NO125629B - - Google Patents
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- Publication number
- NO125629B NO125629B NO165161A NO16516166A NO125629B NO 125629 B NO125629 B NO 125629B NO 165161 A NO165161 A NO 165161A NO 16516166 A NO16516166 A NO 16516166A NO 125629 B NO125629 B NO 125629B
- Authority
- NO
- Norway
- Prior art keywords
- reaction
- aluminum
- alcohol
- aluminum chloride
- minutes
- Prior art date
Links
- 238000006243 chemical reaction Methods 0.000 claims description 22
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 20
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 20
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical compound Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 claims description 18
- 229910052782 aluminium Inorganic materials 0.000 claims description 15
- 238000000034 method Methods 0.000 claims description 11
- 239000003054 catalyst Substances 0.000 claims description 5
- BRMYZIKAHFEUFJ-UHFFFAOYSA-L mercury diacetate Chemical compound CC(=O)O[Hg]OC(C)=O BRMYZIKAHFEUFJ-UHFFFAOYSA-L 0.000 claims description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- 238000004519 manufacturing process Methods 0.000 claims description 4
- 125000004432 carbon atom Chemical group C* 0.000 claims description 2
- 238000010438 heat treatment Methods 0.000 description 10
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 8
- 229910052739 hydrogen Inorganic materials 0.000 description 8
- 239000001257 hydrogen Substances 0.000 description 8
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 6
- 239000011541 reaction mixture Substances 0.000 description 6
- 238000010992 reflux Methods 0.000 description 6
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 5
- 238000001816 cooling Methods 0.000 description 4
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 4
- 239000007787 solid Substances 0.000 description 4
- 230000015572 biosynthetic process Effects 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 150000001298 alcohols Chemical class 0.000 description 2
- 239000003153 chemical reaction reagent Substances 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 239000007858 starting material Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 150000001299 aldehydes Chemical class 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 150000004703 alkoxides Chemical class 0.000 description 1
- 125000002915 carbonyl group Chemical group [*:2]C([*:1])=O 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 239000011888 foil Substances 0.000 description 1
- XMBWDFGMSWQBCA-UHFFFAOYSA-N hydrogen iodide Chemical compound I XMBWDFGMSWQBCA-UHFFFAOYSA-N 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 229960002523 mercuric chloride Drugs 0.000 description 1
- 229960003671 mercuric iodide Drugs 0.000 description 1
- LWJROJCJINYWOX-UHFFFAOYSA-L mercury dichloride Chemical compound Cl[Hg]Cl LWJROJCJINYWOX-UHFFFAOYSA-L 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
- C07C249/04—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
- C07C249/08—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes by reaction of hydroxylamines with carbonyl compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C251/00—Compounds containing nitrogen atoms doubly-bound to a carbon skeleton
- C07C251/32—Oximes
- C07C251/34—Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals
- C07C251/44—Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals with the carbon atom of at least one of the oxyimino groups being part of a ring other than a six-membered aromatic ring
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NL6513426A NL6513426A (pt) | 1965-10-16 | 1965-10-16 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| NO125629B true NO125629B (pt) | 1972-10-09 |
Family
ID=19794388
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO165161A NO125629B (pt) | 1965-10-16 | 1966-10-14 |
Country Status (12)
| Country | Link |
|---|---|
| AT (1) | AT265240B (pt) |
| BE (1) | BE688260A (pt) |
| CH (1) | CH481888A (pt) |
| DE (1) | DE1272288B (pt) |
| DK (1) | DK117701B (pt) |
| ES (1) | ES332252A1 (pt) |
| FR (1) | FR1496435A (pt) |
