PT94532A - Processo para a fabricacao de espumas de poliuretano sem o emprego de agentes de expansao inertes - Google Patents
Processo para a fabricacao de espumas de poliuretano sem o emprego de agentes de expansao inertesInfo
- Publication number
- PT94532A PT94532A PT94532A PT9453290A PT94532A PT 94532 A PT94532 A PT 94532A PT 94532 A PT94532 A PT 94532A PT 9453290 A PT9453290 A PT 9453290A PT 94532 A PT94532 A PT 94532A
- Authority
- PT
- Portugal
- Prior art keywords
- employment
- manufacture
- polyurethane foams
- expansion agents
- inert expansion
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/2805—Compounds having only one group containing active hydrogen
- C08G18/2815—Monohydroxy compounds
- C08G18/283—Compounds containing ether groups, e.g. oxyalkylated monohydroxy compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/48—Polyethers
- C08G18/4804—Two or more polyethers of different physical or chemical nature
- C08G18/4816—Two or more polyethers of different physical or chemical nature mixtures of two or more polyetherpolyols having at least three hydroxy groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/63—Block or graft polymers obtained by polymerising compounds having carbon-to-carbon double bonds on to polymers
- C08G18/632—Block or graft polymers obtained by polymerising compounds having carbon-to-carbon double bonds on to polymers onto polyethers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/65—Low-molecular-weight compounds having active hydrogen with high-molecular-weight compounds having active hydrogen
- C08G18/66—Compounds of groups C08G18/42, C08G18/48, or C08G18/52
- C08G18/6666—Compounds of group C08G18/48 or C08G18/52
- C08G18/667—Compounds of group C08G18/48 or C08G18/52 with compounds of group C08G18/32 or polyamines of C08G18/38
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G2110/00—Foam properties
- C08G2110/0008—Foam properties flexible
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G2110/00—Foam properties
- C08G2110/0041—Foam properties having specified density
- C08G2110/005—< 50kg/m3
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G2110/00—Foam properties
- C08G2110/0083—Foam properties prepared using water as the sole blowing agent
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polyurethanes Or Polyureas (AREA)
- Manufacture Of Porous Articles, And Recovery And Treatment Of Waste Products (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US07/373,244 US4950694A (en) | 1989-06-29 | 1989-06-29 | Preparation of polyurethane foams without using inert blowing agents |
Publications (2)
Publication Number | Publication Date |
---|---|
PT94532A true PT94532A (pt) | 1991-02-08 |
PT94532B PT94532B (pt) | 1997-02-28 |
Family
ID=23471574
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PT94532A PT94532B (pt) | 1989-06-29 | 1990-06-28 | Processo para a fabricacao de espumas de poliuretano sem o emprego de agentes de expansao inertes |
Country Status (19)
Country | Link |
---|---|
US (1) | US4950694A (pt) |
EP (1) | EP0406702B1 (pt) |
JP (1) | JP2678518B2 (pt) |
KR (1) | KR970000939B1 (pt) |
AR (1) | AR244728A1 (pt) |
