PL191326B1 - Kompozycja katalizatora, sposób wytwarzania kompozycji katalizatora oraz zastosowanie kompozycji katalizatora do usuwania wosku z wsadu węglowodorowego - Google Patents
Kompozycja katalizatora, sposób wytwarzania kompozycji katalizatora oraz zastosowanie kompozycji katalizatora do usuwania wosku z wsadu węglowodorowegoInfo
- Publication number
- PL191326B1 PL191326B1 PL348352A PL34835299A PL191326B1 PL 191326 B1 PL191326 B1 PL 191326B1 PL 348352 A PL348352 A PL 348352A PL 34835299 A PL34835299 A PL 34835299A PL 191326 B1 PL191326 B1 PL 191326B1
- Authority
- PL
- Poland
- Prior art keywords
- crystallites
- zeolite
- catalyst composition
- binder
- metallosilicate
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims abstract description 66
- 230000003197 catalytic effect Effects 0.000 title claims description 30
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 102
- 239000003054 catalyst Substances 0.000 claims abstract description 79
- 239000000203 mixture Substances 0.000 claims abstract description 52
- 239000011230 binding agent Substances 0.000 claims abstract description 43
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 39
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 claims abstract description 29
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 17
- 239000000843 powder Substances 0.000 claims abstract description 16
- 150000002500 ions Chemical class 0.000 claims abstract description 13
- 229910001868 water Inorganic materials 0.000 claims abstract description 10
- 238000001354 calcination Methods 0.000 claims abstract description 6
- 239000008240 homogeneous mixture Substances 0.000 claims abstract description 6
- 238000001035 drying Methods 0.000 claims abstract description 5
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims description 71
- 239000010457 zeolite Substances 0.000 claims description 67
- 229910021536 Zeolite Inorganic materials 0.000 claims description 53
- 229910000323 aluminium silicate Inorganic materials 0.000 claims description 20
- 238000009835 boiling Methods 0.000 claims description 19
- 229930195733 hydrocarbon Natural products 0.000 claims description 16
- 150000002430 hydrocarbons Chemical class 0.000 claims description 16
- 239000004215 Carbon black (E152) Substances 0.000 claims description 15
- 229910052751 metal Inorganic materials 0.000 claims description 15
- 239000002184 metal Substances 0.000 claims description 15
- 229910052697 platinum Inorganic materials 0.000 claims description 13
- 239000002245 particle Substances 0.000 claims description 12
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical group [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 claims description 11
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 8
- 150000003839 salts Chemical class 0.000 claims description 7
- 239000013078 crystal Substances 0.000 claims description 6
- 229940104869 fluorosilicate Drugs 0.000 claims description 6
- 238000005984 hydrogenation reaction Methods 0.000 claims description 6
- 239000000126 substance Substances 0.000 claims description 6
- 229910052782 aluminium Inorganic materials 0.000 claims description 5
- 238000004517 catalytic hydrocracking Methods 0.000 claims description 5
- 229910052763 palladium Inorganic materials 0.000 claims description 5
- 239000007864 aqueous solution Substances 0.000 claims description 4
- 150000001768 cations Chemical class 0.000 claims description 4
- 229910001657 ferrierite group Inorganic materials 0.000 claims description 4
- 229910052909 inorganic silicate Inorganic materials 0.000 claims description 4
- 238000002360 preparation method Methods 0.000 claims description 4
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 claims description 3
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 3
- 229910017052 cobalt Inorganic materials 0.000 claims description 3
- 239000010941 cobalt Substances 0.000 claims description 3