| GB (1) | GB1138750A (pt) |
| IL (1) | IL26663A (pt) |
| NL (1) | NL6513426A (pt) |
| NO (1) | NO125629B (pt) |
| SE (1) | SE338985B (pt) |
Families Citing this family (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL135679C (pt) * | 1968-11-12 | 1900-01-01 | ||
| NL6914306A (pt) * | 1969-09-20 | 1971-03-23 | ||
| US3862230A (en) * | 1969-09-20 | 1975-01-21 | Stamicarbon | Continuous preparation of cyclohexanone oxime |
| DE2029114C2 (de) * | 1970-06-12 | 1982-07-01 | Stamicarbon B.V., 6160 Geleen | Verfahren zur Herstellung von Cyclohexanonoxim |
| US3625835A (en) * | 1970-06-15 | 1971-12-07 | Stamicarbon | Process for the recovery of cyclohexanone oxime by plural stage, vacuum distillation per a |
| NL7008838A (pt) * | 1970-06-17 | 1971-12-21 | ||
| DE2508247C3 (de) * | 1975-02-26 | 1981-03-12 | Basf Ag, 6700 Ludwigshafen | Verfahren zur Herstellung von Cyclohexanonoxim |
| US4104359A (en) * | 1977-02-28 | 1978-08-01 | Amax Inc. | Regeneration of organic extractants containing α-hydroxyoximes |
| DE3942334A1 (de) * | 1989-12-21 | 1991-06-27 | Basf Ag | Verfahren zur aufarbeitung von salzsaeure, schwefelsaeure und deren hydroxylammonium- und ammoniumsalze enthaltenden waessrigen mutterlaugen |
| US5254734A (en) * | 1991-02-13 | 1993-10-19 | Mitsubishi Kasei Corporation | Method for preparing an oxime |
| KR100843925B1 (ko) * | 2000-06-05 | 2008-07-03 | 디에스엠 아이피 어셋츠 비.브이. | 시클로헥사논 옥심의 제조방법 |
| EP1299353B1 (en) | 2000-06-05 | 2006-04-12 | DSM IP Assets B.V. | Process for the preparation of cyclohexanone oxime |
| EP1318141A1 (en) | 2001-12-04 | 2003-06-11 | Dsm Nv | Process for treating an aqueous medium containing phosphate, cyclohexanone and cyclohexanone oxime |
| DE60210500T2 (de) * | 2001-12-04 | 2006-11-30 | Dsm Ip Assets B.V. | Verfahren zur behandlung eines phosphatsalzes und organische verbindungen enthaltendes wässriges medium |
| WO2003048110A1 (en) | 2001-12-04 | 2003-06-12 | Dsm Ip Assets B.V. | Process for treating an aqueous medium containing cyclohexanone oxime and cyclohexanone |
| KR101078927B1 (ko) * | 2003-01-30 | 2011-11-01 | 디에스엠 아이피 어셋츠 비.브이. | 사이클로헥산온 옥심, 사이클로헥산온 및 유기 용매를포함하는 유기 용액을 처리하는 방법 |
| TW200829544A (en) * | 2007-01-05 | 2008-07-16 | China Petrochemical Dev Corp | Method for preparing cyclohexanone oxime |
| CN103193672B (zh) * | 2013-03-11 | 2014-09-17 | 浙江圣安化工有限公司 | 一种肟的蒸馏方法 |
| CN105384656B (zh) * | 2015-10-23 | 2017-08-25 | 中石化南京工程有限公司 | 一种环己酮肟化的方法 |
| CN105348145B (zh) * | 2015-10-23 | 2018-02-06 | 中石化南京工程有限公司 | 氨法烟气脱硫副产环己酮肟的方法 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2270204A (en) * | 1938-11-28 | 1942-01-13 | Du Pont | Process of producing oximes |
| DE1081884B (de) * | 1959-02-13 | 1960-05-19 | Basf Ag | Verfahren zur Herstellung von Cyclododecanonoxim |
| GB972107A (en) * | 1962-09-01 | 1964-10-07 | Basf Ag | Production of oximes of cycloaliphatic ketones |
| NL301053A (pt) * | 1963-11-27 |
-
1965
- 1965-10-16 NL NL6513426A patent/NL6513426A/xx unknown
-
1966
- 1966-10-06 GB GB44743/66A patent/GB1138750A/en not_active Expired
- 1966-10-07 DE DEP1272A patent/DE1272288B/de active Pending
- 1966-10-07 AT AT942866A patent/AT265240B/de active
- 1966-10-10 IL IL26663A patent/IL26663A/xx unknown
- 1966-10-10 CH CH1454566A patent/CH481888A/de not_active IP Right Cessation
- 1966-10-12 FR FR79609A patent/FR1496435A/fr not_active Expired
- 1966-10-14 BE BE688260D patent/BE688260A/xx not_active IP Right Cessation
- 1966-10-14 SE SE14007/66A patent/SE338985B/xx unknown
- 1966-10-14 ES ES0332252A patent/ES332252A1/es not_active Expired
- 1966-10-14 NO NO165161A patent/NO125629B/no unknown
- 1966-10-17 DK DK535566AA patent/DK117701B/da unknown
Also Published As
| Publication number | Publication date |
|---|---|
| DK117701B (da) | 1970-05-25 |
| GB1138750A (en) | 1969-01-01 |
| FR1496435A (fr) | 1967-09-29 |
| AT265240B (de) | 1968-10-10 |
| DE1272288B (de) | 1968-07-11 |
| SE338985B (pt) | 1971-09-27 |
| ES332252A1 (es) | 1967-07-16 |
| IL26663A (en) | 1970-09-17 |
| NL6513426A (pt) | 1967-04-17 |
| CH481888A (de) | 1969-11-30 |
| BE688260A (pt) | 1967-04-14 |
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