SK282576B6 - Spôsob výroby časticovej detergentnej zmesi - Google Patents
Spôsob výroby časticovej detergentnej zmesi Download PDFInfo
- Publication number
- SK282576B6 SK282576B6 SK145-97A SK14597A SK282576B6 SK 282576 B6 SK282576 B6 SK 282576B6 SK 14597 A SK14597 A SK 14597A SK 282576 B6 SK282576 B6 SK 282576B6
- Authority
- SK
- Slovakia
- Prior art keywords
- detergent
- bulk density
- particulate
- acid precursor
- neutralizing agent
- Prior art date
Links
- 239000003599 detergent Substances 0.000 title claims abstract description 48
- 239000000203 mixture Substances 0.000 title claims abstract description 31
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 8
- 239000002253 acid Substances 0.000 claims abstract description 27
- 239000000463 material Substances 0.000 claims abstract description 20
- 239000002243 precursor Substances 0.000 claims abstract description 19
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 17
- 230000003472 neutralizing effect Effects 0.000 claims abstract description 17
- 239000011236 particulate material Substances 0.000 claims abstract description 10
- 239000007788 liquid Substances 0.000 claims abstract description 4
- 239000003945 anionic surfactant Substances 0.000 claims description 8
- 239000002245 particle Substances 0.000 abstract description 22
- 238000006386 neutralization reaction Methods 0.000 abstract description 16
- 239000004094 surface-active agent Substances 0.000 abstract description 8
- 125000000129 anionic group Chemical group 0.000 abstract 1
- 238000000034 method Methods 0.000 description 29
- 239000000843 powder Substances 0.000 description 24
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 14
- HWGNBUXHKFFFIH-UHFFFAOYSA-I pentasodium;[oxido(phosphonatooxy)phosphoryl] phosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O HWGNBUXHKFFFIH-UHFFFAOYSA-I 0.000 description 13
- 235000019832 sodium triphosphate Nutrition 0.000 description 13
- 229910021532 Calcite Inorganic materials 0.000 description 8
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 6
- 238000009826 distribution Methods 0.000 description 6
- 230000000694 effects Effects 0.000 description 6
- 229910000029 sodium carbonate Inorganic materials 0.000 description 6
- 235000017550 sodium carbonate Nutrition 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- 239000000047 product Substances 0.000 description 5
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 description 4
- 239000000945 filler Substances 0.000 description 4
- 239000012628 flowing agent Substances 0.000 description 4
- 150000003839 salts Chemical class 0.000 description 4
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 3
- 230000002378 acidificating effect Effects 0.000 description 3
- 238000005243 fluidization Methods 0.000 description 3
- 238000009472 formulation Methods 0.000 description 3
- 239000000377 silicon dioxide Substances 0.000 description 3
- 239000000344 soap Substances 0.000 description 3
- 238000001694 spray drying Methods 0.000 description 3
- 102000004190 Enzymes Human genes 0.000 description 2
- 108090000790 Enzymes Proteins 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 229910000288 alkali metal carbonate Inorganic materials 0.000 description 2
- 150000008041 alkali metal carbonates Chemical class 0.000 description 2
- 229910052910 alkali metal silicate Inorganic materials 0.000 description 2
- 239000004927 clay Substances 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 238000004090 dissolution Methods 0.000 description 2
- 239000008187 granular material Substances 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 229910010272 inorganic material Inorganic materials 0.000 description 2
