RO86839B - Procedeu pentru prepararea de arilfosfine mono, di sau tri-sulfonate - Google Patents

Procedeu pentru prepararea de arilfosfine mono, di sau tri-sulfonate

Info

Publication number
RO86839B
RO86839B RO112074A RO11207483A RO86839B RO 86839 B RO86839 B RO 86839B RO 112074 A RO112074 A RO 112074A RO 11207483 A RO11207483 A RO 11207483A RO 86839 B RO86839 B RO 86839B
Authority
RO
Romania
Prior art keywords
mono
preparation
aqueous solution
trisulphonated
arylphosphines
Prior art date
Application number
RO112074A
Other languages
English (en)
Other versions
RO86839A (ro
Inventor
Roderich Gartner
Cornils Bey
Helmut Springer
Peter Lappe
Original Assignee
Ruhrchemie Aktiengesellschaft
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ruhrchemie Aktiengesellschaft filed Critical Ruhrchemie Aktiengesellschaft
Publication of RO86839A publication Critical patent/RO86839A/ro
Publication of RO86839B publication Critical patent/RO86839B/ro

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/50—Organo-phosphines
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/50—Organo-phosphines
    • C07F9/505—Preparation; Separation; Purification; Stabilisation
    • C07F9/5054—Preparation; Separation; Purification; Stabilisation by a process in which the phosphorus atom is not involved
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/28—Phosphorus compounds with one or more P—C bonds
    • C07F9/50—Organo-phosphines
    • C07F9/505—Preparation; Separation; Purification; Stabilisation
    • C07F9/5095—Separation; Purification; Stabilisation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Saccharide Compounds (AREA)
  • Plural Heterocyclic Compounds (AREA)

Abstract

Inventia se refera la un procedeupentru prepararea dearilfosfine mono-, di sau trisulfonate prin sulfonarea triarilfosfinelor cu acid sulfuric, concentrat la 0...40 degree C si diluarea amestecului de sulfonare cua pa, care consta în aceea ca solutia apoasa de extrage cu solutia în toluensau într-o fractiune de hidrocarburi similare cu cerozina a unei amine alifatice, ramificate sau neramificate cu 13...36 atomi de carbon, utilizîndu-se pentru fiecare echivalent de acid sulfonic 0,5...1,5 mol de amina, se separa faza organica, se aduce în contact intim cu solutia apoasa a unui hidroxid alcalin, a unui carbonat alcalin sau cu amoniac, adaosul bazei dizolvate în apa avînd loc de preferinta în portiuni, iar dupa adaugare fiecarei portiuni de baza se separa faza apoasa si se izoleaza din ea arilfosfina sulfonata.
RO112074A 1982-09-22 1983-09-15 Procedeu pentru prepararea de arilfosfine mono, di sau tri-sulfonate RO86839B (ro)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19823235030 DE3235030A1 (de) 1982-09-22 1982-09-22 Verfahren zur herstellung von sulfonierten arylphosphinen

Publications (2)

Publication Number Publication Date
RO86839A RO86839A (ro) 1985-05-20
RO86839B true RO86839B (ro) 1985-05-31

Family

ID=6173829

Family Applications (1)

Application Number Title Priority Date Filing Date
RO112074A RO86839B (ro) 1982-09-22 1983-09-15 Procedeu pentru prepararea de arilfosfine mono, di sau tri-sulfonate

Country Status (17)

Country Link
US (1) US4483802A (ro)
EP (1) EP0107006B1 (ro)
JP (1) JPS5973594A (ro)
KR (1) KR870000132B1 (ro)
AT (1) ATE16598T1 (ro)
AU (1) AU555066B2 (ro)
BR (1) BR8304994A (ro)
CA (1) CA1190562A (ro)
CS (1) CS240975B2 (ro)
DE (2) DE3235030A1 (ro)
ES (1) ES525640A0 (ro)
HU (1) HU188490B (ro)
IE (1) IE56109B1 (ro)
RO (1) RO86839B (ro)
SU (1) SU1480773A3 (ro)
YU (1) YU43550B (ro)
ZA (1) ZA836874B (ro)