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims description 3
- 229910052759 nickel Inorganic materials 0.000 claims description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims description 2
- 229910052796 boron Inorganic materials 0.000 claims description 2
- 229910052733 gallium Inorganic materials 0.000 claims description 2
- 229910052742 iron Inorganic materials 0.000 claims description 2
- 229910052755 nonmetal Inorganic materials 0.000 claims description 2
- 125000004430 oxygen atom Chemical group O* 0.000 claims description 2
- 229910052719 titanium Inorganic materials 0.000 claims description 2
- 125000004429 atom Chemical group 0.000 claims 1
- 230000001747 exhibiting effect Effects 0.000 claims 1
- 239000002253 acid Substances 0.000 abstract description 19
- 238000012545 processing Methods 0.000 abstract description 2
- 229910052914 metal silicate Inorganic materials 0.000 abstract 3
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 21
- 239000001993 wax Substances 0.000 description 20
- -1 for example Substances 0.000 description 19
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 17
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 14
- 239000003921 oil Substances 0.000 description 13
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 description 13
- 239000000243 solution Substances 0.000 description 12
- 239000012530 fluid Substances 0.000 description 11
- 229910052739 hydrogen Inorganic materials 0.000 description 10
- 239000001257 hydrogen Substances 0.000 description 10
- 229910052814 silicon oxide Inorganic materials 0.000 description 10
- 239000010687 lubricating oil Substances 0.000 description 9
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 8
- 229910021529 ammonia Inorganic materials 0.000 description 8
- 239000002199 base oil Substances 0.000 description 8
- 238000006243 chemical reaction Methods 0.000 description 8
- 238000004821 distillation Methods 0.000 description 8
- 230000001050 lubricating effect Effects 0.000 description 8
- 238000002156 mixing Methods 0.000 description 8
- 238000005292 vacuum distillation Methods 0.000 description 8
- 150000001875 compounds Chemical class 0.000 description 7
- 238000001125 extrusion Methods 0.000 description 7
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 6
- 230000015572 biosynthetic process Effects 0.000 description 6
- 239000008367 deionised water Substances 0.000 description 6
- 229910021641 deionized water Inorganic materials 0.000 description 6
- 239000007789 gas Substances 0.000 description 6
- 239000000463 material Substances 0.000 description 6
- 229910052717 sulfur Inorganic materials 0.000 description 6
- 239000011593 sulfur Substances 0.000 description 6
- 238000003786 synthesis reaction Methods 0.000 description 6
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 description 5
- 239000008119 colloidal silica Substances 0.000 description 5
- 239000011148 porous material Substances 0.000 description 5
- 239000004698 Polyethylene Substances 0.000 description 4
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 4
- 239000003795 chemical substances by application Substances 0.000 description 4
- 230000000052 comparative effect Effects 0.000 description 4
- 229910052906 cristobalite Inorganic materials 0.000 description 4
- 239000012535 impurity Substances 0.000 description 4
- 238000011068 loading method Methods 0.000 description 4
- 229920000609 methyl cellulose Polymers 0.000 description 4
- 239000001923 methylcellulose Substances 0.000 description 4
- 235000010981 methylcellulose Nutrition 0.000 description 4
- 229910052757 nitrogen Inorganic materials 0.000 description 4
- RVTZCBVAJQQJTK-UHFFFAOYSA-N oxygen(2-);zirconium(4+) Chemical compound [O-2].[O-2].[Zr+4] RVTZCBVAJQQJTK-UHFFFAOYSA-N 0.000 description 4
- 229920000573 polyethylene Polymers 0.000 description 4
- 229910001928 zirconium oxide Inorganic materials 0.000 description 4