- 239000011147 inorganic material Substances 0.000 description 2
- 229910052943 magnesium sulfate Inorganic materials 0.000 description 2
- 235000019341 magnesium sulphate Nutrition 0.000 description 2
- 239000010451 perlite Substances 0.000 description 2
- 235000019362 perlite Nutrition 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 239000010802 sludge Substances 0.000 description 2
- 239000007858 starting material Substances 0.000 description 2
- QJRVOJKLQNSNDB-UHFFFAOYSA-N 4-dodecan-3-ylbenzenesulfonic acid Chemical compound CCCCCCCCCC(CC)C1=CC=C(S(O)(=O)=O)C=C1 QJRVOJKLQNSNDB-UHFFFAOYSA-N 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-M Bicarbonate Chemical class OC([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-M 0.000 description 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 1
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 1
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
- 229910021536 Zeolite Inorganic materials 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- 239000012670 alkaline solution Substances 0.000 description 1
- 239000012683 anionic precursor Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000004566 building material Substances 0.000 description 1
- 229910000019 calcium carbonate Inorganic materials 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 125000002091 cationic group Chemical group 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 239000003085 diluting agent Substances 0.000 description 1
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- -1 fluorescent Substances 0.000 description 1
- 238000005469 granulation Methods 0.000 description 1
- 230000003179 granulation Effects 0.000 description 1
- 159000000011 group IA salts Chemical class 0.000 description 1
- 229910017053 inorganic salt Inorganic materials 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000002736 nonionic surfactant Substances 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 235000020030 perry Nutrition 0.000 description 1
- 239000012254 powdered material Substances 0.000 description 1
- 229940088417 precipitated calcium carbonate Drugs 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 230000003134 recirculating effect Effects 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 235000003441 saturated fatty acids Nutrition 0.000 description 1
- 150000004671 saturated fatty acids Chemical class 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 239000001509 sodium citrate Substances 0.000 description 1
- NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical compound O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- 239000011343 solid material Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 1
- 150000004670 unsaturated fatty acids Chemical class 0.000 description 1
- 239000010457 zeolite Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/06—Powder; Flakes; Free-flowing mixtures; Sheets
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/04—Special methods for preparing compositions containing mixtures of detergents by chemical means, e.g. by sulfonating in the presence of other compounding ingredients followed by neutralising
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Detergent Compositions (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB9415904A GB9415904D0 (en) | 1994-08-05 | 1994-08-05 | Process for the production of detergent composition |
| PCT/EP1995/002935 WO1996004359A1 (fr) | 1994-08-05 | 1995-07-24 | Granulation survenant dans un lit fluidise |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| SK14597A3 SK14597A3 (en) | 1997-07-09 |
