims description 43
- DIOQZVSQGTUSAI-UHFFFAOYSA-N decane Chemical compound CCCCCCCCCC DIOQZVSQGTUSAI-UHFFFAOYSA-N 0.000 claims description 32
- 239000000835 fiber Substances 0.000 claims description 32
- 239000000047 product Substances 0.000 claims description 32
- 239000004408 titanium dioxide Substances 0.000 claims description 29
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 26
- 239000003795 chemical substances by application Substances 0.000 claims description 25
- 239000011362 coarse particle Substances 0.000 claims description 25
- 238000010521 absorption reaction Methods 0.000 claims description 24
- 229920005992 thermoplastic resin Polymers 0.000 claims description 22
- 238000000354 decomposition reaction Methods 0.000 claims description 20
- 239000011164 primary particle Substances 0.000 claims description 20
- 239000013078 crystal Substances 0.000 claims description 19
- WOCIAKWEIIZHES-UHFFFAOYSA-N ruthenium(iv) oxide Chemical compound O=[Ru]=O WOCIAKWEIIZHES-UHFFFAOYSA-N 0.000 claims description 18
- 239000006097 ultraviolet radiation absorber Substances 0.000 claims description 15
- 229910052751 metal Inorganic materials 0.000 claims description 13
- 239000002184 metal Substances 0.000 claims description 13
- 239000011521 glass Substances 0.000 claims description 12
- 238000007254 oxidation reaction Methods 0.000 claims description 12
- 238000000576 coating method Methods 0.000 claims description 10
- 239000000049 pigment Substances 0.000 claims description 10
- 238000000862 absorption spectrum Methods 0.000 claims description 9
- 239000011248 coating agent Substances 0.000 claims description 9
- 239000000463 material Substances 0.000 claims description 9
- 229910044991 metal oxide Inorganic materials 0.000 claims description 9
- 150000004706 metal oxides Chemical class 0.000 claims description 9
- 239000003921 oil Substances 0.000 claims description 9
- 239000004698 Polyethylene Substances 0.000 claims description 8
- 238000000465 moulding Methods 0.000 claims description 8
- 229920000573 polyethylene Polymers 0.000 claims description 8
- 239000004576 sand Substances 0.000 claims description 8
- 239000000377 silicon dioxide Substances 0.000 claims description 8
- 239000002537 cosmetic Substances 0.000 claims description 7
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 7
- 238000005562 fading Methods 0.000 claims description 7
- 239000000194 fatty acid Substances 0.000 claims description 7
- 229930195729 fatty acid Natural products 0.000 claims description 7
- 239000000123 paper Substances 0.000 claims description 7
- 239000004793 Polystyrene Substances 0.000 claims description 5
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims description 5
- RJGDLRCDCYRQOQ-UHFFFAOYSA-N anthrone Chemical compound C1=CC=C2C(=O)C3=CC=CC=C3CC2=C1 RJGDLRCDCYRQOQ-UHFFFAOYSA-N 0.000 claims description 5
- 239000004417 polycarbonate Substances 0.000 claims description 5
- 229920000515 polycarbonate Polymers 0.000 claims description 5
- 229920000728 polyester Polymers 0.000 claims description 5