- 229920003091 Methocel™ Polymers 0.000 description 3
- 230000008901 benefit Effects 0.000 description 3
- 229920003086 cellulose ether Polymers 0.000 description 3
- 229910052681 coesite Inorganic materials 0.000 description 3
- 229910052593 corundum Inorganic materials 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 3
- 239000000395 magnesium oxide Substances 0.000 description 3
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 description 3
- 201000011540 mitochondrial DNA depletion syndrome 4a Diseases 0.000 description 3
- 229910000510 noble metal Inorganic materials 0.000 description 3
- 235000012239 silicon dioxide Nutrition 0.000 description 3
- 239000011734 sodium Substances 0.000 description 3
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical class [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 description 3
- 239000002904 solvent Substances 0.000 description 3
- 229910052682 stishovite Inorganic materials 0.000 description 3
- 229910052905 tridymite Inorganic materials 0.000 description 3
- 229910001845 yogo sapphire Inorganic materials 0.000 description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 2
- 229920000663 Hydroxyethyl cellulose Polymers 0.000 description 2
- 239000004354 Hydroxyethyl cellulose Substances 0.000 description 2
- 229920001479 Hydroxyethyl methyl cellulose Polymers 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 description 2
- 238000002441 X-ray diffraction Methods 0.000 description 2
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 2
- 229910052810 boron oxide Inorganic materials 0.000 description 2
- JKWMSGQKBLHBQQ-UHFFFAOYSA-N diboron trioxide Chemical compound O=BOB=O JKWMSGQKBLHBQQ-UHFFFAOYSA-N 0.000 description 2
- LIWAQLJGPBVORC-UHFFFAOYSA-N ethylmethylamine Chemical compound CCNC LIWAQLJGPBVORC-UHFFFAOYSA-N 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- YBMRDBCBODYGJE-UHFFFAOYSA-N germanium dioxide Chemical compound O=[Ge]=O YBMRDBCBODYGJE-UHFFFAOYSA-N 0.000 description 2
- NAQMVNRVTILPCV-UHFFFAOYSA-N hexane-1,6-diamine Chemical compound NCCCCCCN NAQMVNRVTILPCV-UHFFFAOYSA-N 0.000 description 2
- 235000019447 hydroxyethyl cellulose Nutrition 0.000 description 2
- 239000001866 hydroxypropyl methyl cellulose Substances 0.000 description 2
- 229920003088 hydroxypropyl methyl cellulose Polymers 0.000 description 2
- 235000010979 hydroxypropyl methyl cellulose Nutrition 0.000 description 2
- UFVKGYZPFZQRLF-UHFFFAOYSA-N hydroxypropyl methyl cellulose Chemical compound OC1C(O)C(OC)OC(CO)C1OC1C(O)C(O)C(OC2C(C(O)C(OC3C(C(O)C(O)C(CO)O3)O)C(CO)O2)O)C(CO)O1 UFVKGYZPFZQRLF-UHFFFAOYSA-N 0.000 description 2
- 229910052809 inorganic oxide Inorganic materials 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000002844 melting Methods 0.000 description 2
- 230000008018 melting Effects 0.000 description 2
- 150000002739 metals Chemical class 0.000 description 2
- 239000002808 molecular sieve Substances 0.000 description 2
- 229910052750 molybdenum Inorganic materials 0.000 description 2
- 239000011733 molybdenum Substances 0.000 description 2
- 229910052680 mordenite Inorganic materials 0.000 description 2
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 2
- LXPCOISGJFXEJE-UHFFFAOYSA-N oxifentorex Chemical compound C=1C=CC=CC=1C[N+](C)([O-])C(C)CC1=CC=CC=C1 LXPCOISGJFXEJE-UHFFFAOYSA-N 0.000 description 2
- 238000005191 phase separation Methods 0.000 description 2
- CPRMKOQKXYSDML-UHFFFAOYSA-M rubidium hydroxide Chemical compound [OH-].[Rb+] CPRMKOQKXYSDML-UHFFFAOYSA-M 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- ZCUFMDLYAMJYST-UHFFFAOYSA-N thorium dioxide Chemical compound O=[Th]=O ZCUFMDLYAMJYST-UHFFFAOYSA-N 0.000 description 2
- 229910003452 thorium oxide Inorganic materials 0.000 description 2
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 2
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 2
- 229910052721 tungsten Inorganic materials 0.000 description 2
