RU2002114864A - Поглощающий материал и способ его изготовления - Google Patents
Поглощающий материал и способ его изготовленияInfo
- Publication number
- RU2002114864A RU2002114864A RU2002114864/15A RU2002114864A RU2002114864A RU 2002114864 A RU2002114864 A RU 2002114864A RU 2002114864/15 A RU2002114864/15 A RU 2002114864/15A RU 2002114864 A RU2002114864 A RU 2002114864A RU 2002114864 A RU2002114864 A RU 2002114864A
- Authority
- RU
- Russia
- Prior art keywords
- weight
- oxide
- boehmite
- magnesium
- peptized
- Prior art date
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
- B01J20/28054—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
- B01J20/28057—Surface area, e.g. B.E.T specific surface area
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/04—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising compounds of alkali metals, alkaline earth metals or magnesium
- B01J20/041—Oxides or hydroxides
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/06—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising oxides or hydroxides of metals not provided for in group B01J20/04
- B01J20/08—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising oxides or hydroxides of metals not provided for in group B01J20/04 comprising aluminium oxide or hydroxide; comprising bauxite
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
- B01J20/28054—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their surface properties or porosity
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/30—Processes for preparing, regenerating, or reactivating
- B01J20/3007—Moulding, shaping or extruding
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/30—Processes for preparing, regenerating, or reactivating
- B01J20/3078—Thermal treatment, e.g. calcining or pyrolizing
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G25/00—Refining of hydrocarbon oils in the absence of hydrogen, with solid sorbents
- C10G25/003—Specific sorbent material, not covered by C10G25/02 or C10G25/03
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2220/00—Aspects relating to sorbent materials
- B01J2220/40—Aspects relating to the composition of sorbent or filter aid materials
- B01J2220/42—Materials comprising a mixture of inorganic materials
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S423/00—Chemistry of inorganic compounds
- Y10S423/09—Reaction techniques
- Y10S423/14—Ion exchange; chelation or liquid/liquid ion extraction
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Analytical Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- General Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
- Compositions Of Oxide Ceramics (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
- Treating Waste Gases (AREA)
Claims (10)
1. Поглощающий материал, содержащий от 50 до 96% по весу оксида алюминия и от 50 до 4% по весу оксидов щелочноземельных металлов, выбранных из оксида кальция и оксида магния, причем весовое отношение оксида кальция к оксиду магния составляет от 90:10 до 50:50, при этом указанный материал имеет BET площадь поверхности, составляющую, по меньшей мере, 100 м2/г.
2. Материал по п.1, отличающийся тем, что он имеет кажущуюся пористость от 60 до 80%.
3. Материал по п.1, отличающийся тем, что он содержит менее 1% включений других металлов или оксидов металлов.
4. Способ изготовления поглощающего материала, отличающийся тем, что он включает в себя следующие операции:
a) образование пептизированной водной суспензии, которая содержит от 50 до 97% по весу бемита, от 50 до 3% по весу смеси карбоната кальция и карбоната магния, причем относительное весовое отношение карбоната кальция к карбонату магния составляет от 10:1 до 50:50, при этом веса бемита и смеси карбонатов определяют в пересчете на вес твердых веществ в суспензии;
b) формирование изделий желательной формы из пептизированной суспензии; и
c) сушка для удаления воды и затем обжиг полученных изделий при температуре от 650 до 850°С.
5. Способ по п.4, отличающийся тем, что сушку проводят при температуре ниже 150°С.
6. Способ по п.4, отличающийся тем, что обжиг продолжают до тех пор, пока не будет дальнейшей потери веса материала.
7. Способ по п.4, отличающийся тем, что время обжига устанавливают таким образом, что готовый продукт имеет площадь поверхности, составляющую по меньшей мере 200 м2/г.
8. Способ по п.4, отличающийся тем, что бемит пептизируют с использованием органической кислоты.
9. Способ по п.8, отличающийся тем, что пептизирующей кислотой является муравьиная кислота.