- 229920002223 polystyrene Polymers 0.000 claims description 5
- 239000004952 Polyamide Substances 0.000 claims description 4
- 239000012773 agricultural material Substances 0.000 claims description 4
- 229910052681 coesite Inorganic materials 0.000 claims description 4
- 239000007822 coupling agent Substances 0.000 claims description 4
- 229910052906 cristobalite Inorganic materials 0.000 claims description 4
- 239000004744 fabric Substances 0.000 claims description 4
- 239000010985 leather Substances 0.000 claims description 4
- 229920002647 polyamide Polymers 0.000 claims description 4
- 230000002829 reductive effect Effects 0.000 claims description 4
- 229910052682 stishovite Inorganic materials 0.000 claims description 4
- 229910052905 tridymite Inorganic materials 0.000 claims description 4
- 102100027045 High affinity choline transporter 1 Human genes 0.000 claims description 3
- 101000693882 Homo sapiens High affinity choline transporter 1 Proteins 0.000 claims description 3
- 239000004566 building material Substances 0.000 claims description 3
- 235000013305 food Nutrition 0.000 claims description 3
- 239000004745 nonwoven fabric Substances 0.000 claims description 3
- 210000002784 stomach Anatomy 0.000 claims description 3
- 238000009941 weaving Methods 0.000 claims description 2
- ZEYHEAKUIGZSGI-UHFFFAOYSA-N 4-methoxybenzoic acid Chemical compound COC1=CC=C(C(O)=O)C=C1 ZEYHEAKUIGZSGI-UHFFFAOYSA-N 0.000 claims 1
- 210000003298 dental enamel Anatomy 0.000 claims 1
- 239000000088 plastic resin Substances 0.000 claims 1
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 claims 1
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 claims 1
- 239000010408 film Substances 0.000 description 145
- 235000014692 zinc oxide Nutrition 0.000 description 143
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 41
- 229920005989 resin Polymers 0.000 description 35
- 239000011347 resin Substances 0.000 description 35
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 27
- 239000002994 raw material Substances 0.000 description 25
- 239000003960 organic solvent Substances 0.000 description 22
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 21
- 238000012360 testing method Methods 0.000 description 20
- 230000015572 biosynthetic process Effects 0.000 description 19
- 239000004033 plastic Substances 0.000 description 18
- 229920003023 plastic Polymers 0.000 description 17
- 230000000694 effects Effects 0.000 description 16
- 239000000243 solution Substances 0.000 description 16
- 239000002585 base Substances 0.000 description 15
- CETPSERCERDGAM-UHFFFAOYSA-N ceric oxide Chemical compound O=[Ce]=O CETPSERCERDGAM-UHFFFAOYSA-N 0.000 description 15
- 229910000422 cerium(IV) oxide Inorganic materials 0.000 description 15
- 239000012141 concentrate Substances 0.000 description 15
- 239000004743 Polypropylene Substances 0.000 description 14
- 229920001155 polypropylene Polymers 0.000 description 14
- 238000002835 absorbance Methods 0.000 description 13
- 230000006866 deterioration Effects 0.000 description 13
