RU2016145616A - Способ получения смоляных систем акриловых порошковых покрытий - Google Patents
Способ получения смоляных систем акриловых порошковых покрытий Download PDFInfo
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- 239000000843 powder Substances 0.000 title claims 8
- 229920005989 resin Polymers 0.000 title claims 5
- 239000011347 resin Substances 0.000 title claims 5
- 238000004519 manufacturing process Methods 0.000 title 1
- 238000000034 method Methods 0.000 claims 15
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims 8
- 239000011248 coating agent Substances 0.000 claims 6
- 238000000576 coating method Methods 0.000 claims 6
- 239000000178 monomer Substances 0.000 claims 6
- 239000002245 particle Substances 0.000 claims 6
- 230000002209 hydrophobic effect Effects 0.000 claims 5
- 239000004593 Epoxy Substances 0.000 claims 4
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims 4
- 239000000377 silicon dioxide Substances 0.000 claims 4
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 claims 3
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 claims 3
- 239000008199 coating composition Substances 0.000 claims 3
- 239000003999 initiator Substances 0.000 claims 3
- 229910052809 inorganic oxide Inorganic materials 0.000 claims 3
- 239000000203 mixture Substances 0.000 claims 3
- 239000003125 aqueous solvent Substances 0.000 claims 2
- MLFHJEHSLIIPHL-UHFFFAOYSA-N isoamyl acetate Chemical compound CC(C)CCOC(C)=O MLFHJEHSLIIPHL-UHFFFAOYSA-N 0.000 claims 2
- 239000000758 substrate Substances 0.000 claims 2
- COXCGWKSEPPDAA-UHFFFAOYSA-N 2,4-dimethylpentanenitrile Chemical compound CC(C)CC(C)C#N COXCGWKSEPPDAA-UHFFFAOYSA-N 0.000 claims 1
- XMNIXWIUMCBBBL-UHFFFAOYSA-N 2-(2-phenylpropan-2-ylperoxy)propan-2-ylbenzene Chemical compound C=1C=CC=CC=1C(C)(C)OOC(C)(C)C1=CC=CC=C1 XMNIXWIUMCBBBL-UHFFFAOYSA-N 0.000 claims 1
- IFXDUNDBQDXPQZ-UHFFFAOYSA-N 2-methylbutan-2-yl 2-ethylhexaneperoxoate Chemical compound CCCCC(CC)C(=O)OOC(C)(C)CC IFXDUNDBQDXPQZ-UHFFFAOYSA-N 0.000 claims 1
- RCEJCSULJQNRQQ-UHFFFAOYSA-N 2-methylbutanenitrile Chemical compound CCC(C)C#N RCEJCSULJQNRQQ-UHFFFAOYSA-N 0.000 claims 1
- 239000004342 Benzoyl peroxide Substances 0.000 claims 1
- OMPJBNCRMGITSC-UHFFFAOYSA-N Benzoylperoxide Chemical compound C=1C=CC=CC=1C(=O)OOC(=O)C1=CC=CC=C1 OMPJBNCRMGITSC-UHFFFAOYSA-N 0.000 claims 1
- DKPFZGUDAPQIHT-UHFFFAOYSA-N Butyl acetate Natural products CCCCOC(C)=O DKPFZGUDAPQIHT-UHFFFAOYSA-N 0.000 claims 1
- NTIZESTWPVYFNL-UHFFFAOYSA-N Methyl isobutyl ketone Chemical compound CC(C)CC(C)=O NTIZESTWPVYFNL-UHFFFAOYSA-N 0.000 claims 1
- UIHCLUNTQKBZGK-UHFFFAOYSA-N Methyl isobutyl ketone Natural products CCC(C)C(C)=O UIHCLUNTQKBZGK-UHFFFAOYSA-N 0.000 claims 1
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 claims 1
- 230000002378 acidificating effect Effects 0.000 claims 1
- 239000000956 alloy Substances 0.000 claims 1
- 229910045601 alloy Inorganic materials 0.000 claims 1
- 229910052782 aluminium Inorganic materials 0.000 claims 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims 1
- 235000019400 benzoyl peroxide Nutrition 0.000 claims 1
- 239000002131 composite material Substances 0.000 claims 1
- 238000006482 condensation reaction Methods 0.000 claims 1
- 239000003431 cross linking reagent Substances 0.000 claims 1