10. Способ по п.4, отличающийся тем, что компоненты вводят в таком количестве, чтобы получить состав готового продукта, который содержит от 50 до 96% по весу оксида алюминия и 50-4% по весу оксидов щелочноземельных металлов, выбранных из оксида кальция и оксида магния, причем весовое отношение оксида кальция к оксиду магния составляет от 10:1 до 50:50.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US09/476,898 | 2000-01-03 | ||
| US09/476,898 US6207612B1 (en) | 2000-01-03 | 2000-01-03 | Removal of impurities from hydrocarbon streams |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| RU2218210C1 RU2218210C1 (ru) | 2003-12-10 |
| RU2002114864A true RU2002114864A (ru) | 2004-02-20 |
Family
ID=23893699
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RU2002114864/15A RU2218210C1 (ru) | 2000-01-03 | 2000-12-27 | Поглощающий материал и способ его изготовления |
Country Status (15)
| Country | Link |
|---|---|
| US (1) | US6207612B1 (ru) |
| EP (1) | EP1261422B1 (ru) |
| JP (1) | JP3842648B2 (ru) |
| KR (1) | KR100464474B1 (ru) |
| CN (1) | CN1143731C (ru) |
| AR (1) | AR026785A1 (ru) |
| AU (1) | AU755910B2 (ru) |
| BR (1) | BR0016893A (ru) |
| CA (1) | CA2389991C (ru) |
| DE (1) | DE60011944T2 (ru) |
| ES (1) | ES2223643T3 (ru) |
| MX (1) | MXPA02006653A (ru) |
| NO (1) | NO326365B1 (ru) |
| RU (1) | RU2218210C1 (ru) |
| WO (1) | WO2001049408A1 (ru) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6372124B2 (en) * | 2000-01-03 | 2002-04-16 | Saint-Gobain Norpro Corporation | Removal of impurities from hydrocarbon streams |
| JP2001219056A (ja) * | 2000-02-14 | 2001-08-14 | Miura Co Ltd | ダイオキシン類の吸着材 |
| US7021049B2 (en) * | 2000-09-29 | 2006-04-04 | Ford Global Technologies, Llc | Vehicle sulfur oxide trap and related method |
| US6605557B2 (en) | 2001-05-04 | 2003-08-12 | Saint-Gobain Norpro Corporation | Halogen-resistant media |
| RU2269501C2 (ru) | 2001-05-17 | 2006-02-10 | Сент-Гобэн Керамикс Энд Пластикс, Инк. | Керамический материал и способ его изготовления |
| US7790653B2 (en) * | 2001-10-11 | 2010-09-07 | South Dakota School Of Mines & Technology | Method and composition to reduce the amounts of arsenic in water |
| US20090246523A1 (en) | 2008-03-28 | 2009-10-01 | Shizhong Jason Zhao | Small Diameter Calcium Aluminate Based Catalyst Supports by Extrusion and Pelletizing |
| CA2696378C (en) * | 2009-03-13 | 2014-10-14 | Woodrising Resources Ltd. | Method for removal of volatile phosphates from hydrocarbons |
| RU2545307C1 (ru) * | 2013-09-05 | 2015-03-27 | Общество с ограниченной ответственностью Научно-Производственная фирма "ОЛКАТ" | Адсорбент для очистки газов от сероводорода и способ его приготовления |
| JP6332860B2 (ja) * | 2014-10-08 | 2018-05-30 | 公益財団法人北九州産業学術推進機構 | 炭化水素油の精製方法 |
| CN108148614A (zh) * | 2017-11-27 | 2018-06-12 | 湖北爱国石化有限公司 | 一种吸附法生产白油的生产工艺 |
Family Cites Families (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3468625A (en) * | 1966-11-18 | 1969-09-23 | Exxon Research Engineering Co | Preparation of crystalline alumina by homogeneous precipitation |
| US3862054A (en) * | 1972-05-26 | 1975-01-21 | Dmitry Vladimirovich Sokolsky | Adsorbent for purifying vegetable oils from phosphorus containing compounds |
| US3992329A (en) * | 1974-09-18 | 1976-11-16 | Corning Glass Works | Support of alumina-magnesia for the adsorption of glucose isomerase enzymes |
| US4147665A (en) * | 1976-06-07 | 1979-04-03 | Agency Of Industrial Science & Technology | Magnesia adsorbent |
| NL176066C (nl) * | 1978-05-26 | 1985-02-18 | Inst Kataliza Sibirskogo Otdel | Werkwijze voor het bereiden van geactiveerde korrels aluminiumoxyde. |
| US4224191A (en) * | 1979-03-05 | 1980-09-23 | Chevron Research Company | High-copper-level comulled sulfur sorbent |
| US4376103A (en) * | 1981-10-26 | 1983-03-08 | Standard Oil Company (Indiana) | Removing sulfur oxides from a gas |
| US4529502A (en) * | 1984-02-27 | 1985-07-16 | Uop Inc. | Sulfur oxide acceptance from a flue gas |
