SU374320A1 - - Google Patents

Info

Publication number

SU374320A1

SU374320A1 SU1651781A SU1651781A SU374320A1 SU 374320 A1 SU374320 A1 SU 374320A1 SU 1651781 A SU1651781 A SU 1651781A SU 1651781 A SU1651781 A SU 1651781A SU 374320 A1 SU374320 A1 SU 374320A1

Authority

SU

USSR - Soviet Union

Prior art keywords

mol

solution

benzene

soluble

methyl

Prior art date

1971-04-29

Links

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• UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 27
• 239000000243 solution Substances 0.000 description 9
• KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 description 8
• 238000000034 method Methods 0.000 description 8
• FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 description 6
• LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
• 239000007864 aqueous solution Substances 0.000 description 4
• 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 4
• 159000000000 sodium salts Chemical class 0.000 description 4
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
• WFDIJRYMOXRFFG-UHFFFAOYSA-N Acetic anhydride Chemical compound CC(=O)OC(C)=O WFDIJRYMOXRFFG-UHFFFAOYSA-N 0.000 description 3
• 235000019441 ethanol Nutrition 0.000 description 3
• 239000000843 powder Substances 0.000 description 3
• 238000002360 preparation method Methods 0.000 description 3
• 239000000047 product Substances 0.000 description 3
• RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
• UMXSHEUZMQMOHJ-UHFFFAOYSA-K F[Sn](C=C)(F)F Chemical compound F[Sn](C=C)(F)F UMXSHEUZMQMOHJ-UHFFFAOYSA-K 0.000 description 2
• FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
• 125000000217 alkyl group Chemical group 0.000 description 2
• 125000003118 aryl group Chemical group 0.000 description 2
• 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 2
• 239000002244 precipitate Substances 0.000 description 2
• 239000011541 reaction mixture Substances 0.000 description 2
• 238000003756 stirring Methods 0.000 description 2
• OBETXYAYXDNJHR-SSDOTTSWSA-M (2r)-2-ethylhexanoate Chemical compound CCCC[C@@H](CC)C([O-])=O OBETXYAYXDNJHR-SSDOTTSWSA-M 0.000 description 1
• -1 al | kenyl Chemical group 0.000 description 1
• 125000003342 alkenyl group Chemical group 0.000 description 1
• OBETXYAYXDNJHR-UHFFFAOYSA-N alpha-ethylcaproic acid Natural products CCCCC(CC)C(O)=O OBETXYAYXDNJHR-UHFFFAOYSA-N 0.000 description 1
• 239000007795 chemical reaction product Substances 0.000 description 1
• 150000001875 compounds Chemical class 0.000 description 1
• 238000010908 decantation Methods 0.000 description 1
• 125000005909 ethyl alcohol group Chemical group 0.000 description 1
• XOQNTEXYXRKHRE-UHFFFAOYSA-K ethyl(trifluoro)stannane Chemical compound [F-].[F-].[F-].CC[Sn+3] XOQNTEXYXRKHRE-UHFFFAOYSA-K 0.000 description 1
• 238000001914 filtration Methods 0.000 description 1
• 230000003993 interaction Effects 0.000 description 1
• 238000002844 melting Methods 0.000 description 1
• 230000008018 melting Effects 0.000 description 1
• OKKJLVBELUTLKV-UHFFFAOYSA-N methanol Natural products OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 1
• 239000000203 mixture Substances 0.000 description 1
• UBOGEXSQACVGEC-UHFFFAOYSA-K phenyltin(3+);trichloride Chemical compound Cl[Sn](Cl)(Cl)C1=CC=CC=C1 UBOGEXSQACVGEC-UHFFFAOYSA-K 0.000 description 1
• 238000011084 recovery Methods 0.000 description 1
• 229940096017 silver fluoride Drugs 0.000 description 1
• REYHXKZHIMGNSE-UHFFFAOYSA-M silver monofluoride Chemical compound [F-].[Ag+] REYHXKZHIMGNSE-UHFFFAOYSA-M 0.000 description 1
• 239000011780 sodium chloride Substances 0.000 description 1
• 239000000126 substance Substances 0.000 description 1
• URNVMBADOXXKOA-UHFFFAOYSA-K trichloro(ethenyl)stannane Chemical compound Cl[Sn](Cl)(Cl)C=C URNVMBADOXXKOA-UHFFFAOYSA-K 0.000 description 1
• MEBRQLCKPRKBOH-UHFFFAOYSA-K trichloro(ethyl)stannane Chemical compound CC[Sn](Cl)(Cl)Cl MEBRQLCKPRKBOH-UHFFFAOYSA-K 0.000 description 1
• XAIPAYFAKXNGSA-UHFFFAOYSA-K trifluoro(phenyl)stannane Chemical compound F[Sn](F)(F)C1=CC=CC=C1 XAIPAYFAKXNGSA-UHFFFAOYSA-K 0.000 description 1
• 238000005406 washing Methods 0.000 description 1