- 238000001035 drying Methods 0.000 description 13
- 239000000758 substrate Substances 0.000 description 13
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 12
- 230000008859 change Effects 0.000 description 12
- 239000012071 phase Substances 0.000 description 12
- 239000002904 solvent Substances 0.000 description 12
- 239000011882 ultra-fine particle Substances 0.000 description 12
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 description 11
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 10
- 229910052684 Cerium Inorganic materials 0.000 description 10
- GWXLDORMOJMVQZ-UHFFFAOYSA-N cerium Chemical compound [Ce] GWXLDORMOJMVQZ-UHFFFAOYSA-N 0.000 description 10
- 230000000052 comparative effect Effects 0.000 description 10
- 239000000126 substance Substances 0.000 description 10
- 238000005259 measurement Methods 0.000 description 9
- 238000002156 mixing Methods 0.000 description 9
- 238000003756 stirring Methods 0.000 description 9
- 239000002253 acid Substances 0.000 description 8
- 238000004898 kneading Methods 0.000 description 8
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 7
- PTFCDOFLOPIGGS-UHFFFAOYSA-N Zinc dication Chemical compound [Zn+2] PTFCDOFLOPIGGS-UHFFFAOYSA-N 0.000 description 7
- 238000002347 injection Methods 0.000 description 7
- 239000007924 injection Substances 0.000 description 7
- 239000007788 liquid Substances 0.000 description 7
- 239000011859 microparticle Substances 0.000 description 7
- 238000000926 separation method Methods 0.000 description 7
- 239000000725 suspension Substances 0.000 description 7
- CXWXQJXEFPUFDZ-UHFFFAOYSA-N tetralin Chemical compound C1=CC=C2CCCCC2=C1 CXWXQJXEFPUFDZ-UHFFFAOYSA-N 0.000 description 7
- ATRRKUHOCOJYRX-UHFFFAOYSA-N Ammonium bicarbonate Chemical compound [NH4+].OC([O-])=O ATRRKUHOCOJYRX-UHFFFAOYSA-N 0.000 description 6
- KJTLSVCANCCWHF-UHFFFAOYSA-N Ruthenium Chemical compound [Ru] KJTLSVCANCCWHF-UHFFFAOYSA-N 0.000 description 6
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 6
- 239000001099 ammonium carbonate Substances 0.000 description 6
- 230000005540 biological transmission Effects 0.000 description 6
- 238000001354 calcination Methods 0.000 description 6
- 150000004665 fatty acids Chemical class 0.000 description 6
- 239000012510 hollow fiber Substances 0.000 description 6
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 6
- 230000004048 modification Effects 0.000 description 6
- 238000012986 modification Methods 0.000 description 6
- 230000009467 reduction Effects 0.000 description 6
- 229910052707 ruthenium Inorganic materials 0.000 description 6
- 150000003839 salts Chemical class 0.000 description 6
- 238000005406 washing Methods 0.000 description 6
- WJMXTYZCTXTFJM-UHFFFAOYSA-N 1,1,1,2-tetraethoxydecane Chemical compound C(C)OC(C(OCC)(OCC)OCC)CCCCCCCC WJMXTYZCTXTFJM-UHFFFAOYSA-N 0.000 description 5
- TUSDEZXZIZRFGC-UHFFFAOYSA-N 1-O-galloyl-3,6-(R)-HHDP-beta-D-glucose Natural products OC1C(O2)COC(=O)C3=CC(O)=C(O)C(O)=C3C3=C(O)C(O)=C(O)C=C3C(=O)OC1C(O)C2OC(=O)C1=CC(O)=C(O)C(O)=C1 TUSDEZXZIZRFGC-UHFFFAOYSA-N 0.000 description 5