| US4571445A (en) * | 1984-12-24 | 1986-02-18 | Shell Oil Company | Process for removal of sulfur compounds from conjugated diolefins |
| US4639259A (en) * | 1985-10-09 | 1987-01-27 | Kaiser Aluminum & Chemical Corporation | Promoted scavenger for purifying HCl-contaminated gases |
| JPS62108781A (ja) * | 1985-11-07 | 1987-05-20 | 山中陶土合資会社 | 多孔質セラミツクス |
| US4923843A (en) * | 1986-09-25 | 1990-05-08 | Aluminum Company Of America | Peptized activated carbon/alumina composite |
| US5268091A (en) * | 1989-08-08 | 1993-12-07 | Institut Francais De Petrole | Method for removing arsenic and phosphorus contained in liquid hydrocarbon cuts, nickel based retaining material |
| US5389260A (en) * | 1993-04-02 | 1995-02-14 | Clack Corporation | Brine seal for tubular filter |
| US5389240A (en) | 1993-08-02 | 1995-02-14 | Uop | Naphthenic acid removal as an adjunct to liquid hydrocarbon sweetening |
| US6074984A (en) * | 1996-11-18 | 2000-06-13 | Bulldog Technologies U.S.A., Inc. | SOx Additive systems based upon use of multiple particle species |
| US6013600A (en) * | 1997-05-23 | 2000-01-11 | Laroche Industries Inc. | Alumina bodies containing alkali or alkaline earth metal compounds |
| CA2225297C (en) * | 1997-12-19 | 2009-02-10 | Trysol Limited | Purification of broken frac fluid |
| US6039865A (en) * | 1997-12-19 | 2000-03-21 | Trisol Inc. | Removal of phosphates from hydrocarbon streams |
-
2000
- 2000-01-03 US US09/476,898 patent/US6207612B1/en not_active Expired - Lifetime
- 2000-12-27 WO PCT/US2000/035364 patent/WO2001049408A1/en active IP Right Grant
- 2000-12-27 DE DE60011944T patent/DE60011944T2/de not_active Expired - Lifetime
- 2000-12-27 RU RU2002114864/15A patent/RU2218210C1/ru not_active IP Right Cessation
- 2000-12-27 MX MXPA02006653A patent/MXPA02006653A/es active IP Right Grant
- 2000-12-27 EP EP00989506A patent/EP1261422B1/en not_active Expired - Lifetime
- 2000-12-27 KR KR10-2002-7008640A patent/KR100464474B1/ko not_active IP Right Cessation
- 2000-12-27 JP JP2001549766A patent/JP3842648B2/ja not_active Expired - Fee Related
- 2000-12-27 CA CA002389991A patent/CA2389991C/en not_active Expired - Fee Related
- 2000-12-27 CN CNB008180504A patent/CN1143731C/zh not_active Expired - Fee Related
- 2000-12-27 AU AU26004/01A patent/AU755910B2/en not_active Ceased
- 2000-12-27 ES ES00989506T patent/ES2223643T3/es not_active Expired - Lifetime
- 2000-12-27 BR BR0016893-9A patent/BR0016893A/pt active Search and Examination
-
2001
- 2001-01-03 AR ARP010100019A patent/AR026785A1/es active IP Right Grant
-
2002
- 2002-06-24 NO NO20023054A patent/NO326365B1/no not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| ES2223643T3 (es) | 2005-03-01 |
| NO20023054L (no) | 2002-06-24 |
| MXPA02006653A (es) | 2002-09-30 |
| BR0016893A (pt) | 2002-10-08 |
| AR026785A1 (es) | 2003-02-26 |
| KR100464474B1 (ko) | 2005-01-03 |
| EP1261422A1 (en) | 2002-12-04 |
| CA2389991C (en) | 2007-02-20 |
| CN1143731C (zh) | 2004-03-31 |
| AU2600401A (en) | 2001-07-16 |
| US6207612B1 (en) | 2001-03-27 |
| JP2003519006A (ja) | 2003-06-17 |
| JP3842648B2 (ja) | 2006-11-08 |
| CA2389991A1 (en) | 2001-07-12 |
| WO2001049408A1 (en) | 2001-07-12 |
| NO20023054D0 (no) | 2002-06-24 |
| DE60011944T2 (de) | 2005-07-14 |
| RU2218210C1 (ru) | 2003-12-10 |
| AU755910B2 (en) | 2003-01-02 |
| NO326365B1 (no) | 2008-11-17 |
| CN1414877A (zh) | 2003-04-30 |
| EP1261422B1 (en) | 2004-06-30 |
| KR20020080358A (ko) | 2002-10-23 |
| DE60011944D1 (de) | 2004-08-05 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| RH4A | Copy of patent granted that was duplicated for the russian federation |
Effective date: 20051215 |
|
| MM4A | The patent is invalid due to non-payment of fees |
Effective date: 20041228 |
|
| PD4A | Correction of name of patent owner | ||
| NF4A | Reinstatement of patent | ||
| MM4A | The patent is invalid due to non-payment of fees |
Effective date: 20121228 |