AT (1) | ATE149535T1 (pt) |
AU (1) | AU633111B2 (pt) |
BR (1) | BR9003079A (pt) |
CA (1) | CA2020081C (pt) |
DD (1) | DD300650A5 (pt) |
DE (1) | DE69030029T2 (pt) |
DK (1) | DK0406702T3 (pt) |
ES (1) | ES2099077T3 (pt) |
FI (1) | FI903275A0 (pt) |
GR (1) | GR3023213T3 (pt) |
IE (1) | IE902372A1 (pt) |
NO (1) | NO179287C (pt) |
PT (1) | PT94532B (pt) |
ZA (1) | ZA905061B (pt) |
Families Citing this family (77)
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JP2917319B2 (ja) * | 1989-10-19 | 1999-07-12 | 株式会社ブリヂストン | 低密度軟質ポリウレタンフォームの製造方法 |
JPH03239716A (ja) * | 1990-02-19 | 1991-10-25 | Sanyo Chem Ind Ltd | 軟質ポリウレタンフォーム形成組成物および製法 |
US5177119A (en) * | 1990-04-25 | 1993-01-05 | Arco Chemical Technology, L.P. | Polyurethane foams blown only with water |
US5084486A (en) * | 1990-12-20 | 1992-01-28 | Union Carbide Chemicals & Plastics Technology Corporation | Reactive feed stream to replace inert blowing agent feed stream in a polyurethane foam process |
AU654333B2 (en) * | 1991-04-03 | 1994-11-03 | Huntsman Ici Chemicals Llc | Manufacture of cellular polymers and compositions therefor |
US5124368A (en) * | 1991-07-29 | 1992-06-23 | Arco Chemical Technology, L.P. | Pour-in-place flexible polyurethane foam articles |
HRP920243A2 (en) | 1991-08-20 | 1996-06-30 | Dow Chemical Co | Polyurethanes of improved physical properties |
US5373028A (en) * | 1991-08-20 | 1994-12-13 | The Dow Chemical Company | Polyurethane foams having reduced visible emissions during curing |
US5876134A (en) * | 1992-02-14 | 1999-03-02 | The Gillette Company | Foam grip |
US5169872A (en) * | 1992-05-11 | 1992-12-08 | Dow Corning Corporation | Process for preparing rigid polyurethane and polyisocyanurate foams having enhanced benefits |
JP3317308B2 (ja) | 1992-08-26 | 2002-08-26 | セイコーエプソン株式会社 | 積層型インクジェット記録ヘッド、及びその製造方法 |
US6601949B1 (en) | 1992-08-26 | 2003-08-05 | Seiko Epson Corporation | Actuator unit for ink jet recording head |
US5232957A (en) * | 1992-09-11 | 1993-08-03 | Davidson Textron Inc. | RIM molded energy absorbing polyurethane foam |
US5312847A (en) * | 1993-03-16 | 1994-05-17 | The Dow Chemical Company | Polyurethane foam containing a particulate organic solid and a process for the preparation thereof |
US5382602A (en) * | 1993-06-09 | 1995-01-17 | Duffy; Robert D. | Flexible slabstock polyurethane foam formulation for a rapid-cool process |
US5278197A (en) * | 1993-07-06 | 1994-01-11 | Miles Inc. | Soft, flexible polyurethane foam |
ZA945718B (en) * | 1993-08-03 | 1995-03-09 | Osi Specialties Inc | Process for forming polyurethane foam using mechanical cooling and an additive |
USRE36233E (en) * | 1993-08-03 | 1999-06-22 | Osi Specialties, Inc. | Use of softening additives in polyurethane foam |
US6521674B1 (en) | 1993-10-01 | 2003-02-18 | Carpenter Co. | Latex-like flexible polyurethane foam and process for making same |
DE69434514T2 (de) | 1993-12-24 | 2006-06-22 | Seiko Epson Corp. | Tintenstrahlaufzeichnungskopf |
US5880756A (en) | 1993-12-28 | 1999-03-09 | Seiko Epson Corporation | Ink jet recording head |
GB9404127D0 (en) * | 1994-03-03 | 1994-04-20 | Polyol Int Bv | Process for producing a soft, flexible, hot molded poyurethane foam |
