SU315357A1 - - Google Patents

Info

Publication number

SU315357A1

SU315357A1 SU1328068A SU1328068A SU315357A1 SU 315357 A1 SU315357 A1 SU 315357A1 SU 1328068 A SU1328068 A SU 1328068A SU 1328068 A SU1328068 A SU 1328068A SU 315357 A1 SU315357 A1 SU 315357A1

Authority

SU

USSR - Soviet Union

Prior art keywords

acid

methyl

benzoxazolyl

naphthylamine

isolated

Prior art date

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• 239000002253 acid Substances 0.000 description 9
• 238000000034 method Methods 0.000 description 8
• HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 6
• -1 2-BENZOXAZOLYL Chemical class 0.000 description 5
• LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
• ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 description 3
• 239000003960 organic solvent Substances 0.000 description 3
• 239000000047 product Substances 0.000 description 3
• RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
• 239000011230 binding agent Substances 0.000 description 2
• 150000008280 chlorinated hydrocarbons Chemical group 0.000 description 2
• 150000004820 halides Chemical class 0.000 description 2
• 239000000203 mixture Substances 0.000 description 2
• 238000002360 preparation method Methods 0.000 description 2
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
• BCMCBBGGLRIHSE-UHFFFAOYSA-N 1,3-benzoxazole Chemical class C1=CC=C2OC=NC2=C1 BCMCBBGGLRIHSE-UHFFFAOYSA-N 0.000 description 1
• NGNBDVOYPDDBFK-UHFFFAOYSA-N 2-[2,4-di(pentan-2-yl)phenoxy]acetyl chloride Chemical compound CCCC(C)C1=CC=C(OCC(Cl)=O)C(C(C)CCC)=C1 NGNBDVOYPDDBFK-UHFFFAOYSA-N 0.000 description 1
• 150000007860 aryl ester derivatives Chemical class 0.000 description 1
• 230000015572 biosynthetic process Effects 0.000 description 1
• 238000006243 chemical reaction Methods 0.000 description 1
• 239000007795 chemical reaction product Substances 0.000 description 1
• 239000003795 chemical substances by application Substances 0.000 description 1
• 239000013078 crystal Substances 0.000 description 1
• 150000002148 esters Chemical class 0.000 description 1
• 238000001704 evaporation Methods 0.000 description 1
• 230000008020 evaporation Effects 0.000 description 1
• 239000000706 filtrate Substances 0.000 description 1
• 238000002955 isolation Methods 0.000 description 1
• VUYJXUZTXIBVJE-UHFFFAOYSA-N methyl(naphthalen-1-yl)carbamodithioic acid Chemical compound C1=CC=C2C(N(C(S)=S)C)=CC=CC2=C1 VUYJXUZTXIBVJE-UHFFFAOYSA-N 0.000 description 1
• 150000007530 organic bases Chemical group 0.000 description 1
• 239000002244 precipitate Substances 0.000 description 1
• 238000003756 stirring Methods 0.000 description 1
• 239000000126 substance Substances 0.000 description 1
• ILWRPSCZWQJDMK-UHFFFAOYSA-N triethylazanium;chloride Chemical compound Cl.CCN(CC)CC ILWRPSCZWQJDMK-UHFFFAOYSA-N 0.000 description 1