- 238000007580 dry-mixing Methods 0.000 claims 1
- 238000005242 forging Methods 0.000 claims 1
- VOZRXNHHFUQHIL-UHFFFAOYSA-N glycidyl methacrylate Chemical compound CC(=C)C(=O)OCC1CO1 VOZRXNHHFUQHIL-UHFFFAOYSA-N 0.000 claims 1
- 238000000227 grinding Methods 0.000 claims 1
- CATSNJVOTSVZJV-UHFFFAOYSA-N heptan-2-one Chemical compound CCCCCC(C)=O CATSNJVOTSVZJV-UHFFFAOYSA-N 0.000 claims 1
- FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 claims 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims 1
- 229940117955 isoamyl acetate Drugs 0.000 claims 1
- 229910052751 metal Inorganic materials 0.000 claims 1
- 239000002184 metal Substances 0.000 claims 1
- 229910044991 metal oxide Inorganic materials 0.000 claims 1
- 150000004706 metal oxides Chemical class 0.000 claims 1
- ZQMHJBXHRFJKOT-UHFFFAOYSA-N methyl 2-[(1-methoxy-2-methyl-1-oxopropan-2-yl)diazenyl]-2-methylpropanoate Chemical compound COC(=O)C(C)(C)N=NC(C)(C)C(=O)OC ZQMHJBXHRFJKOT-UHFFFAOYSA-N 0.000 claims 1
- 238000002156 mixing Methods 0.000 claims 1
- YKYONYBAUNKHLG-UHFFFAOYSA-N n-Propyl acetate Natural products CCCOC(C)=O YKYONYBAUNKHLG-UHFFFAOYSA-N 0.000 claims 1
- 150000003961 organosilicon compounds Chemical class 0.000 claims 1
- RPQRDASANLAFCM-UHFFFAOYSA-N oxiran-2-ylmethyl prop-2-enoate Chemical compound C=CC(=O)OCC1CO1 RPQRDASANLAFCM-UHFFFAOYSA-N 0.000 claims 1
- 229920000058 polyacrylate Polymers 0.000 claims 1
- 239000002952 polymeric resin Substances 0.000 claims 1
- 230000000379 polymerizing effect Effects 0.000 claims 1
- 229940090181 propyl acetate Drugs 0.000 claims 1
- 150000004760 silicates Chemical class 0.000 claims 1
- OPQYOFWUFGEMRZ-UHFFFAOYSA-N tert-butyl 2,2-dimethylpropaneperoxoate Chemical compound CC(C)(C)OOC(=O)C(C)(C)C OPQYOFWUFGEMRZ-UHFFFAOYSA-N 0.000 claims 1
- WYKYCHHWIJXDAO-UHFFFAOYSA-N tert-butyl 2-ethylhexaneperoxoate Chemical compound CCCCC(CC)C(=O)OOC(C)(C)C WYKYCHHWIJXDAO-UHFFFAOYSA-N 0.000 claims 1
- PFBLRDXPNUJYJM-UHFFFAOYSA-N tert-butyl 2-methylpropaneperoxoate Chemical compound CC(C)C(=O)OOC(C)(C)C PFBLRDXPNUJYJM-UHFFFAOYSA-N 0.000 claims 1
- GJBRNHKUVLOCEB-UHFFFAOYSA-N tert-butyl benzenecarboperoxoate Chemical compound CC(C)(C)OOC(=O)C1=CC=CC=C1 GJBRNHKUVLOCEB-UHFFFAOYSA-N 0.000 claims 1
- -1 tert-butyl peroxyethyl acetate Chemical compound 0.000 claims 1
- CIHOLLKRGTVIJN-UHFFFAOYSA-N tert‐butyl hydroperoxide Chemical compound CC(C)(C)OO CIHOLLKRGTVIJN-UHFFFAOYSA-N 0.000 claims 1
- NQPDZGIKBAWPEJ-UHFFFAOYSA-N valeric acid Chemical compound CCCCC(O)=O NQPDZGIKBAWPEJ-UHFFFAOYSA-N 0.000 claims 1
- 239000008096 xylene Substances 0.000 claims 1
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/03—Powdery paints
- C09D5/033—Powdery paints characterised by the additives
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- C08F2/00—Processes of polymerisation
- C08F2/04—Polymerisation in solution
- C08F2/06—Organic solvent
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- C08F2/00—Processes of polymerisation
- C08F2/44—Polymerisation in the presence of compounding ingredients, e.g. plasticisers, dyestuffs, fillers
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- C08F20/00—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride, ester, amide, imide or nitrile thereof
- C08F20/02—Monocarboxylic acids having less than ten carbon atoms, Derivatives thereof