- 239000010937 tungsten Substances 0.000 description 2
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 description 1
- RPZANUYHRMRTTE-UHFFFAOYSA-N 2,3,4-trimethoxy-6-(methoxymethyl)-5-[3,4,5-trimethoxy-6-(methoxymethyl)oxan-2-yl]oxyoxane;1-[[3,4,5-tris(2-hydroxybutoxy)-6-[4,5,6-tris(2-hydroxybutoxy)-2-(2-hydroxybutoxymethyl)oxan-3-yl]oxyoxan-2-yl]methoxy]butan-2-ol Chemical compound COC1C(OC)C(OC)C(COC)OC1OC1C(OC)C(OC)C(OC)OC1COC.CCC(O)COC1C(OCC(O)CC)C(OCC(O)CC)C(COCC(O)CC)OC1OC1C(OCC(O)CC)C(OCC(O)CC)C(OCC(O)CC)OC1COCC(O)CC RPZANUYHRMRTTE-UHFFFAOYSA-N 0.000 description 1
- FRWYFWZENXDZMU-UHFFFAOYSA-N 2-iodoquinoline Chemical compound C1=CC=CC2=NC(I)=CC=C21 FRWYFWZENXDZMU-UHFFFAOYSA-N 0.000 description 1
- 239000005995 Aluminium silicate Substances 0.000 description 1
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonium chloride Substances [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 1
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 1
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 1
- 229920000896 Ethulose Polymers 0.000 description 1
- 239000001859 Ethyl hydroxyethyl cellulose Substances 0.000 description 1
- 108010010803 Gelatin Proteins 0.000 description 1
- 229920003108 Methocel™ A4M Polymers 0.000 description 1
- MXRIRQGCELJRSN-UHFFFAOYSA-N O.O.O.[Al] Chemical compound O.O.O.[Al] MXRIRQGCELJRSN-UHFFFAOYSA-N 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 238000013019 agitation Methods 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical group [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 description 1
- 235000012211 aluminium silicate Nutrition 0.000 description 1
- JYIBXUUINYLWLR-UHFFFAOYSA-N aluminum;calcium;potassium;silicon;sodium;trihydrate Chemical compound O.O.O.[Na].[Al].[Si].[K].[Ca] JYIBXUUINYLWLR-UHFFFAOYSA-N 0.000 description 1
- 235000011114 ammonium hydroxide Nutrition 0.000 description 1
- 229910021417 amorphous silicon Inorganic materials 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- QKCDTYMOGWZDHX-UHFFFAOYSA-N azanide;platinum(4+) Chemical compound N[Pt](N)(N)N QKCDTYMOGWZDHX-UHFFFAOYSA-N 0.000 description 1
- LTPBRCUWZOMYOC-UHFFFAOYSA-N beryllium oxide Inorganic materials O=[Be] LTPBRCUWZOMYOC-UHFFFAOYSA-N 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 229910052804 chromium Inorganic materials 0.000 description 1
- 239000011651 chromium Substances 0.000 description 1
- 239000004927 clay Substances 0.000 description 1
- 230000003749 cleanliness Effects 0.000 description 1
- 229910001603 clinoptilolite Inorganic materials 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 239000010779 crude oil Substances 0.000 description 1
- 239000008121 dextrose Substances 0.000 description 1
- GUJOJGAPFQRJSV-UHFFFAOYSA-N dialuminum;dioxosilane;oxygen(2-);hydrate Chemical compound O.[O-2].[O-2].[O-2].[Al+3].[Al+3].O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O GUJOJGAPFQRJSV-UHFFFAOYSA-N 0.000 description 1
- IJKVHSBPTUYDLN-UHFFFAOYSA-N dihydroxy(oxo)silane Chemical compound O[Si](O)=O IJKVHSBPTUYDLN-UHFFFAOYSA-N 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 229910052675 erionite Inorganic materials 0.000 description 1
- 235000019326 ethyl hydroxyethyl cellulose Nutrition 0.000 description 1
- 239000012013 faujasite Substances 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 239000003063 flame retardant Substances 0.000 description 1
- 238000007701 flash-distillation Methods 0.000 description 1
- 238000005194 fractionation Methods 0.000 description 1
- 239000000295 fuel oil Substances 0.000 description 1
- ZZUFCTLCJUWOSV-UHFFFAOYSA-N furosemide Chemical compound C1=C(Cl)C(S(=O)(=O)N)=CC(C(O)=O)=C1NCC1=CC=CO1 ZZUFCTLCJUWOSV-UHFFFAOYSA-N 0.000 description 1
- 239000000499 gel Substances 0.000 description 1
- 239000008273 gelatin Substances 0.000 description 1
- 229920000159 gelatin Polymers 0.000 description 1
- 235000019322 gelatine Nutrition 0.000 description 1