Families Citing this family (33)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2549840B1 (fr) * 1983-07-28 1986-03-21 Rhone Poulenc Sante Nouvelles phosphines chirales sulfonees, leur preparation et leur emploi en catalyse asymetrique
FR2550202B1 (fr) * 1983-08-03 1986-03-21 Rhone Poulenc Rech Procede de preparation de tri(m-sulfophenyl) phosphine
DE3420493A1 (de) * 1984-06-01 1985-12-05 Ruhrchemie Ag, 4200 Oberhausen Quartaere ammoniumsalze sulfonierter triarylphosphine
DE3431643A1 (de) * 1984-08-29 1986-03-13 Ruhrchemie Ag, 4200 Oberhausen Verfahren zur abtrennung und reindarstellung von salzen der diphenylphosphinphenyl-m-sulfonsaeure, phenylphosphin-di(m-phenylsulfonsaeure) und/oder triphenylphosphin-tri(m-sulfonsaeure)
DE3534314A1 (de) * 1985-09-26 1987-04-02 Ruhrchemie Ag Verfahren zur herstellung von aldehyden
DE3534317A1 (de) * 1985-09-26 1987-04-02 Ruhrchemie Ag Verfahren zur herstellung von nonadecandiolen
US4716250A (en) * 1986-07-10 1987-12-29 Union Carbide Corporation Hydroformylation using low volatile/organic soluble phosphine ligands
FR2606202B1 (fr) * 1986-10-30 1992-09-18 Commissariat Energie Atomique Procede de recuperation de composes organophosphores acides et/ou d'ions organophosphate presents dans une solution aqueuse et son utilisation pour le traitement d'effluents aqueux
US4731486A (en) * 1986-11-18 1988-03-15 Union Carbide Corporation Hydroformylation using low volatile phosphine ligands
US5246901A (en) * 1988-05-23 1993-09-21 Catalytica, Inc. Polysulfonic acids
US5180854A (en) * 1988-07-14 1993-01-19 Union Carbide Chemicals & Plastics Technology Corporation Process for catalyst aldehyde product separation
US4965404A (en) * 1989-03-09 1990-10-23 Kuraray Company, Ltd. Process for the preparation of lithium diphenylphosphinobenzene-m-monosulfonate
US5274183A (en) * 1990-12-17 1993-12-28 Hoechst Aktiengesellschaft Water-soluble sulfonated diphosphines
DE4139651A1 (de) * 1991-12-02 1993-06-03 Hoechst Ag Verfahren zur abtrennung organischer phosphorverbindungen und weiterer verunreinigungen aus verduennter schwefelsaeure
TW248563B (ro) * 1993-06-29 1995-06-01 Hoechst Ag
DE4426671A1 (de) * 1994-07-28 1996-02-01 Hoechst Ag Verfahren zur Kreuzkupplung von aromatischen Borverbindungen mit aromatischen Halogenverbindungen oder Perfluoralkylsulfonaten
DE4427428A1 (de) 1994-08-03 1996-02-29 Basf Ag Verfahren zur Herstellung von Aldehyden
DE4435190A1 (de) * 1994-09-30 1996-04-04 Hoechst Ag Verfahren zur Herstellung von sulfonierten Arylphosphinen
DE4435171A1 (de) * 1994-09-30 1996-04-04 Hoechst Ag 5-H-Phenyl(di-3,13-sulfonato)dibenzophosphol und ein Verfahren zu seiner Herstellung
DE19822968A1 (de) 1998-05-25 1999-12-02 Rwe Dea Ag Verfahren zur katalytischen Hydroformylierung von Olefinen
FR2787786B1 (fr) * 1998-12-23 2001-02-02 Rhone Poulenc Fibres Procede de preparation de composes organophosphores sulfones hydrosolubles et la realisation de reactions organiques avec catalyse biphasique
DE19918284C1 (de) * 1999-04-22 2000-12-14 Celanese Chem Europe Gmbh Verfahren zur Herstellung von sulfonierten Arylphosphinen
SG93931A1 (en) * 2001-04-13 2003-01-21 Kuraray Co Phosphonium salts and processes for production of and uses for the same, and phosphines deriving the same and processes for production of the phosphines
US7663002B2 (en) * 2006-05-15 2010-02-16 Dow Global Technologies, Inc. Hydroformylation process and product separation with improved recovery of rhodium
CN101778812B (zh) * 2007-06-13 2015-02-18 陶氏环球技术有限责任公司 用于醛产物分离的提取方法和催化剂的回收
EP2231682B1 (en) * 2008-01-15 2016-01-06 Dow Global Technologies LLC Sulfonated organophosphine compounds and use thereof in hydroformylation processes
US8466306B2 (en) * 2008-01-15 2013-06-18 Dow Global Technologies Llc Sulfonated organophosphine compounds and use in hydroformylation processes
EP2231683B1 (en) * 2008-01-15 2016-03-23 Dow Global Technologies LLC Sulfonated organophosphine compounds and use thereof in hydroformylation processes
CN103420843A (zh) * 2013-07-30 2013-12-04 苏州环科新材料有限公司 二异十三胺的合成方法
EP3728174B1 (en) 2017-12-20 2022-11-30 DSM IP Assets B.V. Synthesis of alkyl 2-acetyl-5,9,13-trimethyltetradeca-4,8,12-trienoates and derivatives by a non-continuous production process
EP3844293A4 (en) 2018-08-30 2022-06-08 Checkerspot, Inc. HYDROFORMYLATED TRIGLYCERIDES AND THEIR USES
CN118124217A (zh) 2019-12-18 2024-06-04 格纹蛱蝶公司 微生物衍生材料在聚合物应用中的用途
WO2023102069A1 (en) 2021-12-01 2023-06-08 Checkerspot, Inc. Polyols, polyurethane dispersions, and uses thereof