- C08F20/10—Esters
- C08F20/12—Esters of monohydric alcohols or phenols
- C08F20/16—Esters of monohydric alcohols or phenols of phenols or of alcohols containing two or more carbon atoms
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- C08F212/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring
- C08F212/02—Monomers containing only one unsaturated aliphatic radical
- C08F212/04—Monomers containing only one unsaturated aliphatic radical containing one ring
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- C08F220/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride ester, amide, imide or nitrile thereof
- C08F220/02—Monocarboxylic acids having less than ten carbon atoms; Derivatives thereof
- C08F220/10—Esters
- C08F220/12—Esters of monohydric alcohols or phenols
- C08F220/16—Esters of monohydric alcohols or phenols of phenols or of alcohols containing two or more carbon atoms
- C08F220/18—Esters of monohydric alcohols or phenols of phenols or of alcohols containing two or more carbon atoms with acrylic or methacrylic acids
- C08F220/1811—C10or C11-(Meth)acrylate, e.g. isodecyl (meth)acrylate, isobornyl (meth)acrylate or 2-naphthyl (meth)acrylate
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- C08F220/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride ester, amide, imide or nitrile thereof
- C08F220/02—Monocarboxylic acids having less than ten carbon atoms; Derivatives thereof
- C08F220/10—Esters
- C08F220/26—Esters containing oxygen in addition to the carboxy oxygen
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- C08F220/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride ester, amide, imide or nitrile thereof
- C08F220/02—Monocarboxylic acids having less than ten carbon atoms; Derivatives thereof
- C08F220/10—Esters
- C08F220/26—Esters containing oxygen in addition to the carboxy oxygen
- C08F220/32—Esters containing oxygen in addition to the carboxy oxygen containing epoxy radicals
- C08F220/325—Esters containing oxygen in addition to the carboxy oxygen containing epoxy radicals containing glycidyl radical, e.g. glycidyl (meth)acrylate
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- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
- C09D133/04—Homopolymers or copolymers of esters
- C09D133/06—Homopolymers or copolymers of esters of esters containing only carbon, hydrogen and oxygen, the oxygen atom being present only as part of the carboxyl radical
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Claims (15)
1. Способ получения смоляной системы акрилового порошкового покрытия, включающий в себя полимеризацию в растворе по меньшей мере одного акрилового мономера в неводном растворителе в присутствии гидрофобной субмикронной частицы и инициатора.
2. Способ по п. 1, где по меньшей мере один акриловый мономер выбирают из имеющих эпоксидную функциональность, гидроксильную функциональность или кислую функциональность мономеров или их сочетаний.
3. Способ по любому из пп. 1 или 2, где по меньшей мере один мономер имеет эпоксидную функциональность и выбран из глицидилметакрилата или глицидилакрилата.
4. Способ по любому из пп. 1-3, где по меньшей мере один мономер включен в количестве от примерно 10 мас. % до примерно 40 мас. % в расчете на все мономеры, подлежащие сополимеризации.