- 239000001263 FEMA 3042 Substances 0.000 description 5
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 5
- YBGZDTIWKVFICR-JLHYYAGUSA-N Octyl 4-methoxycinnamic acid Chemical compound CCCCC(CC)COC(=O)\C=C\C1=CC=C(OC)C=C1 YBGZDTIWKVFICR-JLHYYAGUSA-N 0.000 description 5
- LRBQNJMCXXYXIU-PPKXGCFTSA-N Penta-digallate-beta-D-glucose Natural products OC1=C(O)C(O)=CC(C(=O)OC=2C(=C(O)C=C(C=2)C(=O)OC[C@@H]2[C@H]([C@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)[C@@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)[C@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)O2)OC(=O)C=2C=C(OC(=O)C=3C=C(O)C(O)=C(O)C=3)C(O)=C(O)C=2)O)=C1 LRBQNJMCXXYXIU-PPKXGCFTSA-N 0.000 description 5
- 239000002250 absorbent Substances 0.000 description 5
- 230000002745 absorbent Effects 0.000 description 5
- 239000006096 absorbing agent Substances 0.000 description 5
- 229920000122 acrylonitrile butadiene styrene Polymers 0.000 description 5
- 239000003513 alkali Substances 0.000 description 5
- 230000001276 controlling effect Effects 0.000 description 5
- 239000010410 layer Substances 0.000 description 5
- 230000003647 oxidation Effects 0.000 description 5
- 230000000704 physical effect Effects 0.000 description 5
- 239000002002 slurry Substances 0.000 description 5
- 238000004381 surface treatment Methods 0.000 description 5
- LRBQNJMCXXYXIU-NRMVVENXSA-N tannic acid Chemical compound OC1=C(O)C(O)=CC(C(=O)OC=2C(=C(O)C=C(C=2)C(=O)OC[C@@H]2[C@H]([C@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)[C@@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)[C@@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)O2)OC(=O)C=2C=C(OC(=O)C=3C=C(O)C(O)=C(O)C=3)C(O)=C(O)C=2)O)=C1 LRBQNJMCXXYXIU-NRMVVENXSA-N 0.000 description 5
- 229940033123 tannic acid Drugs 0.000 description 5
- 235000015523 tannic acid Nutrition 0.000 description 5
- 229920002258 tannic acid Polymers 0.000 description 5
- 229910052719 titanium Inorganic materials 0.000 description 5
- 229910000013 Ammonium bicarbonate Inorganic materials 0.000 description 4
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 4
- OAKJQQAXSVQMHS-UHFFFAOYSA-N Hydrazine Chemical compound NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 description 4
- UFWIBTONFRDIAS-UHFFFAOYSA-N Naphthalene Chemical compound C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 description 4
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 4
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 4
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
- 230000002776 aggregation Effects 0.000 description 4
- 229910052783 alkali metal Inorganic materials 0.000 description 4
- 125000000217 alkyl group Chemical group 0.000 description 4
- 229910021529 ammonia Inorganic materials 0.000 description 4
- 235000012538 ammonium bicarbonate Nutrition 0.000 description 4
- 239000007864 aqueous solution Substances 0.000 description 4
- 125000004432 carbon atom Chemical group C* 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 4
- 239000003086 colorant Substances 0.000 description 4
