RU2551851C2 - Способ получения кристаллического твердого вещества из производных глицин-n,n-диуксусной кислоты - Google Patents
Способ получения кристаллического твердого вещества из производных глицин-n,n-диуксусной кислоты Download PDFInfo
- Publication number
- RU2551851C2 RU2551851C2 RU2012111127/04A RU2012111127A RU2551851C2 RU 2551851 C2 RU2551851 C2 RU 2551851C2 RU 2012111127/04 A RU2012111127/04 A RU 2012111127/04A RU 2012111127 A RU2012111127 A RU 2012111127A RU 2551851 C2 RU2551851 C2 RU 2551851C2
- Authority
- RU
- Russia
- Prior art keywords
- formula
- diacetic acid
- glycine
- crystalline solid
- compound
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C229/00—Compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C229/02—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton
- C07C229/04—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated
- C07C229/06—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having only one amino and one carboxyl group bound to the carbon skeleton
- C07C229/10—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having only one amino and one carboxyl group bound to the carbon skeleton the nitrogen atom of the amino group being further bound to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings
- C07C229/16—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having only one amino and one carboxyl group bound to the carbon skeleton the nitrogen atom of the amino group being further bound to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings to carbon atoms of hydrocarbon radicals substituted by amino or carboxyl groups, e.g. ethylenediamine-tetra-acetic acid, iminodiacetic acids
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05D—INORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
- C05D9/00—Other inorganic fertilisers
- C05D9/02—Other inorganic fertilisers containing trace elements
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C227/38—Separation; Purification; Stabilisation; Use of additives
- C07C227/40—Separation; Purification
- C07C227/42—Crystallisation
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/26—Organic compounds containing nitrogen
- C11D3/33—Amino carboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/32—Organic compounds containing nitrogen
- C11D7/3245—Aminoacids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
- C07B2200/00—Indexing scheme relating to specific properties of organic compounds
- C07B2200/13—Crystalline forms, e.g. polymorphs
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2602/00—Systems containing two condensed rings
- C07C2602/02—Systems containing two condensed rings the rings having only two atoms in common
- C07C2602/04—One of the condensed rings being a six-membered aromatic ring
- C07C2602/12—One of the condensed rings being a six-membered aromatic ring the other ring being at least seven-membered
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Crystallography & Structural Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Detergent Compositions (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102009038951A DE102009038951A1 (de) | 2009-08-26 | 2009-08-26 | Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität |
| DE102009038951.2 | 2009-08-26 | ||
| PCT/EP2010/005219 WO2011023382A2 (de) | 2009-08-26 | 2010-08-25 | Verfahren zur herstellung eines kristallinen feststoffes aus glycin-n, n-diessigsäure-derivaten mit hinreichend geringer hygroskopizität |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| RU2012111127A RU2012111127A (ru) | 2013-10-10 |
| RU2551851C2 true RU2551851C2 (ru) | 2015-05-27 |
Family
ID=43500504
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RU2012111127/04A RU2551851C2 (ru) | 2009-08-26 | 2010-08-25 | Способ получения кристаллического твердого вещества из производных глицин-n,n-диуксусной кислоты |
Country Status (17)
| Country | Link |
|---|---|
| US (2) | US9376649B2 (https=) |
| EP (1) | EP2470496B2 (https=) |
| JP (1) | JP5756107B2 (https=) |