5. Способ по любому из пп. 1-4, где одна или более акриловых полимерных смоляных систем имеет эпоксидную функциональность и имеет эквивалентную массу по эпоксиду (EEW) от примерно 250 до примерно 750.
6. Способ по любому из пп. 1-5, где неводный растворитель выбирают из группы, состоящей из толуола, ксилола, этилацетата, бутилацетата, пропилацетата, метиламилкетона, изоамилацетата, метилэтилкетона, метилизобутилкетона и их смесей.
7. Способ по любому из пп. 1-6, где одна или более гидрофобных субмикронных частиц, каждая, содержат неорганический оксид и одно или более кремнийорганических соединений.
8. Способ по п. 7, где частицу неорганического оксида выбирают из группы, состоящей из диоксида кремния, тонкодисперсного диоксида кремния, оксидов металлов, силикатов, органо-неорганических оксидных композитов и их смесей.
9. Способ по любому из пп. 1-8, где одна или более гидрофобных субмикронных частиц представляет собой обработанный тонкодисперсный диоксид кремния, образованный продуктом реакции конденсации тонкодисперсного диоксида кремния, обработанного диметилдигалогенсиланом.
10. Способ по любому из пп. 1-9, где одна или более гидрофобных субмикронных частиц присутствует в смоляной системе порошкового покрытия в диапазоне от примерно 0,01 мас. % до примерно 2,0 мас. % в расчете на суммарную массу смоляной системы порошкового покрытия.
11. Способ по любому из пп. 1-10, где один или более инициаторов представляет собой термический или радикальный инициатор, выбранный из группы, состоящей из трет-бутилперокси-2-этилгексаноата, трет-амилперокси-2-этилгексаноата, трет-бутилпероксидиэтилацетата, трет-бутилпероксиизобутирата, бензоилпероксида, т-бутилгидропероксида, трет-бутилпербензоата, пероксида кумола, диметилазобисизобутирата, 2,2ʹ-азобис(2-метилбутиронитрила), 2,2ʹ-азобис(2,4-диметил-пентаннитрила), 2,2ʹ-азобис(2-метилпропаннитрила), т-бутилпероксипивалата их смесей.
12. Способ получения композиции порошкового покрытия, включающий в себя смешивание смоляной системы порошкового покрытия, полученной согласно способу по любому из пп. 1-11, с одним или более сшивающими агентами.
13. Способ по п. 12, дополнительной включающий в себя сухое смешивание, измельчение и экструдирование полученной в результате акриловой композиции порошкового покрытия, содержащей гидрофобные субмикронные частицы.
14. Покрытие на металлической подложке, содержащее композицию порошкового покрытия, полученную согласно способу по пп. 12 или 13.
15. Покрытие по п. 14, где подложка содержит алюминий или ковочный сплав.
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201461986433P | 2014-04-30 | 2014-04-30 | |
| US61/986,433 | 2014-04-30 | ||
| EP14176750 | 2014-07-11 | ||
| EP14176750.9 | 2014-07-11 | ||
| PCT/EP2015/059118 WO2015165860A1 (en) | 2014-04-30 | 2015-04-28 | Process for making acrylic powder coating resin systems |
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| RU2016145616A3 RU2016145616A3 (ru) | 2018-11-30 |
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| EP (1) | EP3137510B1 (ru) |
| JP (1) | JP6442528B2 (ru) |