- 239000002270 dispersing agent Substances 0.000 description 4
- 239000006185 dispersion Substances 0.000 description 4
- 238000004090 dissolution Methods 0.000 description 4
- 229910052736 halogen Inorganic materials 0.000 description 4
- 150000002367 halogens Chemical class 0.000 description 4
- 239000001257 hydrogen Substances 0.000 description 4
- 229910052739 hydrogen Inorganic materials 0.000 description 4
- DLINORNFHVEIFE-UHFFFAOYSA-N hydrogen peroxide;zinc Chemical compound [Zn].OO DLINORNFHVEIFE-UHFFFAOYSA-N 0.000 description 4
- 230000007062 hydrolysis Effects 0.000 description 4
- 238000006460 hydrolysis reaction Methods 0.000 description 4
- 229910052742 iron Inorganic materials 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- 229920000642 polymer Polymers 0.000 description 4
- 230000001681 protective effect Effects 0.000 description 4
- 239000011163 secondary particle Substances 0.000 description 4
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 4
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 3
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 3
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 3
- 239000004721 Polyphenylene oxide Substances 0.000 description 3
- 239000004734 Polyphenylene sulfide Substances 0.000 description 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 3
- 229910004298 SiO 2 Inorganic materials 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 description 3
- 239000000654 additive Substances 0.000 description 3
- 239000000853 adhesive Substances 0.000 description 3
- 230000001070 adhesive effect Effects 0.000 description 3
- 238000004220 aggregation Methods 0.000 description 3
- 150000001298 alcohols Chemical class 0.000 description 3
- 125000001931 aliphatic group Chemical group 0.000 description 3
- 150000001340 alkali metals Chemical class 0.000 description 3
- 229910052782 aluminium Inorganic materials 0.000 description 3
- 230000003078 antioxidant effect Effects 0.000 description 3
- 229910052797 bismuth Inorganic materials 0.000 description 3
- JCXGWMGPZLAOME-UHFFFAOYSA-N bismuth atom Chemical compound [Bi] JCXGWMGPZLAOME-UHFFFAOYSA-N 0.000 description 3
- 239000000919 ceramic Substances 0.000 description 3
- 239000000460 chlorine Substances 0.000 description 3
- 239000010949 copper Substances 0.000 description 3
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 3
- 238000010828 elution Methods 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 150000002148 esters Chemical class 0.000 description 3
- 238000001914 filtration Methods 0.000 description 3
- 150000002430 hydrocarbons Chemical group 0.000 description 3
- 239000012535 impurity Substances 0.000 description 3
- 150000002576 ketones Chemical class 0.000 description 3
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 3
- XANYBGJNPZKYMQ-UHFFFAOYSA-N octan-3-yl 3-(4-methoxyphenyl)prop-2-enoate Chemical compound CCCCCC(CC)OC(=O)C=CC1=CC=C(OC)C=C1 XANYBGJNPZKYMQ-UHFFFAOYSA-N 0.000 description 3
- 239000011368 organic material Substances 0.000 description 3