EP0692507A1 (en) * | 1994-07-11 | 1996-01-17 | Basf Corporation | Flexible open-cell polyurethane foam |
US5907338A (en) * | 1995-01-13 | 1999-05-25 | Burr; Ronald F. | High-performance ink jet print head |
US5596059A (en) * | 1995-07-26 | 1997-01-21 | Arco Chemical Technology, L.P. | Polyether polyols suitable for mflexible polyurethane foam prepared by co-initiation of aqueous solutions of solid polyhydroxyl initiators |
KR100224595B1 (ko) * | 1997-04-26 | 1999-10-15 | 윤종용 | 개방셀 경질 폴리우레탄 발포체 및 그 제조방법과, 그를 이용한 진공단열 판넬의 제조방법 |
DE19741257A1 (de) * | 1997-09-19 | 1999-03-25 | Basf Ag | Verfahren zur Herstellung von Polyurethanschaumstoffen |
US6136879A (en) * | 1997-10-28 | 2000-10-24 | Tokai Rubber Industries, Ltd. | Soft polyurethane foam, method of producing the same and vehicle interior member using the same |
ITMI981101A1 (it) * | 1998-05-19 | 1999-11-19 | Vefer Spa | Procedimento e impianto per realizzare poliuretani espansi addittivati con lattice di gomma finalizzati all'ottenimento di maggiore comfort |
US20050166302A1 (en) * | 1998-09-03 | 2005-08-04 | Mjd Innovations, L.L.C. | Non-resiliency body-contact protective helmet interface structure |
WO2001002484A1 (en) * | 1999-07-01 | 2001-01-11 | E.I. Du Pont De Nemours And Company | Crosslinked foam of ethylene vinyl acetate copolymer and acid copolymer |
WO2001030895A1 (en) * | 1999-10-29 | 2001-05-03 | Shell Internationale Research Maatschappij B.V. | Process for the preparation of a flexible polyurethane foam |
WO2002010245A1 (en) | 2000-08-01 | 2002-02-07 | Huntsman International Llc | Manufacture of mdi-tdi based flexible polyurethane foams |
DE10110553A1 (de) * | 2001-03-05 | 2002-09-12 | Basf Ag | Verfahren zur Herstellung von Polyurethan-Weichschaumstoffen |
EP1404736B1 (en) * | 2001-04-27 | 2008-12-10 | Huntsman International Llc | Process for making visco-elastic foam |
JP4785382B2 (ja) | 2002-05-24 | 2011-10-05 | テンピュール・ワールド・エルエルシー | 快適枕 |
US20040126556A1 (en) * | 2002-12-27 | 2004-07-01 | Nowak Michael T. | Grip element |
US20040192800A1 (en) * | 2003-02-06 | 2004-09-30 | Shidaker Trent A. | Unreinforced reaction injection molded structural foams |
US7168216B2 (en) * | 2003-06-06 | 2007-01-30 | Hans T. Hagen, Jr. | Insulated stud panel and method of making such |
CA2469986A1 (en) | 2003-06-06 | 2004-12-06 | Hagen, Hans T., Iii | Insulated stud panel and method of making such |
US20050261386A1 (en) * | 2004-05-24 | 2005-11-24 | Schneider Bruce H | Latex-enhanced polyurethane foam cushioning |
US7268170B2 (en) * | 2004-10-13 | 2007-09-11 | Bayer Materialscience Llc | Foam modifier, foams prepared from this novel foam modifier and a process for the preparation of these foams |
US7469437B2 (en) | 2005-06-24 | 2008-12-30 | Tempur-Pedic Management, Inc. | Reticulated material body support and method |
US7875675B2 (en) * | 2005-11-23 | 2011-01-25 | Milgard Manufacturing Incorporated | Resin for composite structures |
DE102005056246A1 (de) * | 2005-11-25 | 2007-06-06 | Goldschmidt Gmbh | Gepfropfte Polyether-Copolymerisate und deren Verwendung zur Stabilisierung von Schaumstoffen |