| KR (1) | KR101755736B1 (https=) |
| CN (1) | CN102574775B (https=) |
| AU (1) | AU2010288872A1 (https=) |
| BR (1) | BR112012004179B1 (https=) |
| CA (1) | CA2771916C (https=) |
| DE (1) | DE102009038951A1 (https=) |
| ES (1) | ES2563323T5 (https=) |
| MX (1) | MX2012002244A (https=) |
| MY (1) | MY158464A (https=) |
| PL (1) | PL2470496T5 (https=) |
| RU (1) | RU2551851C2 (https=) |
| SG (1) | SG178352A1 (https=) |
| WO (1) | WO2011023382A2 (https=) |
| ZA (1) | ZA201202132B (https=) |
Families Citing this family (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102009038951A1 (de) * | 2009-08-26 | 2011-03-03 | Inprotec Ag | Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität |
| CA2776570A1 (en) | 2009-10-12 | 2011-04-21 | Basf Se | Process for the preparation of a powder comprising one or more complexing agent salts |
| DE102009060814A1 (de) | 2009-12-30 | 2011-07-07 | inprotec AG, 79423 | Verfahren zur Herstellung eines Feststoffs mit hinreichend geringer Hygroskopizität, der Glutaminsäure-N,N-diessigsäure (GLDA) oder ein Derivat davon enthält |
| PL2621892T3 (pl) * | 2010-09-27 | 2015-12-31 | Basf Se | Sposób wytwarzania granulatu zawierającego jedną lub większą liczbę soli kompleksotwórczych |
| US9227915B2 (en) * | 2011-05-03 | 2016-01-05 | Basf Se | Process for the preparation of a crystalline L-MGDA trialkali metal salt |
| GB2491619B (en) * | 2011-06-09 | 2014-10-01 | Pq Silicas Bv | Builder granules and process for their preparation |
| EP2931699A1 (en) | 2012-12-14 | 2015-10-21 | Akzo Nobel Chemicals International B.V. | Crystalline particles of glutamic acid n,n-diacetic acid |
| US9738594B2 (en) | 2012-12-14 | 2017-08-22 | Akzo Nobel Chemicals International B.V. | Crystalline particles of salts of glutamic acid N,N-diacetic acid |
| WO2015173157A2 (en) * | 2014-05-13 | 2015-11-19 | Akzo Nobel Chemicals International B.V. | Process to crystallize chelating agents |
| JP2019507671A (ja) * | 2015-12-11 | 2019-03-22 | ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ | 顆粒の製造方法 |
| CN109415662A (zh) * | 2016-06-20 | 2019-03-01 | 巴斯夫欧洲公司 | 粉末和颗粒以及制备该粉末和颗粒的方法 |
| WO2018153876A1 (en) * | 2017-02-24 | 2018-08-30 | Basf Se | Process for making solid methylglycine diacetate (mgda) alkali metal salt, and solid particles |
| US10836709B2 (en) | 2017-07-07 | 2020-11-17 | Nouryon Chemicals International B.V. | Process to prepare a solid composition of an amino acid diacetic acid |
| JP2021526523A (ja) | 2018-05-30 | 2021-10-07 | ビーエイエスエフ・ソシエタス・エウロパエアＢａｓｆ Ｓｅ | 固体メチルグリシンジアセテート（ｍｇｄａ）アルカリ金属塩を製造する方法、及び固体粒子 |
| CA3104879A1 (en) | 2018-06-26 | 2020-01-02 | Juul Labs, Inc. | Devices and methods for cessation of nicotine addiction |
| WO2020127349A1 (en) | 2018-12-21 | 2020-06-25 | Nouryon Chemicals International B.V. | Crumbly phase composition of methylglycine n,n diacetic acid |
| KR102771094B1 (ko) | 2019-11-21 | 2025-02-24 | (주)아모레퍼시픽 | 고함량의 락테이트 금속염 및 실리콘계 오일의 혼합물을 포함하는 w/s형 화장료 조성물 |
| EP4168388A1 (en) | 2020-06-19 | 2023-04-26 | Nouryon Chemicals International B.V. | Process to prepare a co granule of methylglycine n,n diacetic acid salts employing a crumbly phase composition of methylglycine n,n diacetic acid salts |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE19649681A1 (de) * | 1996-11-29 | 1998-06-04 | Basf Ag | Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität |
| RU2305604C2 (ru) * | 2001-04-13 | 2007-09-10 | Уреа Касале С.А. | Гранулятор с псевдоожиженным слоем и используемый в нем распылитель |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3932316A (en) | 1974-11-13 | 1976-01-13 | The Procter & Gamble Company | Free flowing detergent compositions containing benzoate salts |
| JPH0678225B2 (ja) | 1985-11-27 | 1994-10-05 | 株式会社林原生物化学研究所 | 脱水医薬品とその製造方法 |
| DE4319935A1 (de) * | 1993-06-16 | 1994-12-22 | Basf Ag | Verwendung von Glycin-N,N-diessigsäure-Derivaten als Komplexbildner für Erdalkali- und Schwermetallionen |
| JP4711471B2 (ja) | 1996-07-05 | 2011-06-29 | 三菱商事フードテック株式会社 | 結晶マルチトール及びそれを含有する含蜜結晶の製造方法 |