- 235000011852 gelatine desserts Nutrition 0.000 description 1
- 229940119177 germanium dioxide Drugs 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
- 229920003063 hydroxymethyl cellulose Polymers 0.000 description 1
- 229940031574 hydroxymethyl cellulose Drugs 0.000 description 1
- 238000005470 impregnation Methods 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910044991 metal oxide Inorganic materials 0.000 description 1
- 150000004706 metal oxides Chemical class 0.000 description 1
- 229910052901 montmorillonite Inorganic materials 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 1
- 235000011837 pasties Nutrition 0.000 description 1
- 235000020030 perry Nutrition 0.000 description 1
- FFNMBRCFFADNAO-UHFFFAOYSA-N pirenzepine hydrochloride Chemical compound [H+].[H+].[Cl-].[Cl-].C1CN(C)CCN1CC(=O)N1C2=NC=CC=C2NC(=O)C2=CC=CC=C21 FFNMBRCFFADNAO-UHFFFAOYSA-N 0.000 description 1
- 239000004014 plasticizer Substances 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 102220076896 rs767072861 Human genes 0.000 description 1
- 229910001953 rubidium(I) oxide Inorganic materials 0.000 description 1
- HSFQBFMEWSTNOW-UHFFFAOYSA-N sodium;carbanide Chemical group [CH3-].[Na+] HSFQBFMEWSTNOW-UHFFFAOYSA-N 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 150000003568 thioethers Chemical class 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- 239000004408 titanium dioxide Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G45/00—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds
- C10G45/58—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to change the structural skeleton of some of the hydrocarbon content without cracking the other hydrocarbons present, e.g. lowering pour point; Selective hydrocracking of normal paraffins
- C10G45/60—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to change the structural skeleton of some of the hydrocarbon content without cracking the other hydrocarbons present, e.g. lowering pour point; Selective hydrocracking of normal paraffins characterised by the catalyst used
- C10G45/64—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to change the structural skeleton of some of the hydrocarbon content without cracking the other hydrocarbons present, e.g. lowering pour point; Selective hydrocracking of normal paraffins characterised by the catalyst used containing crystalline alumino-silicates, e.g. molecular sieves
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J29/00—Catalysts comprising molecular sieves
- B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
- B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J29/00—Catalysts comprising molecular sieves
- B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
- B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
- B01J29/40—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11, as exemplified by patent documents US3702886, GB1334243 and US3709979, respectively
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
- B01J2229/10—After treatment, characterised by the effect to be obtained
- B01J2229/16—After treatment, characterised by the effect to be obtained to increase the Si/Al ratio; Dealumination
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
- B01J2229/30—After treatment, characterised by the means used
- B01J2229/32—Reaction with silicon compounds, e.g. TEOS, siliconfluoride
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
- B01J2229/30—After treatment, characterised by the means used
- B01J2229/42—Addition of matrix or binder particles
Landscapes
- Chemical & Material Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Materials Engineering (AREA)
- General Chemical & Material Sciences (AREA)
- Catalysts (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
- Silicates, Zeolites, And Molecular Sieves (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP98402839 | 1998-11-16 | ||
| EP99402401 | 1999-09-27 | ||
