TW201219981A - Process for producing electrode materials - Google Patents
Process for producing electrode materials Download PDFInfo
- Publication number
- TW201219981A TW201219981A TW100133827A TW100133827A TW201219981A TW 201219981 A TW201219981 A TW 201219981A TW 100133827 A TW100133827 A TW 100133827A TW 100133827 A TW100133827 A TW 100133827A TW 201219981 A TW201219981 A TW 201219981A
- Authority
- TW
- Taiwan
- Prior art keywords
- mixed oxide
- phosphorus
- electrode material
- compound
- sulfur
- Prior art date
Links
- 239000007772 electrode material Substances 0.000 title claims abstract description 28
- 238000000034 method Methods 0.000 title claims abstract description 26
- 229910052698 phosphorus Inorganic materials 0.000 claims abstract description 33
- 239000011574 phosphorus Substances 0.000 claims abstract description 33
- 150000001875 compounds Chemical class 0.000 claims abstract description 27
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims abstract description 26
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims abstract description 22
- 229910052717 sulfur Inorganic materials 0.000 claims abstract description 20
- 239000011593 sulfur Substances 0.000 claims abstract description 20
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000001301 oxygen Substances 0.000 claims abstract description 13
- 229910052760 oxygen Inorganic materials 0.000 claims abstract description 13
- 229910052783 alkali metal Inorganic materials 0.000 claims abstract description 9
- 150000002894 organic compounds Chemical class 0.000 claims abstract description 9
- 229910052723 transition metal Inorganic materials 0.000 claims abstract description 9
- 150000003624 transition metals Chemical class 0.000 claims abstract description 9
- 150000001340 alkali metals Chemical class 0.000 claims abstract description 8
- 150000001768 cations Chemical class 0.000 claims abstract description 8
- 150000003863 ammonium salts Chemical class 0.000 claims abstract description 6
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 33
- 239000007789 gas Substances 0.000 claims description 15
- 229910052799 carbon Inorganic materials 0.000 claims description 14
- 229910052596 spinel Inorganic materials 0.000 claims description 14
- 239000011029 spinel Substances 0.000 claims description 14
- 229910052751 metal Inorganic materials 0.000 claims description 13
- 239000002184 metal Substances 0.000 claims description 13
- 230000003647 oxidation Effects 0.000 claims description 12
- 238000007254 oxidation reaction Methods 0.000 claims description 12
- 239000011230 binding agent Substances 0.000 claims description 11
- 150000003839 salts Chemical class 0.000 claims description 10
- 239000000203 mixture Substances 0.000 claims description 9
- 125000000217 alkyl group Chemical group 0.000 claims description 7
- 239000001257 hydrogen Substances 0.000 claims description 7
- 229910052739 hydrogen Inorganic materials 0.000 claims description 7
- 150000002739 metals Chemical class 0.000 claims description 7
- 230000000737 periodic effect Effects 0.000 claims description 7
- 239000012071 phase Substances 0.000 claims description 6
- 238000004519 manufacturing process Methods 0.000 claims description 5
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- 150000001335 aliphatic alkanes Chemical class 0.000 claims description 2
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims description 2
- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims 2
- 239000000126 substance Substances 0.000 claims 2
- ABLZXFCXXLZCGV-UHFFFAOYSA-N Phosphorous acid Chemical class OP(O)=O ABLZXFCXXLZCGV-UHFFFAOYSA-N 0.000 claims 1
- 150000003013 phosphoric acid derivatives Chemical class 0.000 claims 1
- 229910000314 transition metal oxide Inorganic materials 0.000 claims 1
- 229910052744 lithium Inorganic materials 0.000 abstract description 9
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 abstract description 8
- -1 alkaline earth metal cation Chemical class 0.000 description 47
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Classifications
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
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- C01G45/00—Compounds of manganese
- C01G45/12—Complex oxides containing manganese and at least one other metal element
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G45/00—Compounds of manganese
- C01G45/12—Complex oxides containing manganese and at least one other metal element
- C01G45/1221—Manganates or manganites with trivalent manganese, tetravalent manganese or mixtures thereof
- C01G45/1228—Manganates or manganites with trivalent manganese, tetravalent manganese or mixtures thereof of the type (MnO2)-, e.g. LiMnO2 or Li(MxMn1-x)O2
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G45/00—Compounds of manganese
- C01G45/12—Complex oxides containing manganese and at least one other metal element
- C01G45/1221—Manganates or manganites with trivalent manganese, tetravalent manganese or mixtures thereof
- C01G45/1242—Manganates or manganites with trivalent manganese, tetravalent manganese or mixtures thereof of the type (Mn2O4)-, e.g. LiMn2O4 or Li(MxMn2-x)O4
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G53/00—Compounds of nickel
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G53/00—Compounds of nickel