| DE102004032320A1 (de) * | 2004-07-02 | 2006-01-19 | Basf Ag | Mischpulver oder Mischgranulat auf Basis von MGDA |
| MX2009013320A (es) * | 2007-07-03 | 2010-01-20 | Basf Se | Proceso para producir un solido de flujo libre y estable al almacenamiento que comprende esencialmente acido a-alanina-n, n-diacetico y/o uno o mas derivados de acido a-alanina-n, n-diacetico. |
| PT3061744T (pt) * | 2008-04-01 | 2018-06-19 | Unilever Nv | Preparação de grânulos de fluxo livre de ácido metilglicina diacético |
| FR2935383B1 (fr) * | 2008-08-26 | 2010-10-01 | Pancosma Sa Pour L Ind Des Pro | Procede et dispositif pour la fabrication de complexes organometalliques en poudre. |
| JP5745507B2 (ja) * | 2009-05-20 | 2015-07-08 | ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ | グリシン−ｎ，ｎ−二酢酸の１種以上の誘導体および／またはグルタミン−ｎ，ｎ−二酢酸の１種以上の誘導体を含む粉末ならびにメチルグリシン−ｎ，ｎ−二酢酸三ナトリウム塩粉末の調製方法 |
| DE102009038951A1 (de) * | 2009-08-26 | 2011-03-03 | Inprotec Ag | Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität |
| CA2776570A1 (en) * | 2009-10-12 | 2011-04-21 | Basf Se | Process for the preparation of a powder comprising one or more complexing agent salts |
| GB2491619B (en) * | 2011-06-09 | 2014-10-01 | Pq Silicas Bv | Builder granules and process for their preparation |
-
2009
- 2009-08-26 DE DE102009038951A patent/DE102009038951A1/de not_active Withdrawn
-
2010
- 2010-08-25 US US13/391,397 patent/US9376649B2/en active Active
- 2010-08-25 MX MX2012002244A patent/MX2012002244A/es active IP Right Grant
- 2010-08-25 AU AU2010288872A patent/AU2010288872A1/en not_active Abandoned
- 2010-08-25 SG SG2012009312A patent/SG178352A1/en unknown
- 2010-08-25 ES ES10747834T patent/ES2563323T5/es active Active
- 2010-08-25 MY MYPI2012000735A patent/MY158464A/en unknown
- 2010-08-25 RU RU2012111127/04A patent/RU2551851C2/ru active
- 2010-08-25 CA CA2771916A patent/CA2771916C/en not_active Expired - Fee Related
- 2010-08-25 BR BR112012004179A patent/BR112012004179B1/pt active IP Right Grant
- 2010-08-25 WO PCT/EP2010/005219 patent/WO2011023382A2/de not_active Ceased
- 2010-08-25 KR KR1020127007333A patent/KR101755736B1/ko not_active Expired - Fee Related
- 2010-08-25 PL PL10747834.9T patent/PL2470496T5/pl unknown
- 2010-08-25 EP EP10747834.9A patent/EP2470496B2/de active Active
- 2010-08-25 CN CN201080037900.3A patent/CN102574775B/zh active Active
- 2010-08-25 JP JP2012525929A patent/JP5756107B2/ja active Active
-
2012
- 2012-03-22 ZA ZA2012/02132A patent/ZA201202132B/en unknown
-
2016
- 2016-04-12 US US15/096,678 patent/US9751829B2/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE19649681A1 (de) * | 1996-11-29 | 1998-06-04 | Basf Ag | Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität |
| RU2305604C2 (ru) * | 2001-04-13 | 2007-09-10 | Уреа Касале С.А. | Гранулятор с псевдоожиженным слоем и используемый в нем распылитель |
Also Published As
| Publication number | Publication date |
|---|---|
| MY158464A (en) | 2016-10-14 |
| MX2012002244A (es) | 2012-03-29 |
| PL2470496T3 (pl) | 2016-06-30 |
| US20120149936A1 (en) | 2012-06-14 |
| ES2563323T5 (es) | 2024-10-16 |
| CN102574775B (zh) | 2014-09-24 |
| JP2013503119A (ja) | 2013-01-31 |
| KR20120089470A (ko) | 2012-08-10 |
| WO2011023382A2 (de) | 2011-03-03 |
| AU2010288872A1 (en) | 2012-03-08 |
| JP5756107B2 (ja) | 2015-07-29 |
| EP2470496A2 (de) | 2012-07-04 |
| CA2771916A1 (en) | 2011-03-03 |
| US20160221930A1 (en) | 2016-08-04 |
| KR101755736B1 (ko) | 2017-07-07 |
| DE102009038951A1 (de) | 2011-03-03 |
| BR112012004179A2 (pt) | 2016-03-29 |
| CN102574775A (zh) | 2012-07-11 |
| WO2011023382A3 (de) | 2011-05-12 |
| ZA201202132B (en) | 2013-05-29 |
| US9751829B2 (en) | 2017-09-05 |
| CA2771916C (en) | 2017-07-25 |
| EP2470496B1 (de) | 2016-01-06 |
| ES2563323T3 (es) | 2016-03-14 |
| SG178352A1 (en) | 2012-03-29 |
| BR112012004179B1 (pt) | 2018-09-11 |
| PL2470496T5 (pl) | 2024-07-15 |
| RU2012111127A (ru) | 2013-10-10 |
| EP2470496B2 (de) | 2024-03-27 |
| US9376649B2 (en) | 2016-06-28 |
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