| PCT/EP1999/009024 WO2000029511A1 (en) | 1998-11-16 | 1999-11-12 | Catalytic dewaxing process |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| PL348352A1 PL348352A1 (en) | 2002-05-20 |
| PL191326B1 true PL191326B1 (pl) | 2006-04-28 |
Family
ID=26151742
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PL348352A PL191326B1 (pl) | 1998-11-16 | 1999-11-12 | Kompozycja katalizatora, sposób wytwarzania kompozycji katalizatora oraz zastosowanie kompozycji katalizatora do usuwania wosku z wsadu węglowodorowego |
Country Status (14)
| Country | Link |
|---|---|
| US (1) | US6576120B1 (enExample) |
| EP (1) | EP1137741B1 (enExample) |
| JP (1) | JP2002530470A (enExample) |
| CN (2) | CN1264954C (enExample) |
| AT (1) | ATE305499T1 (enExample) |
| AU (1) | AU754266B2 (enExample) |
| CA (1) | CA2350581C (enExample) |
| DE (1) | DE69927519T2 (enExample) |
| DK (1) | DK1137741T3 (enExample) |
| ES (1) | ES2251249T3 (enExample) |
| HU (1) | HUP0104314A3 (enExample) |
| PL (1) | PL191326B1 (enExample) |
| RU (1) | RU2235115C2 (enExample) |
| WO (1) | WO2000029511A1 (enExample) |
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| US6709570B1 (en) | 1999-09-27 | 2004-03-23 | Shell Oil Company | Method for preparing a catalyst |
| RU2263706C2 (ru) | 2000-07-17 | 2005-11-10 | Шелл Интернэшнл Рисерч Маатсхаппий Б.В. | Способ получения бесцветного смазочного базового масла |
| JP4496633B2 (ja) | 2000-09-29 | 2010-07-07 | 東ソー株式会社 | トリエチレンジアミン製造用成形体触媒とその製造法及びトリエチレンジアミンの製造方法 |
| CA2432034A1 (en) | 2000-12-19 | 2002-06-27 | Shell Internationale Research Maatschappij B.V. | Process to prepare a spindle oil, light machine oil and a medium machine oil |
| DK1370633T3 (da) | 2001-02-13 | 2005-11-21 | Shell Int Research | Smöremiddelsammensætning |
| AR032932A1 (es) | 2001-03-05 | 2003-12-03 | Shell Int Research | Procedimiento para preparar un aceite de base lubricante y un gas oil |
| MY139353A (en) | 2001-03-05 | 2009-09-30 | Shell Int Research | Process to prepare a lubricating base oil and a gas oil |
| AR032941A1 (es) | 2001-03-05 | 2003-12-03 | Shell Int Research | Un procedimiento para preparar un aceite base lubricante y aceite base obtenido, con sus diversas utilizaciones |
| CN1503835A (zh) | 2001-04-19 | 2004-06-09 | ���ʿ����о�����˾ | 一种制备高饱和物含量基油的方法 |
| TWI277649B (en) | 2001-06-07 | 2007-04-01 | Shell Int Research | Process to prepare a base oil from slack-wax |
| BR0213160A (pt) | 2001-10-16 | 2004-09-14 | Shell Int Research | Processo para beneficiamento adicional de um óleo lubrificante usado pré-processado |
| EP1487942B2 (en) | 2002-02-25 | 2011-08-24 | Shell Internationale Research Maatschappij B.V. | Process to prepare a catalytically dewaxed gas oil or gas oil blending component |
| EP1666569B1 (en) | 2002-07-12 | 2018-12-26 | Shell International Research Maatschappij B.V. | Lubricant formulation and its use |
| BR0312667B1 (pt) | 2002-07-18 | 2012-11-27 | processo para preparar uma cera microcristalina e um combustìvel de destilado médio. | |
| KR20050025627A (ko) | 2002-07-19 | 2005-03-14 | 쉘 인터내셔날 리써취 마트샤피지 비.브이. | Ｅｐｄｍ 및 파라핀계 오일을 함유하는 조성물 |
| CN1723263A (zh) | 2002-12-09 | 2006-01-18 | 国际壳牌研究有限公司 | 润滑剂的生产方法 |
| MXPA05005975A (es) * | 2002-12-09 | 2005-08-18 | Shell Int Research | Proceso para la preparacion de un combustible base que tiene un indice de viscosidad de entre 80 y 140. |
| EP1464396A1 (en) * | 2003-03-10 | 2004-10-06 | Shell Internationale Researchmaatschappij B.V. | Process for preparing a lubricating base oil and a gas oil |
| US7141529B2 (en) * | 2003-03-21 | 2006-11-28 | Chevron U.S.A. Inc. | Metal loaded microporous material for hydrocarbon isomerization processes |
| US7815789B2 (en) * | 2003-06-23 | 2010-10-19 | Shell Oil Company | Process to prepare a lubricating base oil |
| CN100358979C (zh) * | 2003-06-27 | 2008-01-02 | 国际壳牌研究有限公司 | 制备润滑基础油的方法 |
