SU1584762A3 - Способ получени фольгированного металлом слоистого материала - Google Patents

Способ получени фольгированного металлом слоистого материала Download PDF

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SU1584762A3
SU1584762A3 SU833583670A SU3583670A SU1584762A3 SU 1584762 A3 SU1584762 A3 SU 1584762A3 SU 833583670 A SU833583670 A SU 833583670A SU 3583670 A SU3583670 A SU 3583670A SU 1584762 A3 SU1584762 A3 SU 1584762A3
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epoxy resin
paper
fabric
epoxy
amount
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SU833583670A
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Янагида Томоми
Адзики Минутори
Сузуки Сигеру
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Сумитомо Бейклайт Компани Лимитед (Фирма)
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Priority claimed from JP6405082A external-priority patent/JPS58181636A/ja
Priority claimed from JP6405482A external-priority patent/JPS58181640A/ja
Priority claimed from JP6405282A external-priority patent/JPS58181638A/ja
Priority claimed from JP6405382A external-priority patent/JPS58181639A/ja
Priority claimed from JP6405182A external-priority patent/JPS58181637A/ja
Priority claimed from JP6405582A external-priority patent/JPS58181641A/ja
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    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B15/00—Layered products comprising a layer of metal
    • B32B15/04—Layered products comprising a layer of metal comprising metal as the main or only constituent of a layer, which is next to another layer of the same or of a different material
    • B32B15/08—Layered products comprising a layer of metal comprising metal as the main or only constituent of a layer, which is next to another layer of the same or of a different material of synthetic resin
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B15/00—Layered products comprising a layer of metal
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    • B32B15/085—Layered products comprising a layer of metal comprising metal as the main or only constituent of a layer, which is next to another layer of the same or of a different material of synthetic resin comprising polyolefins
    • B—PERFORMING OPERATIONS; TRANSPORTING
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    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
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    • B32B27/06—Layered products comprising a layer of synthetic resin as the main or only constituent of a layer, which is next to another layer of the same or of a different material
    • B32B27/10—Layered products comprising a layer of synthetic resin as the main or only constituent of a layer, which is next to another layer of the same or of a different material of paper or cardboard
    • B—PERFORMING OPERATIONS; TRANSPORTING
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    • B32B27/28—Layered products comprising a layer of synthetic resin comprising synthetic resins not wholly covered by any one of the sub-groups B32B27/30 - B32B27/42
    • B32B27/285—Layered products comprising a layer of synthetic resin comprising synthetic resins not wholly covered by any one of the sub-groups B32B27/30 - B32B27/42 comprising polyethers
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    • H—ELECTRICITY
    • H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
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    • H05K2201/0158—Polyalkene or polyolefin, e.g. polyethylene [PE], polypropylene [PP]
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Abstract

Изобретение относитс  к электротехнике и может быть применено, в частности, при изготовлении фольгированных диэлектриков. Цель изобретени  - повышение диэлектрических свойств при высокой температуре и влажности. Изготовл ют листы на основе полиэтилена высокой плотности путем экструдировани  в нити композиции, включающей 100 мас.ч. полиэтилена высокой плотности, 0,1 - 0,2 мас. ч. радикального инициатора, имеющего период полураспада при температуре 140° 6 мин и менее, силана общей формулы RR 1S
Y 2, где R - одновалентна  олефинова  ненасыщенна  группа, св занна  с атомом кремни  посредством кремниево-углеродной св зи и содержаща  углерод, водород и, если необходимо, кислород, R 1 - гидролизуема  гидроуглеродна  группа, Y - гидролизуема  органическа  группа, в количестве 1,5 - 2,0 мас.ч. Осуществл ют рубку нитей в гранулы и обработку гранул пнеформованием или шприцеванием, а подложку выполн ют из бумаги или ткани, содержащей 5 - 35% эпоксидной смолы от массы всей бумаги или ткани и оловоорганический катализатор в количестве 3,5 - 9,0 мас.ч. на 100 мас.ч. эпоксидной смолы или эпоксидную смолу и оловоорганический катализатор в количестве 0,5 - 10,0% в расчете на массу бумаги или ткани. После изготовлени  листов осуществл ют стопирование по меньшей мере двух упом нутых листов, между листами располагают упом нутую подложку, с одной стороны на лист полиэтилена накладывают тонкую пластину металлической фольги, после чего полученный пакет формуют при температуре 160°С давлением 60 кг/см 2 в течение 120 мин. 1 табл.