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| CN (1) | CN106232628B (ru) |
| AU (1) | AU2015252211B2 (ru) |
| BR (1) | BR112016024670A2 (ru) |
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| RU (1) | RU2687075C2 (ru) |
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| KR102002359B1 (ko) | 2017-05-26 | 2019-07-23 | 케이에스케미칼 주식회사 | 부착성과 경화성이 개선된 분체도료용 레벨링제 조성물 및 그 제조방법 |
| CN110760916B (zh) * | 2019-11-18 | 2022-04-05 | 和县科嘉阀门铸造有限公司 | 一种提高镁合金阀门耐蚀性的方法 |
| WO2021215252A1 (ja) * | 2020-04-24 | 2021-10-28 | Dic株式会社 | 粉体塗料用樹脂組成物、粉体塗料、該塗料の塗膜を有する物品 |
| CN117070134B (zh) * | 2023-10-07 | 2023-12-26 | 佛山市南海嘉多彩粉末涂料有限公司 | 一种耐腐蚀户外消光粉末涂料组合物 |
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| US5021297A (en) * | 1988-12-02 | 1991-06-04 | Ppg Industries, Inc. | Process for coating plastic substrates with powder coating compositions |
| US5034432A (en) * | 1988-12-29 | 1991-07-23 | Nippon Paint Co., Ltd. | Powder coatings |
| US5066733A (en) * | 1989-04-03 | 1991-11-19 | Ppg Industries, Inc. | Chip resistant coatings and methods of application |
| JP3276131B2 (ja) * | 1995-01-26 | 2002-04-22 | 日本カーバイド工業株式会社 | 粉体塗料及びその製造方法 |
| US6309572B1 (en) * | 1998-06-04 | 2001-10-30 | Mitsubishi Gas Chemical Company, Inc. | Process for the preparation of powder coating composition |
| DE60033403T2 (de) * | 1999-07-30 | 2007-10-31 | Ppg Industries Ohio, Inc. | Beschichtungszusammensetzungen mit verbesserter kratzfestigkeit, beschichtete oberfläche und verfahren zu deren herstellung |
| US20040191498A1 (en) * | 2003-03-27 | 2004-09-30 | Daniela White | Polymerizable modified particles and methods of using the same |
| JP2004359796A (ja) * | 2003-06-04 | 2004-12-24 | Nippon Synthetic Chem Ind Co Ltd:The | アクリル系樹脂エマルジョンの製造方法 |
| JP2005220208A (ja) * | 2004-02-05 | 2005-08-18 | Asahi Kasei Chemicals Corp | 硬化性組成物の製造方法 |
| JP2006028304A (ja) * | 2004-07-14 | 2006-02-02 | Mitsubishi Gas Chem Co Inc | 粉体塗料の製造方法 |
| US20060058417A1 (en) * | 2004-09-14 | 2006-03-16 | Brandenburg Charles J | Materials leading to improved dental composites and dental composites made therefrom |
| CN100400590C (zh) * | 2005-09-15 | 2008-07-09 | 复旦大学 | 一种高固低粘的纳米复合丙烯酸树脂及其涂层的制备方法 |
| JP2007091795A (ja) * | 2005-09-27 | 2007-04-12 | Dainippon Ink & Chem Inc | 艶消し粉体塗料用樹脂組成物 |
| DE602006018346D1 (de) * | 2005-09-30 | 2010-12-30 | Kaneka Corp | Härtbare zusammensetzung mit verbesserter härtung und lagerstabilität |
| CN1318459C (zh) * | 2005-11-30 | 2007-05-30 | 中国林业科学研究院林产化学工业研究所 | 纳米二氧化硅－丙烯酸酯高分子微球材料的制备方法 |
| JP4094049B2 (ja) * | 2007-09-28 | 2008-06-04 | 三井化学株式会社 | アクリル系熱硬化性粉体塗料組成物 |
| EP2048116A1 (en) * | 2007-10-09 | 2009-04-15 | ChemIP B.V. | Dispersion of nanoparticles in organic solvents |
| DE602008002046D1 (de) * | 2008-01-29 | 2010-09-16 | Rohm & Haas | Acryl-Beschichtungspulver mit hydrophoben Partikeln und Pulverbeschichtungen daraus mit Filiformkorrosionsbeständigkeit |
| DE602008002402D1 (de) * | 2008-03-04 | 2010-10-14 | Rohm & Haas | Lverbeschichtungen daraus mit filiformkorrosionsbeständigkeit |