| RU2258733C2 (ru) * | 2003-10-06 | 2005-08-20 | ОАО "Всероссийский научно-исследовательский институт по переработке нефти" | Способ получения основы смазочных масел |
| EP1548088A1 (en) | 2003-12-23 | 2005-06-29 | Shell Internationale Researchmaatschappij B.V. | Process to prepare a haze free base oil |
| EP1720959B1 (en) * | 2004-02-26 | 2008-06-04 | Shell Internationale Researchmaatschappij B.V. | Process to prepare a lubricating base oil |
| EP1733008A1 (en) * | 2004-03-02 | 2006-12-20 | Shell Internationale Researchmaatschappij B.V. | Process to continuously prepare two or more base oil grades and middle distillates |
| WO2005085394A1 (en) | 2004-03-02 | 2005-09-15 | Shell Internationale Research Maatschappij B.V. | Process to continuously prepare two or more base oil grades and middle distillates |
| ITMI20040798A1 (it) * | 2004-04-23 | 2004-07-23 | Eni Spa | Processo e catalizzatori per l'apertura di anelli naftenici |
| RU2006146061A (ru) | 2004-05-26 | 2008-07-10 | Шелл Интернэшнл Рисерч Маатсхаппий Б.В. (NL) | Алифатический компонент бензина и способ его получения |
| US20060068986A1 (en) * | 2004-09-27 | 2006-03-30 | Dimascio Felice | Catalyst elements and methods of making and using |
| BRPI0517784A (pt) | 2004-11-18 | 2008-10-21 | Shell Int Research | processo para otimizar o rendimento de gasóleos |
| RU2007122455A (ru) | 2004-11-18 | 2008-12-27 | Шелл Интернэшнл Рисерч Маашелл Интернэшнл Рисерч Маатсхаппий Б.В. (Nсхаппий Б.В. (Nl)L) | Способ получения базового масла |
| US20060129013A1 (en) * | 2004-12-09 | 2006-06-15 | Abazajian Armen N | Specific functionalization and scission of linear hydrocarbon chains |
| EP1853682A1 (en) * | 2004-12-23 | 2007-11-14 | Shell Internationale Research Maatschappij B.V. | Process to prepare a lubricating base oil |
| WO2007003623A1 (en) | 2005-07-01 | 2007-01-11 | Shell Internationale Research Maatschappij B.V. | Process to prepare a blended brightstock |
| EA200800523A1 (ru) * | 2005-08-04 | 2008-08-29 | Шеврон Ю.Эс.Эй. Инк. | Способ депарафинизации с использованием цеолитов мтт и gon |
| US20070278134A1 (en) * | 2006-06-01 | 2007-12-06 | Chevron U.S.A. Inc. | Process for producing light neutral base oil having a high viscosity index |
| CN101134170B (zh) * | 2006-08-31 | 2010-08-25 | 中国石油化工股份有限公司 | 一种催化脱蜡催化剂及其制备方法 |
| EP1997868A1 (en) * | 2007-05-30 | 2008-12-03 | Shell Internationale Researchmaatschappij B.V. | Process for producing a naphthenic base oil |
| KR101519409B1 (ko) * | 2007-09-10 | 2015-05-13 | 쉘 인터내셔날 리써취 마트샤피지 비.브이. | Ｚｓｍ-5, 이의 제조 및 에틸벤젠 탈알킬화에서의 이의 용도 |
| EP2075314A1 (en) | 2007-12-11 | 2009-07-01 | Shell Internationale Research Maatschappij B.V. | Grease formulations |
| US8152868B2 (en) | 2007-12-20 | 2012-04-10 | Shell Oil Company | Fuel compositions |
| US8152869B2 (en) | 2007-12-20 | 2012-04-10 | Shell Oil Company | Fuel compositions |
| US8343335B2 (en) * | 2008-02-21 | 2013-01-01 | Exxonmobil Research And Engineering Company | Production of shaped silica bodies |
| CN102105225A (zh) | 2008-07-04 | 2011-06-22 | 国际壳牌研究有限公司 | 催化剂和异构化方法 |
| JP5564769B2 (ja) * | 2008-08-12 | 2014-08-06 | 株式会社明電舎 | 低級炭化水素芳香族化触媒及び芳香族化合物の製造方法 |
| JP5587003B2 (ja) * | 2010-03-25 | 2014-09-10 | 日本碍子株式会社 | ゼオライト構造体の製造方法 |
| RU2581043C2 (ru) * | 2010-10-25 | 2016-04-10 | Шелл Интернэшнл Рисерч Маатсхаппий Б.В. | Композиция для катализатора конверсии углеводородов |
| EP2455161A1 (en) | 2010-11-18 | 2012-05-23 | Shell Internationale Research Maatschappij B.V. | Isomerisation catalyst preparation process |
| EP2455160A1 (en) * | 2010-11-18 | 2012-05-23 | Shell Internationale Research Maatschappij B.V. | Isomerisation catalyst preparation process |
| WO2013090534A1 (en) * | 2011-12-16 | 2013-06-20 | Shell Oil Company | A titania-bound zsm-12 zeolite composition and method of making and using such composition |
| WO2013127592A1 (en) * | 2012-02-29 | 2013-09-06 | Shell Internationale Research Maatschappij B.V. | A titania-bound zeolite eu-2 catalyst composition and method of making and using such composition |