Description

Изобретение относитс  к электротех нике и может быть применено, в частности, при изготовлении фолъгиро- ванных диэлектриков.
Цель изобретени  - повышение диэлектрических свонсть при высокой температуре и влажности .
Пример 1. К 100 мае.ч. полиэтилена высокой плотности добавл етс  2 мае.ч. винилтриметоксисила- на, 0,2 мае.ч. дикумил перекиси и необходимое количество антиоксиданта. После перемешивани  полученна  масса была выдавлена в виде пучка при помощи шприцмашины и порезана дл  гранул ции . Полученные таким образом гранулы были превращены в лист- толщиной 200 мкм пневмоформованием.
Пример 2. К 170 мае.ч. полиэтилена низкой плотности добавл етс  1,5 мае,ч. винилтриэпоксисилана 0,1 мае.ч. дикумил перекиси, 20 мае.ч. галогенсодержащего пламе- замедлител , 10 мае.ч. окиси сурьмы и необходимое количество антиоксиданта . После перемешивани  полученна  смесь была выдавлена в виде пучка при помощи шприцмашины и гранулирована . Полученные таким образом гранулы были отформованы в лист толщиной 200 мкм шприцеванием.
Дл  приготовлени  препрега эпоксидной смолы или тканевой подложки используетс  композици , приведенна  в таблице.
Дл  получени  фольгированного металлом слоистого материала берут два листа полиэтилена, приготовленных по указанной методике, между которыми располагают подложку, полученную из композиций, представленных в таблице. Затем, по меньшей мере, с одной стороны накладывают тонкую пластину металлической фольги, после чего полученный пакет формуют при температуре 160°С давлением 60 кг/см в течение 120 мин. Приготовленный по данному способу слоистый материал обладает высокими диэлектрическими
, 574762

Claims (2)

  1. Формула изобретени  Способ получени  фольгированного металлом слоистого материала, при котором осуществл ют стопирование по меньшей мере двух листов на основе полиэтилена высокой плотности, модифицированного силаном общей формулы
    (I)
    10
    15
    20
    RR1SiYi,
    где R - одновалентна  олефинова  ненасыщенна  группа, св занна  с атомом кремни  посредством кремниево-углеродной св зи и содержаща  углерод, водород и, если необходимо, кислород; R1 - гидролизуема  гидроуглеродна 
    группа; Y - гидролизуема  органическа 
    группа,
    между указанными листами располагают подложку, содержащую эпоксидную смолу и оловоорганический катализатор, а по меньшей мере с одной стороны на лист полиэтилена накладывают тонкую пластину металлической фольги, после чего полученный пакет формуют при температуре 160°С давлением 60 кг/см2 в течение 120 мин, отлйч а ю - щ и и с   тем, что, с целью повышени  диэлектрических свойств при высокой температуре и влажности, изготовление листов на основе полиэтилена осуществл ют путем экструдировани  в эс нити композиции, включающей 100 мае.ч полиэтилена высокой плотности, 0,1-0,2 мае.ч. радикального инициатора , имеющего период полураспада при температуре 140°С 6 мин и менее, си- 40 лана общей формулы (I) в количестве 1,5-2,0 мае.ч., рубку нитей в гранулы и.обработку гранул пнеформованием или шприцеванием, а подложку выполн ют из бумаги или ткани, содержащей
    25
    30
    свойствами, в частности величина тан- 45 5-35% эпоксидной смолы по массе всей генса угла диэлектрических потерь бумаги или ткани, и оловоорганический составл ет 20-10, диэлектрическа  катализатор в ко личестве 3,5- проницаемость 2,9-3,0, дрейф электростатической емкости находитс  в пре9 ,0 мае.ч. на 100 мае.ч. эпоксидной смолы или эпоксидную смолу и оловоорделах 0,9-1,0%, абсорбци  воды 0,02-0,03%, усилие отслаивани  1,7- 2,2 кг/сЯ.
    5-35% эпоксидной смолы по массе всей бумаги или ткани, и оловоорганический катализатор в ко личестве 3,5-
    9,0 мае.ч. на 100 мае.ч. эпоксидной смолы или эпоксидную смолу и оловоор50
    ганический катализатор в количестве 0,5-10,0% по массе в расчете на массу бумаги или ткани.
    Примечание. 1. Бис-фенольна  А типа бронированна  эпоксидна  смола
    (Shell Chemical), эпоксидное число 500, содержание 20%.
  2. 2. Креэал-новолачного типа смола (DAINIPPON INK and Chemical ), эпоксидное число 200.
    Редактор ХиГратилло
    Составитель А.Круглнков
    Техред м.ДидыкКорректор М. Кучер ва ,
    Заказ 2267
    Тираж 440
    ВНИИПИ Государственного комитета по Изобретени м   открыти м при ГКНТ СССР 113035, Москва, Ж-35, Раушска  наб., д. 4/5
    Производственно-издательский комбинат Патент, г. Ужгород, ул. Гагарина, 101
    Подписное
SU833583670A 1982-04-19 1983-04-18 Способ получени фольгированного металлом слоистого материала SU1584762A3 (ru)

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JP6405082A JPS58181636A (ja) 1982-04-19 1982-04-19 金属張板及びその製造方法
JP6405482A JPS58181640A (ja) 1982-04-19 1982-04-19 金属張板及びその製造方法
JP6405282A JPS58181638A (ja) 1982-04-19 1982-04-19 金属張板及びその製造方法
JP6405382A JPS58181639A (ja) 1982-04-19 1982-04-19 金属張板及びその製造方法
JP6405182A JPS58181637A (ja) 1982-04-19 1982-04-19 金属張板及びその製造方法
JP6405582A JPS58181641A (ja) 1982-04-19 1982-04-19 金属張板及びその製造方法

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JP2557898B2 (ja) * 1987-07-31 1996-11-27 株式会社東芝 半導体装置
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DE3313579C2 (ru) 1991-02-14
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US4499145A (en) 1985-02-12
DE3313579A1 (de) 1983-10-20
GB8310331D0 (en) 1983-05-18

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