| SK282576B6 true SK282576B6 (sk) | 2002-10-08 |
Family
ID=10759488
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SK145-97A SK282576B6 (sk) | 1994-08-05 | 1995-07-24 | Spôsob výroby časticovej detergentnej zmesi |
Country Status (13)
| Country | Link |
|---|---|
| EP (1) | EP0775193A1 (fr) |
| CN (1) | CN1115403C (fr) |
| AU (1) | AU702808B2 (fr) |
| BR (1) | BR9508505A (fr) |
| CA (1) | CA2195313A1 (fr) |
| CZ (1) | CZ289884B6 (fr) |
| GB (1) | GB9415904D0 (fr) |
| HU (1) | HU222907B1 (fr) |
| PL (1) | PL181161B1 (fr) |
| SK (1) | SK282576B6 (fr) |
| TW (1) | TW380161B (fr) |
| WO (1) | WO1996004359A1 (fr) |
| ZA (1) | ZA956415B (fr) |
Families Citing this family (29)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB9526097D0 (en) * | 1995-12-20 | 1996-02-21 | Unilever Plc | Process |
| TW397862B (en) * | 1996-09-06 | 2000-07-11 | Kao Corp | Detergent granules and method for producing the same, and high-bulk density detergent composition |
| US6172034B1 (en) | 1996-10-04 | 2001-01-09 | The Procter & Gamble | Process for making a detergent composition by non-tower process |
| US6143711A (en) * | 1996-10-04 | 2000-11-07 | The Procter & Gamble Company | Process for making a detergent composition by non-tower process |
| US6150323A (en) * | 1996-10-04 | 2000-11-21 | The Procter & Gamble Company | Process for making a detergent composition by non-tower process |
| US6211137B1 (en) | 1996-10-04 | 2001-04-03 | The Procter & Gamble Company | Process for making a detergent composition by non-tower process |
| US6136777A (en) * | 1996-10-04 | 2000-10-24 | The Procter & Gamble Company | Process for making a detergent composition by non-tower process |
| US6391844B1 (en) | 1996-10-04 | 2002-05-21 | The Procter & Gamble Company | Process for making a detergent composition by non-tower process |
| US6121229A (en) * | 1996-10-04 | 2000-09-19 | The Procter & Gamble Company | Process for making a detergent composition by non-tower process |
| US6211138B1 (en) | 1996-10-04 | 2001-04-03 | The Procter & Gamble Company | Process for making a detergent composition by non-tower process |
| GB9712580D0 (en) * | 1997-06-16 | 1997-08-20 | Unilever Plc | Production of detergent granulates |
| GB9712583D0 (en) | 1997-06-16 | 1997-08-20 | Unilever Plc | Production of detergent granulates |
| GB9712587D0 (en) * | 1997-06-16 | 1997-08-20 | Unilever Plc | Production of detergent granulates |
| GB9713748D0 (en) * | 1997-06-27 | 1997-09-03 | Unilever Plc | Production of detergent granulates |
| ATE371011T1 (de) * | 1997-07-14 | 2007-09-15 | Procter & Gamble | Verfahren zur herstellung eines waschmittels mit niedriger schüttdichte durch kontrollierte agglomeration in einem wirbelschichttrockner |
| JP2002507629A (ja) * | 1997-07-14 | 2002-03-12 | ザ、プロクター、エンド、ギャンブル、カンパニー | 粒子サイズによって塊状化を制御することによる低密度の洗剤組成物の作製方法 |
| WO1999003965A1 (fr) | 1997-07-15 | 1999-01-28 | The Procter & Gamble Company | Procede de production d'agglomerats detergents fortement actifs par injection d'une pate tensioactive en plusieurs etapes |
| US6440342B1 (en) | 1998-07-08 | 2002-08-27 | The Procter & Gamble Company | Process for making a low density detergent composition by controlling nozzle height in a fluid bed dryer |
| CN1094383C (zh) * | 1998-09-11 | 2002-11-20 | 自贡市化工研究设计院 | 沉淀水合二氧化硅的喷雾—流化床造粒方法 |
| ES2184523T3 (es) | 1998-10-26 | 2003-04-01 | Procter & Gamble | Procedimientos para obtener una composicion detergente granular que tiene un aspecto y solubilidad mejoradas. |
| GB9825563D0 (en) | 1998-11-20 | 1999-01-13 | Unilever Plc | Particulate laundry detergent compositions containing anionic surfactant granules |