| BR112014031227A8 (pt) | 2012-06-21 | 2020-09-24 | Shell Int Research | composição lubrificante, uso de uma composição lubrificante, e, uso de um material de mistura aromático alquilado |
| US20150144528A1 (en) | 2012-06-28 | 2015-05-28 | Shell Oil Company | Process to prepare a gas oil fraction and a residual base oil |
| RU2674703C2 (ru) * | 2012-12-17 | 2018-12-12 | Шелл Интернэшнл Рисерч Маатсхаппий Б.В. | Способ получения гидрированного воска |
| EP2746367A1 (en) | 2012-12-18 | 2014-06-25 | Shell Internationale Research Maatschappij B.V. | Process to prepare base oil and gas oil |
| EP3063254A1 (en) | 2013-10-31 | 2016-09-07 | Shell Internationale Research Maatschappij B.V. | Process for the conversion of a paraffinic feedstock |
| WO2016044646A1 (en) | 2014-09-17 | 2016-03-24 | Ergon, Inc. | Process for producing naphthenic bright stocks |
| EP3194533A1 (en) | 2014-09-17 | 2017-07-26 | Ergon, Inc. | Process for producing naphthenic base oils |
| WO2017109179A1 (en) | 2015-12-23 | 2017-06-29 | Shell Internationale Research Maatschappij B.V. | Process for preparing a base oil having a reduced cloud point |
| US11529618B2 (en) * | 2016-11-28 | 2022-12-20 | Basf Se | Catalyst composite comprising an alkaline earth metal containing CHA zeolite and use thereof in a process for the conversion of oxygenates to olefins |
| RU2768876C2 (ru) | 2016-12-16 | 2022-03-25 | Шелл Интернэшнл Рисерч Маатсхаппий Б.В. | Каталитическая система для депарафинизации |
| EP3559158B1 (en) | 2016-12-23 | 2022-08-03 | Shell Internationale Research Maatschappij B.V. | Method for producing fischer-tropsch feedstock derived haze-free base oil fractions |
| US11078430B2 (en) | 2016-12-23 | 2021-08-03 | Shell Oil Company | Haze-free base oils with high paraffinic content |
| US11351528B2 (en) | 2018-04-17 | 2022-06-07 | Shell Usa, Inc. | Catalyst system for dewaxing |
| WO2023247624A1 (en) | 2022-06-22 | 2023-12-28 | Shell Internationale Research Maatschappij B.V. | A process to prepare kerosene |
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1999
- 1999-11-12 US US09/856,038 patent/US6576120B1/en not_active Expired - Lifetime
- 1999-11-12 WO PCT/EP1999/009024 patent/WO2000029511A1/en not_active Ceased
- 1999-11-12 DK DK99962151T patent/DK1137741T3/da active
- 1999-11-12 DE DE69927519T patent/DE69927519T2/de not_active Expired - Lifetime
- 1999-11-12 CN CN99814636.6A patent/CN1264954C/zh not_active Expired - Lifetime
- 1999-11-12 JP JP2000582498A patent/JP2002530470A/ja not_active Ceased
- 1999-11-12 HU HU0104314A patent/HUP0104314A3/hu unknown
- 1999-11-12 CN CN200410059025.5A patent/CN1597860A/zh active Pending
- 1999-11-12 ES ES99962151T patent/ES2251249T3/es not_active Expired - Lifetime
- 1999-11-12 AU AU18594/00A patent/AU754266B2/en not_active Ceased
- 1999-11-12 RU RU2001116572/04A patent/RU2235115C2/ru active
- 1999-11-12 AT AT99962151T patent/ATE305499T1/de not_active IP Right Cessation
- 1999-11-12 EP EP99962151A patent/EP1137741B1/en not_active Revoked
- 1999-11-12 PL PL348352A patent/PL191326B1/pl unknown
- 1999-11-12 CA CA002350581A patent/CA2350581C/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| ES2251249T3 (es) | 2006-04-16 |
| EP1137741A1 (en) | 2001-10-04 |
| PL348352A1 (en) | 2002-05-20 |
| ATE305499T1 (de) | 2005-10-15 |
| CN1597860A (zh) | 2005-03-23 |
| DE69927519T2 (de) | 2006-06-14 |
| US6576120B1 (en) | 2003-06-10 |
| DE69927519D1 (de) | 2006-02-09 |
| CA2350581C (en) | 2009-12-29 |
| RU2235115C2 (ru) | 2004-08-27 |
| CN1264954C (zh) | 2006-07-19 |
| HUP0104314A2 (hu) | 2002-03-28 |
| AU754266B2 (en) | 2002-11-07 |
| WO2000029511A1 (en) | 2000-05-25 |
| AU1859400A (en) | 2000-06-05 |
| DK1137741T3 (da) | 2006-02-13 |
| CN1330699A (zh) | 2002-01-09 |
| JP2002530470A (ja) | 2002-09-17 |
| EP1137741B1 (en) | 2005-09-28 |
| HUP0104314A3 (en) | 2003-05-28 |
| CA2350581A1 (en) | 2000-05-25 |
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