US20070129451A1 (en) * | 2005-12-01 | 2007-06-07 | Niemann Lance K | Bio-based, insulating foam |
US8656537B2 (en) | 2006-04-20 | 2014-02-25 | Dan Foam Aps | Multi-component pillow and method of manufacturing and assembling same |
US20070293594A1 (en) * | 2006-06-15 | 2007-12-20 | Ladislau Heisler | Viscoelastic polyurethane foam and process for its manufacture |
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CN101842404B (zh) * | 2007-08-27 | 2014-06-18 | 陶氏环球技术有限责任公司 | 具有铋化合物的基于天然油的柔性聚氨酯泡沫的催化剂 |
JP5271548B2 (ja) * | 2008-01-16 | 2013-08-21 | 株式会社イノアックコーポレーション | 難変色性の軟質ポリウレタン発泡体 |
EP2303944B8 (en) | 2008-07-18 | 2017-12-06 | Dow Global Technologies LLC | Cellular structures and viscoelastic polyurethane foams |
EP2337536B1 (en) | 2008-10-02 | 2020-08-12 | L.R. R & D Ltd. | Interface layer wound dressing |
US8901187B1 (en) | 2008-12-19 | 2014-12-02 | Hickory Springs Manufacturing Company | High resilience flexible polyurethane foam using MDI |
US8906975B1 (en) | 2009-02-09 | 2014-12-09 | Hickory Springs Manufacturing Company | Conventional flexible polyurethane foam using MDI |
JP4920051B2 (ja) * | 2009-02-25 | 2012-04-18 | 株式会社日立製作所 | 酸素燃焼ボイラプラント及び酸素燃焼ボイラプラントの運転方法 |
TWI404739B (zh) * | 2009-04-02 | 2013-08-11 | Chung Hsien Tu | 軟質聚氨酯低回彈發泡體及其製備方法 |
JP5528169B2 (ja) * | 2010-03-26 | 2014-06-25 | 東洋ゴム工業株式会社 | 研磨パッドおよびその製造方法、ならびに半導体デバイスの製造方法 |
EP2612886A4 (en) * | 2010-08-31 | 2014-08-27 | Nitto Denko Corp | FOAM, PROCESS FOR MAKING FOAM AND FUNCTIONAL FOAM |
EP2621984B1 (en) | 2010-09-29 | 2015-02-25 | Dow Global Technologies LLC | Use of poly(butylene oxide) polyol to improve durability of mdi-polyurethane foams |
CN103228690B (zh) * | 2010-09-29 | 2016-03-09 | 陶氏环球技术有限责任公司 | 制备高气流和低压缩变定粘弹性聚氨酯泡沫体的方法 |
WO2013042507A1 (ja) | 2011-09-22 | 2013-03-28 | 東洋ゴム工業株式会社 | 研磨パッド |
CN103974990A (zh) | 2012-07-30 | 2014-08-06 | 帝国糖业公司 | 基于糖的聚氨酯、其制备方法、及其使用方法 |
JP6259561B2 (ja) * | 2012-09-28 | 2018-01-10 | 株式会社イノアックコーポレーション | クリーニングローラおよびクリーニングローラに使用されるポリウレタンフォームの製造方法 |
DE112013004958B4 (de) * | 2012-10-10 | 2023-01-26 | Proprietect L.P. | Verfahren zur Herstellung eines frei aufgeschäumten Polyurethan-Schaumstoffs mit niedriger Dichte sowie frei aufgeschäumter Polyurethan-Schaumstoff |
KR101491089B1 (ko) * | 2014-06-27 | 2015-02-10 | 주식회사 세림티티시 | 연질 폴리우레탄폼 |
JP2016044292A (ja) * | 2014-08-26 | 2016-04-04 | 株式会社ブリヂストン | 軟質ウレタンフォーム及びそれを用いてなるシートパッド |
US9951174B2 (en) | 2015-05-20 | 2018-04-24 | Covestro Llc | Polyol compositions, a process for the production of these polyol compositions, and their use in the production of open celled polyurethane foams having high airflow |
WO2018169833A1 (en) | 2017-03-15 | 2018-09-20 | Covestro Llc | Viscoelastic polyurethane foams with reduced temperature sensitivity |
US10766998B2 (en) | 2017-11-21 | 2020-09-08 | Covestro Llc | Flexible polyurethane foams |
US10793692B2 (en) | 2018-10-24 | 2020-10-06 | Covestro Llc | Viscoelastic flexible foams comprising hydroxyl-terminated prepolymers |
KR102140285B1 (ko) * | 2018-12-07 | 2020-07-31 | 서울시립대학교 산학협력단 | 폴리우레탄 폼 성형체 및 폴리우레탄 폼 제조방법 |
CN114514257A (zh) | 2019-10-09 | 2022-05-17 | 科思创有限公司 | 使用光学和红外成像的生产聚氨酯泡沫产品的方法、系统和计算机程序产品 |