- C01G53/40—Complex oxides containing nickel and at least one other metal element
- C01G53/42—Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2
- C01G53/44—Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2 containing manganese
- C01G53/50—Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2 containing manganese of the type (MnO2)n-, e.g. Li(NixMn1-x)O2 or Li(MyNixMn1-x-y)O2
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G53/00—Compounds of nickel
- C01G53/40—Complex oxides containing nickel and at least one other metal element
- C01G53/42—Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2
- C01G53/44—Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2 containing manganese
- C01G53/54—Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2 containing manganese of the type (Mn2O4)-, e.g. Li(NixMn2-x)O4 or Li(MyNixMn2-x-y)O4
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- H—ELECTRICITY
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- H01M10/052—Li-accumulators
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- H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
- H01M4/131—Electrodes based on mixed oxides or hydroxides, or on mixtures of oxides or hydroxides, e.g. LiCoOx
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- H01M4/505—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese of mixed oxides or hydroxides containing manganese for inserting or intercalating light metals, e.g. LiMn2O4 or LiMn2OxFy
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- H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
- H01M4/52—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron
- H01M4/525—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron of mixed oxides or hydroxides containing iron, cobalt or nickel for inserting or intercalating light metals, e.g. LiNiO2, LiCoO2 or LiCoOxFy
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- H01M4/62—Selection of inactive substances as ingredients for active masses, e.g. binders, fillers
- H01M4/624—Electric conductive fillers
- H01M4/625—Carbon or graphite
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/50—Solid solutions
- C01P2002/52—Solid solutions containing elements as dopants
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/80—Particles consisting of a mixture of two or more inorganic phases
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- C01—INORGANIC CHEMISTRY
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- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/40—Electric properties
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
Landscapes
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- General Chemical & Material Sciences (AREA)
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| US9388045B2 (en) | 2013-05-08 | 2016-07-12 | Changs Ascending Enterprise Co. | Synthesis and characterization of lithium nickel manganese cobalt phosphorous oxide |
| KR101684276B1 (ko) * | 2013-09-06 | 2016-12-08 | 주식회사 엘지화학 | 복수의 전극활물질층을 갖는 전극, 이의 제조방법 및 이를 포함하는 전기화학 소자 |
| CA2956032C (en) * | 2014-07-24 | 2019-04-16 | Changs Ascending Enterprise Co., Ltd. | Synthesis and characterization of lithium nickel manganese cobalt phosphorous oxide |
| CN115336085B (zh) * | 2020-06-17 | 2025-12-05 | 广东省皓智科技有限公司 | 复合物的剥离方法 |
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| DE60040964D1 (de) * | 1999-06-04 | 2009-01-15 | Panasonic Corp | Yten und verfahen zu deren herstellung |
| JP2002270184A (ja) * | 2001-03-14 | 2002-09-20 | Hitachi Maxell Ltd | 非水二次電池 |
| JP2002352804A (ja) * | 2001-05-28 | 2002-12-06 | Hitachi Maxell Ltd | 非水二次電池 |
| JP4562496B2 (ja) * | 2004-11-10 | 2010-10-13 | 日本化学工業株式会社 | 改質リチウムマンガン複合酸化物、その製造方法、リチウム二次電池正極活物質組成物及びリチウム二次電池 |
| CN101160684A (zh) * | 2005-03-02 | 2008-04-09 | U芝加哥阿谷尼有限公司 | 用于锂电池的充电过度保护的新型氧化还原穿梭化合物 |
| US7238453B2 (en) * | 2005-04-25 | 2007-07-03 | Ferro Corporation | Non-aqueous electrolytic solution with mixed salts |
| JP5083743B2 (ja) * | 2005-07-06 | 2012-11-28 | 株式会社 東北テクノアーチ | リチウム電池 |
| JP4710916B2 (ja) * | 2008-02-13 | 2011-06-29 | ソニー株式会社 | 非水電解質二次電池用正極活物質、これを用いた非水電解質二次電池用正極および非水電解質二次電池 |
| US8187746B2 (en) * | 2008-05-16 | 2012-05-29 | Uchicago Argonne, Llc | Surface modification agents for lithium batteries |
| FR2937185B1 (fr) * | 2008-10-09 | 2011-02-25 | Batscap Sa | Electrode comprenant un oxyde complexe modifie comme matiere active. |
| JP2010126422A (ja) * | 2008-11-28 | 2010-06-10 | Panasonic Corp | リチウム含有複合酸化物の製造方法および非水系二次電池 |
| JP2010170886A (ja) * | 2009-01-23 | 2010-08-05 | Sony Corp | 電解質および二次電池 |
-
2011
- 2011-09-20 WO PCT/EP2011/066300 patent/WO2012038412A1/de not_active Ceased
- 2011-09-20 JP JP2013528716A patent/JP6305059B2/ja active Active
- 2011-09-20 TW TW100133827A patent/TW201219981A/zh unknown
- 2011-09-20 KR KR1020137010056A patent/KR20130097778A/ko not_active Ceased
- 2011-09-20 EP EP11761551.8A patent/EP2619139B1/de active Active
- 2011-09-20 CN CN201180055691.XA patent/CN103221345B/zh active Active
Also Published As
| Publication number | Publication date |
|---|---|
| CN103221345A (zh) | 2013-07-24 |
| KR20130097778A (ko) | 2013-09-03 |
| JP6305059B2 (ja) | 2018-04-04 |
| EP2619139A1 (de) | 2013-07-31 |
| EP2619139B1 (de) | 2015-11-18 |
| JP2013541147A (ja) | 2013-11-07 |
| WO2012038412A1 (de) | 2012-03-29 |
| CN103221345B (zh) | 2015-10-14 |
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