- 239000005022 packaging material Substances 0.000 description 3
- 239000011941 photocatalyst Substances 0.000 description 3
- 229920000768 polyamine Polymers 0.000 description 3
- 229920000570 polyether Polymers 0.000 description 3
- 229920000139 polyethylene terephthalate Polymers 0.000 description 3
- 239000005020 polyethylene terephthalate Substances 0.000 description 3
- 229920000098 polyolefin Polymers 0.000 description 3
- 229920000069 polyphenylene sulfide Polymers 0.000 description 3
- 239000004800 polyvinyl chloride Substances 0.000 description 3
- 229920000915 polyvinyl chloride Polymers 0.000 description 3
- 235000019353 potassium silicate Nutrition 0.000 description 3
- 239000002243 precursor Substances 0.000 description 3
- 238000012545 processing Methods 0.000 description 3
- 238000010298 pulverizing process Methods 0.000 description 3
- 229910000029 sodium carbonate Inorganic materials 0.000 description 3
- 235000017550 sodium carbonate Nutrition 0.000 description 3
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- 238000001291 vacuum drying Methods 0.000 description 3
- 239000011701 zinc Substances 0.000 description 3
- AFDXODALSZRGIH-QPJJXVBHSA-N (E)-3-(4-methoxyphenyl)prop-2-enoic acid Chemical compound COC1=CC=C(\C=C\C(O)=O)C=C1 AFDXODALSZRGIH-QPJJXVBHSA-N 0.000 description 2
- 125000000022 2-aminoethyl group Chemical group [H]C([*])([H])C([H])([H])N([H])[H] 0.000 description 2
- DLFVBJFMPXGRIB-UHFFFAOYSA-N Acetamide Chemical compound CC(N)=O DLFVBJFMPXGRIB-UHFFFAOYSA-N 0.000 description 2
- USFZMSVCRYTOJT-UHFFFAOYSA-N Ammonium acetate Chemical compound N.CC(O)=O USFZMSVCRYTOJT-UHFFFAOYSA-N 0.000 description 2
- 239000005695 Ammonium acetate Substances 0.000 description 2
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- ROSDSFDQCJNGOL-UHFFFAOYSA-N Dimethylamine Chemical compound CNC ROSDSFDQCJNGOL-UHFFFAOYSA-N 0.000 description 2
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 2
- QUSNBJAOOMFDIB-UHFFFAOYSA-N Ethylamine Chemical compound CCN QUSNBJAOOMFDIB-UHFFFAOYSA-N 0.000 description 2
- 239000005977 Ethylene Substances 0.000 description 2
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 2
- BAVYZALUXZFZLV-UHFFFAOYSA-N Methylamine Chemical compound NC BAVYZALUXZFZLV-UHFFFAOYSA-N 0.000 description 2
- AMQJEAYHLZJPGS-UHFFFAOYSA-N N-Pentanol Chemical compound CCCCCO AMQJEAYHLZJPGS-UHFFFAOYSA-N 0.000 description 2
- 229930182556 Polyacetal Natural products 0.000 description 2
- 239000004642 Polyimide Substances 0.000 description 2
- 229920001328 Polyvinylidene chloride Polymers 0.000 description 2
- 239000009759 San-Chi Substances 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 2
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 2
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 2
- 230000001133 acceleration Effects 0.000 description 2
- 239000012790 adhesive layer Substances 0.000 description 2
- 238000005054 agglomeration Methods 0.000 description 2
- 230000032683 aging Effects 0.000 description 2
- 229940043376 ammonium acetate Drugs 0.000 description 2