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3719703A (en) * 1969-04-29 1973-03-06 Atomic Energy Commission Separation of sulfonic acids from sulfuric acid
US4248802A (en) * 1975-06-20 1981-02-03 Rhone-Poulenc Industries Catalytic hydroformylation of olefins
JPS52116438A (en) * 1975-12-17 1977-09-29 Toyo Soda Mfg Co Ltd Preparation of styrene sulfonic acid salts
US4260750A (en) * 1976-07-27 1981-04-07 Rhone-Poulenc Industries Telomerization process
DE3020526A1 (de) * 1980-05-30 1981-12-10 Basf Ag, 6700 Ludwigshafen Verfahren zur abtrennung wasserloeslicher salze von aromatischen sulfonsaeuren aus sulfiergemischen

Also Published As

Publication number Publication date
ES8405417A1 (es) 1984-06-01
AU1920783A (en) 1984-03-29
CS671183A2 (en) 1985-06-13
AU555066B2 (en) 1986-09-11
EP0107006B1 (de) 1985-11-21
DE3361300D1 (en) 1986-01-02
CS240975B2 (en) 1986-03-13
HU188490B (en) 1986-04-28
JPS6347718B2 (ro) 1988-09-26
SU1480773A3 (ru) 1989-05-15
US4483802A (en) 1984-11-20
KR840006011A (ko) 1984-11-21
JPS5973594A (ja) 1984-04-25
KR870000132B1 (ko) 1987-02-12
ATE16598T1 (de) 1985-12-15
IE56109B1 (en) 1991-04-24
DE3235030A1 (de) 1984-03-22
BR8304994A (pt) 1984-09-04
CA1190562A (en) 1985-07-16
ES525640A0 (es) 1984-06-01
YU43550B (en) 1989-08-31
RO86839A (ro) 1985-05-20
IE832129L (en) 1984-03-22
YU187583A (en) 1986-06-30
EP0107006A1 (de) 1984-05-02
ZA836874B (en) 1984-05-30

Similar Documents

Publication Publication Date Title
KR840006011A (ko) 썰폰화 아릴 포스핀의 제조방법
RO84860B (ro) Procedeu pentru prepararea 9-(1, 3-dihidroxi-2-propeximetil)-guaninei
GB1432533A (en) Preparation of inorganic fluoride-free perfluoroalkane sulphonates
MX2012001350A (es) Recuperacion de plomo en forma de compuesto de plomo de alta pureza a partir de lodo de pasta de electrodo recuperado de baterias de plomo desechadas y/o minerales de plomo.
YU47539B (sh) Koncentrovana tečna deterdžentna kompozicija koja sadrži alkilbenzensulfonat i magnezijum
DE3164128D1 (en) Process for the separation of water-soluble salts of aromatic sulphonic acids from sulphonated mixtures
ES2082847T3 (es) Procedimiento mejorado para la preparacion de derivados de amidoximas.
JP4937067B2 (ja) ナフタレンスルホン酸ホルマリン縮合物ナトリウム塩の製造方法
GB1225218A (ro)
JPH0244833B2 (ro)
FR2171199B1 (ro)
JPS54151956A (en) Production of 2-carboxyanthraquinonemonosulfonic acid and its salt and oxidation and reduction reagent therefrom for wet desulfurization
SU443682A1 (ru) Способ обезвоживани
FR2457280A1 (fr) Procede de production de derives de la serine
US4959490A (en) Process for manufacturing disulfonate surfactants
KR920012101A (ko) 수용성 디포스핀의 제조방법
KR960010671A (ko) 5h- 페닐-3,13- 디설포네이토디벤조포스폴 및 이의 제조방법
US4696770A (en) Method for the synthesis of sulfonated rubrene
KR910011875A (ko) 술폰화 프로필페닐포스핀, 이의 제조방법 및 용도
BR9803921A (pt) Remoção de sais de soluções aquosas de sulfonamidas.
RO95821B1 (ro) Procedeu pentru obtinerea unor saruri alcaline ale esterilor acidului 0,0-dialchilditiofosforic
SU1131872A1 (ru) Способ получени натриевых солей алкилсульфатов
US3974210A (en) Alkylphenol disulfonates of improved color by neutralizing with strong caustic
JPS54130620A (en) Preparation of alpha-quinacridone pigment
GB1219885A (en) Processes for the separation of mixtures of fatty acids and rosin acids