| DE19855380A1 (de) * | 1998-12-01 | 2000-06-08 | Henkel Kgaa | Granulationsverfahren |
| DE19859778A1 (de) | 1998-12-23 | 2000-06-29 | Henkel Kgaa | Mehrphasiges Reinigungsmittel mit Naphthalinsulfonsäure-Formaldehyd-Kondensat |
| ES2250122T3 (es) | 1999-03-30 | 2006-04-16 | Unilever N.V. | Composicion detergente en polvo. |
| GB9927653D0 (en) | 1999-11-22 | 2000-01-19 | Unilever Plc | Process for preparing granular detergent compositions |
| GB0119708D0 (en) * | 2001-08-13 | 2001-10-03 | Unilever Plc | Process for the production of detergent granules |
| GB0119711D0 (en) * | 2001-08-13 | 2001-10-03 | Unilever Plc | Process for the production of detergent granules |
| DE102005005499A1 (de) * | 2005-02-04 | 2006-08-17 | Henkel Kgaa | Verfahren zur Herstellung von Wasch- oder Reinigungsmitteln |
| EP2123742A1 (fr) | 2008-05-14 | 2009-11-25 | The Procter and Gamble Company | Compositions de détergent solide pour lessive comprenant du sel de silicate à faible densité |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3425948A (en) * | 1966-01-03 | 1969-02-04 | Wyandotte Chemicals Corp | Composition and process for light-weight surfactant products |
| ZA72295B (en) * | 1971-02-01 | 1973-09-26 | Colgate Palmolive Co | Method for neutralization of detergent acid |
| GB1404317A (en) * | 1971-10-23 | 1975-08-28 | Bell Chemicals Pty Ltd | Manufacture of detergent powders |
| DD140987B1 (de) * | 1979-01-05 | 1982-06-30 | Manfred Mittelstrass | Kontinuierliches herstellungsverfahren granulierter wasch-und reinigungsmittel in wirbelschichtapparaten |
| RO88903A2 (fr) * | 1983-11-04 | 1986-06-30 | Intreprinderea De Detergenti"Dero",Ro | Procede et installation pour la fabrication des detergents granules |
| US4734224A (en) * | 1986-09-15 | 1988-03-29 | The Dial Corporation | Dry neutralization process for detergent slurries |
| GB8818613D0 (en) * | 1988-08-05 | 1988-09-07 | Paterson Zochonis Uk Ltd | Detergents |
| DE4232874A1 (de) * | 1992-09-30 | 1994-03-31 | Henkel Kgaa | Verfahren zur Herstellung von Tensidgranulaten |
-
1994
- 1994-08-05 GB GB9415904A patent/GB9415904D0/en active Pending
-
1995
- 1995-07-24 WO PCT/EP1995/002935 patent/WO1996004359A1/fr active IP Right Grant
- 1995-07-24 CN CN95194514A patent/CN1115403C/zh not_active Expired - Fee Related
- 1995-07-24 SK SK145-97A patent/SK282576B6/sk unknown
- 1995-07-24 EP EP95927721A patent/EP0775193A1/fr not_active Withdrawn
- 1995-07-24 AU AU31656/95A patent/AU702808B2/en not_active Ceased
- 1995-07-24 CZ CZ1997305A patent/CZ289884B6/cs not_active IP Right Cessation
- 1995-07-24 PL PL95318548A patent/PL181161B1/pl not_active IP Right Cessation
- 1995-07-24 BR BR9508505A patent/BR9508505A/pt not_active IP Right Cessation
- 1995-07-24 CA CA002195313A patent/CA2195313A1/fr not_active Abandoned
- 1995-07-24 HU HU9700357A patent/HU222907B1/hu not_active IP Right Cessation
- 1995-08-01 ZA ZA9506415A patent/ZA956415B/xx unknown
- 1995-08-09 TW TW084108296A patent/TW380161B/zh not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| AU702808B2 (en) | 1999-03-04 |
| HU222907B1 (hu) | 2003-12-29 |
| CN1115403C (zh) | 2003-07-23 |
| BR9508505A (pt) | 1998-05-26 |
| CA2195313A1 (fr) | 1996-02-15 |
| PL181161B1 (pl) | 2001-06-29 |
| EP0775193A1 (fr) | 1997-05-28 |
| HUT77715A (hu) | 1998-07-28 |
| TW380161B (en) | 2000-01-21 |
| ZA956415B (en) | 1997-02-03 |
| CZ289884B6 (cs) | 2002-04-17 |
| PL318548A1 (en) | 1997-06-23 |
| GB9415904D0 (en) | 1994-09-28 |
| CN1155297A (zh) | 1997-07-23 |
| AU3165695A (en) | 1996-03-04 |
| SK14597A3 (en) | 1997-07-09 |
| WO1996004359A1 (fr) | 1996-02-15 |
| MX9700863A (es) | 1997-09-30 |
| CZ30597A3 (en) | 1997-09-17 |
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