SU460620A3 - Способ получени акриламида - Google Patents
Способ получени акриламидаInfo
- Publication number
- SU460620A3 SU460620A3 SU1884185A SU1884185A SU460620A3 SU 460620 A3 SU460620 A3 SU 460620A3 SU 1884185 A SU1884185 A SU 1884185A SU 1884185 A SU1884185 A SU 1884185A SU 460620 A3 SU460620 A3 SU 460620A3
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- water
- acrylonitrile
- acrylamide
- production method
- added
- Prior art date
Links
- HRPVXLWXLXDGHG-UHFFFAOYSA-N Acrylamide Chemical compound NC(=O)C=C HRPVXLWXLXDGHG-UHFFFAOYSA-N 0.000 title description 8
- 238000004519 manufacturing process Methods 0.000 title 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 14
- 238000006243 chemical reaction Methods 0.000 description 10
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 9
- NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 description 8
- 238000000034 method Methods 0.000 description 7
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 5
- 229910052802 copper Inorganic materials 0.000 description 5
- 239000010949 copper Substances 0.000 description 5
- ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical compound [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 239000003054 catalyst Substances 0.000 description 3
- 229910000365 copper sulfate Inorganic materials 0.000 description 3
- 230000036571 hydration Effects 0.000 description 3
- 238000006703 hydration reaction Methods 0.000 description 3
- 239000002244 precipitate Substances 0.000 description 3
- 229910000033 sodium borohydride Inorganic materials 0.000 description 3
- 239000012279 sodium borohydride Substances 0.000 description 3
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 239000008121 dextrose Substances 0.000 description 2
- 239000002638 heterogeneous catalyst Substances 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 239000012300 argon atmosphere Substances 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000000887 hydrating effect Effects 0.000 description 1
- 150000002825 nitriles Chemical class 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000013049 sediment Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
- B01J23/72—Copper
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US05/226,863 US4048226A (en) | 1972-02-16 | 1972-02-16 | Copper catalyst for hydration of nitriles to amides |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU460620A3 true SU460620A3 (ru) | 1975-02-15 |
Family
ID=22850720
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU1884185A SU460620A3 (ru) | 1972-02-16 | 1973-02-15 | Способ получени акриламида |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US4048226A (OSRAM) |
| JP (1) | JPS4947302A (OSRAM) |
| BE (1) | BE795361A (OSRAM) |
| CS (1) | CS162639B2 (OSRAM) |
| DD (1) | DD106165A5 (OSRAM) |
| DE (1) | DE2303648A1 (OSRAM) |
| FR (1) | FR2172303B1 (OSRAM) |
| IT (1) | IT977161B (OSRAM) |
| NL (1) | NL7301092A (OSRAM) |
| RO (1) | RO62799A (OSRAM) |
| SU (1) | SU460620A3 (OSRAM) |
Families Citing this family (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1404532A (en) * | 1972-09-02 | 1975-09-03 | Mitsubishi Chem Ind | Process for hydrating a nitrile to the corresponding amide |
| IT1043441B (it) * | 1975-10-17 | 1980-02-20 | Snam Progetti | Procedimento per la idratazione di nitrili ad ammidi catalizzatore ivi impiegato e procedimento per la sua preparazione |
| JP2990568B2 (ja) * | 1993-12-13 | 1999-12-13 | 花王株式会社 | 銅含有水素化触媒の調製法およびアルコールの製造法 |
| TW316852B (OSRAM) * | 1994-08-02 | 1997-10-01 | Mitsui Toatsu Chemicals | |
| KR20070051281A (ko) * | 2004-08-20 | 2007-05-17 | 이시하라 산교 가부시끼가이샤 | 구리 미립자 및 구리 미립자의 제조 공정 |
| WO2016050817A1 (en) | 2014-09-30 | 2016-04-07 | Basf Se | Method for producing acrylamide from acrylonitrile in an aqueous solution |
| KR20170066471A (ko) | 2014-09-30 | 2017-06-14 | 바스프 에스이 | 낮은 아크릴산 농도를 갖는 아크릴아미드 수용액의 제조 방법 |
| WO2016050819A1 (en) | 2014-09-30 | 2016-04-07 | Basf Se | Method for preparing an acrylamide solution having a low acrylic acid concentration |
| EP3225693A1 (en) | 2016-03-29 | 2017-10-04 | Basf Se | Method for preparing aqueous acrylamide solutions |
| RU2751919C2 (ru) | 2016-03-29 | 2021-07-20 | Басф Се | Способ получения раствора полиакриламида с увеличенной вязкостью |
| EP3225694A1 (en) | 2016-03-29 | 2017-10-04 | Basf Se | Method for the production of acrylamide by defined addition of the biocatalyst |
| CA3156963A1 (en) | 2019-11-05 | 2021-05-14 | Diego GHISLIERI | Method of storing a biocatalyst |
| WO2021204850A1 (en) | 2020-04-09 | 2021-10-14 | Basf Se | Biocatalytic synthesis of monomer mixtures for polyacrylamide manufacturing |
| CN114763268B (zh) * | 2021-01-13 | 2023-11-17 | 中国科学院上海高等研究院 | 一种片状纳米氧化铜及其制备方法和用途 |
| WO2023041515A2 (en) | 2021-09-15 | 2023-03-23 | Basf Se | Method for preparing an aqueous (meth) acrylamide solution |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3597481A (en) * | 1969-01-16 | 1971-08-03 | Dow Chemical Co | Heterogeneous catalyst for the liquid phase hydrolysis of nitriles to amides |
| US3758578A (en) * | 1969-06-23 | 1973-09-11 | Dow Chemical Co | Hydration of nitriles to amides using cupreous catalysts |
| US3962333A (en) * | 1970-12-14 | 1976-06-08 | Mitsui Toatsu Chemicals, Incorporated | Process for the production of acrylamide and methacrylamide |
| JPS547754B1 (OSRAM) * | 1970-12-24 | 1979-04-10 |
-
0
- BE BE795361D patent/BE795361A/xx unknown
-
1972
- 1972-02-16 US US05/226,863 patent/US4048226A/en not_active Expired - Lifetime
-
1973
- 1973-01-25 DE DE2303648A patent/DE2303648A1/de active Pending
- 1973-01-25 NL NL7301092A patent/NL7301092A/xx unknown
- 1973-02-01 IT IT48015/73A patent/IT977161B/it active
- 1973-02-09 DD DD168775A patent/DD106165A5/xx unknown
- 1973-02-14 JP JP48017536A patent/JPS4947302A/ja active Pending
- 1973-02-14 CS CS1073*BA patent/CS162639B2/cs unknown
- 1973-02-15 FR FR7305405A patent/FR2172303B1/fr not_active Expired
- 1973-02-15 SU SU1884185A patent/SU460620A3/ru active
- 1973-02-16 RO RO7300073877A patent/RO62799A/ro unknown
Also Published As
| Publication number | Publication date |
|---|---|
| RO62799A (fr) | 1977-11-15 |
| IT977161B (it) | 1974-09-10 |
| BE795361A (fr) | 1973-08-13 |
| NL7301092A (OSRAM) | 1973-08-20 |
| US4048226A (en) | 1977-09-13 |
| DD106165A5 (OSRAM) | 1974-06-05 |
| DE2303648A1 (de) | 1973-08-30 |
| JPS4947302A (OSRAM) | 1974-05-08 |
| CS162639B2 (OSRAM) | 1975-07-15 |
| FR2172303A1 (OSRAM) | 1973-09-28 |
| FR2172303B1 (OSRAM) | 1976-11-05 |
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