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US11572433B2 (en) | 2021-03-12 | 2023-02-07 | Covestro Llc | In-situ formed polyols, a process for their preparation, foams prepared from these in-situ formed polyols and a process for their preparation |
CN114590907A (zh) * | 2021-03-25 | 2022-06-07 | 景赫新材料科技(浙江)有限公司 | 一种亲水性多孔生物载体及应用 |
US11718705B2 (en) | 2021-07-28 | 2023-08-08 | Covestro Llc | In-situ formed polyether polyols, a process for their preparation, and a process for the preparation of polyurethane foams |
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-
1989
- 1989-06-29 US US07/373,244 patent/US4950694A/en not_active Expired - Lifetime
-
1990
- 1990-06-28 DK DK90112348.9T patent/DK0406702T3/da active
- 1990-06-28 ZA ZA905061A patent/ZA905061B/xx unknown
- 1990-06-28 PT PT94532A patent/PT94532B/pt not_active IP Right Cessation
- 1990-06-28 KR KR1019900009623A patent/KR970000939B1/ko not_active IP Right Cessation
- 1990-06-28 AR AR90317257A patent/AR244728A1/es active
- 1990-06-28 EP EP90112348A patent/EP0406702B1/en not_active Expired - Lifetime
- 1990-06-28 CA CA002020081A patent/CA2020081C/en not_active Expired - Lifetime
- 1990-06-28 FI FI903275A patent/FI903275A0/fi not_active Application Discontinuation
- 1990-06-28 ES ES90112348T patent/ES2099077T3/es not_active Expired - Lifetime
- 1990-06-28 NO NO902888A patent/NO179287C/no unknown
- 1990-06-28 AT AT90112348T patent/ATE149535T1/de not_active IP Right Cessation
- 1990-06-28 DE DE69030029T patent/DE69030029T2/de not_active Expired - Fee Related
- 1990-06-29 IE IE237290A patent/IE902372A1/en unknown
- 1990-06-29 AU AU58036/90A patent/AU633111B2/en not_active Ceased
- 1990-06-29 JP JP2170418A patent/JP2678518B2/ja not_active Expired - Fee Related
- 1990-06-29 BR BR909003079A patent/BR9003079A/pt not_active IP Right Cessation
- 1990-06-29 DD DD342351A patent/DD300650A5/de unknown
-
1997
- 1997-04-21 GR GR970400874T patent/GR3023213T3/el unknown
Also Published As
Publication number | Publication date |
---|---|
AU5803690A (en) | 1991-01-03 |
EP0406702A1 (en) | 1991-01-09 |
US4950694A (en) | 1990-08-21 |
DD300650A5 (de) | 1992-06-25 |
CA2020081C (en) | 1995-06-13 |
CA2020081A1 (en) | 1990-12-30 |
AU633111B2 (en) | 1993-01-21 |
FI903275A0 (fi) | 1990-06-28 |
NO179287B (no) | 1996-06-03 |
JPH0364311A (ja) | 1991-03-19 |
KR970000939B1 (ko) | 1997-01-21 |
GR3023213T3 (en) | 1997-07-30 |
JP2678518B2 (ja) | 1997-11-17 |
NO902888D0 (no) | 1990-06-28 |
AR244728A1 (es) | 1993-11-30 |
BR9003079A (pt) | 1991-08-27 |
NO902888L (no) | 1991-01-02 |
IE902372A1 (en) | 1991-06-19 |
ATE149535T1 (de) | 1997-03-15 |
EP0406702B1 (en) | 1997-03-05 |
DE69030029T2 (de) | 1997-06-12 |
PT94532B (pt) | 1997-02-28 |
IE902372L (en) | 1990-12-29 |
DE69030029D1 (de) | 1997-04-10 |
KR910000844A (ko) | 1991-01-30 |
DK0406702T3 (da) | 1997-09-15 |
ZA905061B (en) | 1991-04-24 |
ES2099077T3 (es) | 1997-05-16 |
NO179287C (no) | 1996-09-11 |
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Effective date: 19961125 |
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Free format text: LAPSE DUE TO NON-PAYMENT OF FEES Effective date: 20040531 |