- 235000019257 ammonium acetate Nutrition 0.000 description 2
- 235000012501 ammonium carbonate Nutrition 0.000 description 2
- VZTDIZULWFCMLS-UHFFFAOYSA-N ammonium formate Chemical compound [NH4+].[O-]C=O VZTDIZULWFCMLS-UHFFFAOYSA-N 0.000 description 2
- 239000003963 antioxidant agent Substances 0.000 description 2
- TZCXTZWJZNENPQ-UHFFFAOYSA-L barium sulfate Chemical compound [Ba+2].[O-]S([O-])(=O)=O TZCXTZWJZNENPQ-UHFFFAOYSA-L 0.000 description 2
- 229910000019 calcium carbonate Inorganic materials 0.000 description 2
- 238000005119 centrifugation Methods 0.000 description 2
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| JP2006077075A (ja) * | 2004-09-08 | 2006-03-23 | Sumitomo Metal Mining Co Ltd | 樹脂組成物と紫外線遮蔽用透明樹脂成形体および紫外線遮蔽用透明樹脂積層体 |
| JP5166689B2 (ja) * | 2005-10-17 | 2013-03-21 | 昭和電工株式会社 | シリカ被覆炭素繊維の製造方法 |
| JP4752525B2 (ja) * | 2006-02-07 | 2011-08-17 | 東洋インキＳｃホールディングス株式会社 | 樹脂組成物 |
| JP5076435B2 (ja) * | 2006-04-05 | 2012-11-21 | 堺化学工業株式会社 | 超微粒子酸化亜鉛及びその製造方法 |
| JP4865388B2 (ja) * | 2006-04-07 | 2012-02-01 | 株式会社 資生堂 | 表面処理酸化亜鉛粉体及びこれを含有する化粧料 |
| JP5200343B2 (ja) * | 2006-07-18 | 2013-06-05 | 東レ株式会社 | 液晶バックライト用白色ポリエステル反射フィルム |
| JP5717339B2 (ja) * | 2006-08-25 | 2015-05-13 | ザッハトレーベン ヒェミー ゲゼルシヤフト ミット ベシュレンクテルハフツングＳａｃｈｔｌｅｂｅｎ Ｃｈｅｍｉｅ ＧｍｂＨ | 無機表面変性された超微粒子 |
| JP2008056873A (ja) * | 2006-09-04 | 2008-03-13 | Kri Inc | ナノコンポジットおよびその製造方法 |
| US20100047590A1 (en) * | 2006-10-06 | 2010-02-25 | Emi Ueda | Ultra-fine zinc oxide particle and method for producing thereof |
| WO2008099458A1 (ja) * | 2007-02-13 | 2008-08-21 | Konica Minolta Opto, Inc. | 熱可塑性樹脂組成物及び光学素子 |
| WO2008099459A1 (ja) * | 2007-02-13 | 2008-08-21 | Konica Minolta Opto, Inc. | 光学用樹脂材料、光学素子及び光学用樹脂材料の製造方法 |
| JP5150826B2 (ja) * | 2007-05-11 | 2013-02-27 | 国立大学法人宇都宮大学 | シリカ被覆酸化亜鉛微粒子の製造方法と、その方法で得られたシリカ被覆酸化亜鉛微粒子 |
| JP5398134B2 (ja) * | 2007-11-15 | 2014-01-29 | 住友金属鉱山株式会社 | 表面処理酸化亜鉛微粒子の製造方法、表面処理酸化亜鉛微粒子、その分散液体および分散固体、並びに酸化亜鉛微粒子被覆基材 |
| JP4655105B2 (ja) | 2008-04-30 | 2011-03-23 | 住友金属鉱山株式会社 | 紫外線遮蔽透明樹脂成形体およびその製造方法 |
| JP2010202731A (ja) * | 2009-03-02 | 2010-09-16 | Shin-Etsu Chemical Co Ltd | 紫外線遮蔽性シリコーンコーティング組成物及び被覆物品 |
| JP2010261012A (ja) * | 2009-04-09 | 2010-11-18 | Shin-Etsu Chemical Co Ltd | 紫外線遮蔽性コーティング組成物及び被覆物品 |
| JP5374286B2 (ja) | 2009-09-14 | 2013-12-25 | 富士フイルム株式会社 | 保護フィルムおよび太陽電池用フロントシート |
| JP5267488B2 (ja) * | 2010-03-11 | 2013-08-21 | 信越化学工業株式会社 | ポリカーボネート樹脂積層体 |
| US20120162332A1 (en) * | 2010-12-22 | 2012-06-28 | Hong Kong Applied Science and Technology Research Institute Company Limited | Sublimation inks for thermal inkjet printers using thermally stable dye particles |
| JP5810906B2 (ja) * | 2011-12-28 | 2015-11-11 | 住友大阪セメント株式会社 | 耐候性粒子と耐候性粒子含有分散液及び耐候性粒子含有樹脂組成物並びにそれを用いた耐候性膜及び耐候性基材 |
| JP6196779B2 (ja) * | 2013-01-31 | 2017-09-13 | 石原産業株式会社 | 絶縁性放熱フィラー及びその製造方法 |
| JP6349877B2 (ja) * | 2013-04-19 | 2018-07-04 | 住友大阪セメント株式会社 | 酸化ケイ素被覆酸化亜鉛とその製造方法及び酸化ケイ素被覆酸化亜鉛含有組成物並びに化粧料 |
| JP6349873B2 (ja) * | 2013-04-19 | 2018-07-04 | 住友大阪セメント株式会社 | 酸化ケイ素被覆酸化亜鉛とその製造方法及び酸化ケイ素被覆酸化亜鉛含有組成物並びに化粧料 |