| CN101358097A (zh) * | 2008-09-19 | 2009-02-04 | 河北科技大学 | 纳米复合粉末涂料及其分散聚合制造方法 |
| RU2404218C1 (ru) * | 2009-06-29 | 2010-11-20 | Государственное образовательное учреждение высшего профессионального образования "Санкт-Петербургский государственный технологический институт (технический университет)" | Порошковая уф-отверждаемая композиция для лаковых покрытий |
| US8513342B2 (en) * | 2009-10-16 | 2013-08-20 | University of Pittsburgh—of the Commonwealth System of Higher Education | Durable superhydrophobic coatings |
| US8586273B2 (en) * | 2009-11-20 | 2013-11-19 | Mitsui Chemicals, Inc. | Binder resin for toner, toner and method for producing same |
| JP6002673B2 (ja) * | 2010-11-18 | 2016-10-05 | ビーエーエスエフ コーティングス ゲゼルシャフト ミット ベシュレンクテル ハフツングＢＡＳＦ Ｃｏａｔｉｎｇｓ ＧｍｂＨ | ポリウレタンコーティング剤、これから製造される、艶消し表面を有する多層塗膜、ならびにその多層塗膜の製造方法 |
| CN103059323B (zh) * | 2011-10-21 | 2014-11-05 | 北京化工大学 | 一种高透明紫外阻隔仿陶瓷纳米复合膜材料的制备方法 |
| JP6072660B2 (ja) * | 2013-09-27 | 2017-02-01 | 第一工業製薬株式会社 | 硬化性樹脂組成物およびハードコート用組成物 |
| SG11201606963XA (en) * | 2014-02-27 | 2016-09-29 | Akzo Nobel Coatings Int Bv | Acrylic resins and powder coating compositions and powder coated substrates including the same |
| WO2017051718A1 (ja) * | 2015-09-24 | 2017-03-30 | 関西ペイント株式会社 | アクリル樹脂被覆シリカ粒子分散体の製造方法 |
-
2015
- 2015-04-28 MX MX2016014022A patent/MX2016014022A/es unknown
- 2015-04-28 AU AU2015252211A patent/AU2015252211B2/en not_active Ceased
- 2015-04-28 ES ES15717922.7T patent/ES2678393T3/es active Active
- 2015-04-28 EP EP15717922.7A patent/EP3137510B1/en active Active
- 2015-04-28 RU RU2016145616A patent/RU2687075C2/ru active
- 2015-04-28 KR KR1020167031106A patent/KR102330128B1/ko active IP Right Grant
- 2015-04-28 MY MYPI2016703824A patent/MY179360A/en unknown
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- 2015-04-28 US US15/307,131 patent/US20170044377A1/en not_active Abandoned
- 2015-04-28 WO PCT/EP2015/059118 patent/WO2015165860A1/en active Application Filing
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- 2015-04-28 JP JP2016564315A patent/JP6442528B2/ja not_active Expired - Fee Related
- 2015-04-28 PL PL15717922T patent/PL3137510T3/pl unknown
- 2015-04-28 CN CN201580020475.XA patent/CN106232628B/zh active Active
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| CN106232628A (zh) | 2016-12-14 |
| PL3137510T3 (pl) | 2018-11-30 |
| WO2015165860A1 (en) | 2015-11-05 |
| RU2687075C2 (ru) | 2019-05-07 |
| CA2946227A1 (en) | 2015-11-05 |
| BR112016024670A2 (pt) | 2017-08-15 |
| EP3137510B1 (en) | 2018-06-06 |
| AU2015252211B2 (en) | 2018-08-30 |
| JP6442528B2 (ja) | 2018-12-19 |
| KR102330128B1 (ko) | 2021-11-23 |
| KR20170002423A (ko) | 2017-01-06 |
| SG11201608931QA (en) | 2016-11-29 |
| US20170044377A1 (en) | 2017-02-16 |
| JP2017518402A (ja) | 2017-07-06 |
| ES2678393T3 (es) | 2018-08-10 |
| AU2015252211A1 (en) | 2016-11-03 |
| CN106232628B (zh) | 2018-11-06 |
| MY179360A (en) | 2020-11-05 |
| EP3137510A1 (en) | 2017-03-08 |
| MX2016014022A (es) | 2017-01-09 |
| RU2016145616A3 (ru) | 2018-11-30 |
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