| EP2995590B1 (en) | 2013-04-19 | 2019-11-13 | Sumitomo Osaka Cement Co., Ltd. | Silicon-oxide-coated zinc oxide and method for manufacturing same, silicon-oxide-coated-zinc-oxide-containing composition, and cosmetic |
| JP2015066865A (ja) * | 2013-09-30 | 2015-04-13 | マツダ株式会社 | 積層塗膜及び塗装物 |
| US9855197B2 (en) | 2013-11-13 | 2018-01-02 | Sumitomo Osaka Cement Co., Ltd. | Zinc oxide which is coated with silicon oxide, method for manufacturing the same, composition which includes the zinc oxide coated with silicon oxide, and cosmetic |
| JP6349875B2 (ja) * | 2014-03-31 | 2018-07-04 | 住友大阪セメント株式会社 | 酸化ケイ素被覆酸化亜鉛とその製造方法及び酸化ケイ素被覆酸化亜鉛含有組成物並びに化粧料 |
| JP6349876B2 (ja) * | 2014-03-31 | 2018-07-04 | 住友大阪セメント株式会社 | 酸化ケイ素被覆酸化亜鉛とその製造方法及び酸化ケイ素被覆酸化亜鉛含有組成物並びに化粧料 |
| KR102246324B1 (ko) | 2014-03-31 | 2021-04-29 | 스미토모 오사카 세멘토 가부시키가이샤 | 산화 규소 피복 산화 아연과 그 제조 방법 및 산화 규소 피복 산화 아연 함유 조성물과 화장료 |
| EP2987834A1 (de) * | 2014-08-18 | 2016-02-24 | Kronos International, Inc. | Verfahren zur Oberflächenbeschichtung von anorganischen Partikeln mit Siliciumdioxid und mindestens einer weiteren anorganischen Verbindung |
| JP6035500B1 (ja) * | 2015-10-05 | 2016-11-30 | エム・テクニック株式会社 | 塗料用ケイ素酸化物被覆酸化鉄組成物 |
| CN109072010B (zh) | 2016-06-02 | 2022-09-23 | M技术株式会社 | 透明材料用紫外线和/或近红外线遮断剂组合物 |
| EP3385337A1 (en) * | 2017-04-05 | 2018-10-10 | Huntsman P&A Uerdingen GmbH | Pigment treated with at least one non-reactive polysiloxane for use in thermoplastics |
| KR102718103B1 (ko) * | 2019-04-24 | 2024-10-16 | 도아고세이가부시키가이샤 | 섬유용 무기입자 및 그 제조 방법 |
| JP7267159B2 (ja) * | 2019-09-12 | 2023-05-01 | 三井金属鉱業株式会社 | 表面処理酸化亜鉛粒子及び塗布用組成物 |
| WO2021200541A1 (ja) * | 2020-03-31 | 2021-10-07 | 住友大阪セメント株式会社 | 表面処理金属酸化物粒子、分散液、化粧料および表面処理金属酸化物粒子の製造方法 |
| CN112812361B (zh) * | 2020-12-31 | 2024-01-09 | 浙江三时纪新材科技有限公司 | 一种二氧化硅粉体填料的制备方法、由此得到的粉体填料及其应用 |
| CN114983884A (zh) * | 2022-05-18 | 2022-09-02 | 青岛周氏塑料包装有限公司 | 一种抑菌保湿生物降解保鲜膜贴及其制备方法 |
| CN119660749A (zh) * | 2024-11-25 | 2025-03-21 | 中南大学 | 一种石英细粉制备光伏坩埚用高纯石英砂的方法 |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH05295141A (ja) * | 1992-04-21 | 1993-11-09 | Toyo Alum Kk | 紫外線吸収性透明フィルム |
| JPH11193354A (ja) * | 1997-12-26 | 1999-07-21 | Fuji Shikiso Kk | シリカ被覆酸化亜鉛粒子、その製法及びその粒子を含有する 組成物 |
| CN1312233C (zh) * | 1999-01-11 | 2007-04-25 | 昭和电工株式会社 | 化妆料、表面疏水化二氧化硅被覆金属氧化物粒子、二氧化硅被覆金属氧化物溶胶、以及它们的制法 |
| JP3503814B2 (ja) * | 1999-04-30 | 2004-03-08 | 冨士色素株式会社 | 変性シリカ被覆金属酸化物、その製法およびそれを含有する組成物 |
| JP4326689B2 (ja) * | 1999-12-24 | 2009-09-09 | 株式会社資生堂 | プラスミノーゲンアクチベーター阻害剤およびそれを配合した皮膚外用剤 |
| US6500415B2 (en) * | 2000-06-05 | 2002-12-31 | Showa Denko K.K. | Cosmetic composition |
| ES2530970T3 (es) * | 2000-06-05 | 2015-03-09 | Showa Denko Kk | Composición cosmética |
| JP2002154915A (ja) * | 2000-09-11 | 2002-05-28 | Showa Denko Kk | 化粧料 |
| JP2002087817A (ja) * | 2000-09-12 | 2002-03-27 | Sumitomo Osaka Cement Co Ltd | 複合酸化亜鉛分散体 |
-
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Also Published As
| Publication number | Publication date |
|---|---|
| JP4582439B2 (ja) | 2010-11-17 |
| TW200401012A (en) | 2004-01-16 |
| JP2004059421A (ja) | 2004-02-26 |
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