NL186572C - Werkwijze ter bereiding van aromatische isocyanaten. - Google Patents
Werkwijze ter bereiding van aromatische isocyanaten.Info
- Publication number
- NL186572C NL186572C NLAANVRAGE7608745,A NL7608745A NL186572C NL 186572 C NL186572 C NL 186572C NL 7608745 A NL7608745 A NL 7608745A NL 186572 C NL186572 C NL 186572C
- Authority
- NL
- Netherlands
- Prior art keywords
- aromatic
- metal
- formula
- reduced pressure
- under reduced
- Prior art date
Links
- 239000012948 isocyanate Substances 0.000 title abstract 4
- 150000002513 isocyanates Chemical class 0.000 title 1
- 238000004519 manufacturing process Methods 0.000 title 1
- -1 aromatic isocyanates Chemical class 0.000 abstract 3
- 125000003118 aryl group Chemical group 0.000 abstract 3
- 239000002184 metal Substances 0.000 abstract 2
- KXDHJXZQYSOELW-UHFFFAOYSA-M Carbamate Chemical compound NC([O-])=O KXDHJXZQYSOELW-UHFFFAOYSA-M 0.000 abstract 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 abstract 1
- 125000002723 alicyclic group Chemical group 0.000 abstract 1
- 125000001931 aliphatic group Chemical group 0.000 abstract 1
- 125000004432 carbon atom Chemical group C* 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 239000012442 inert solvent Substances 0.000 abstract 1
- 150000002736 metal compounds Chemical class 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C263/00—Preparation of derivatives of isocyanic acid
- C07C263/04—Preparation of derivatives of isocyanic acid from or via carbamates or carbamoyl halides
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP50096056A JPS5219624A (en) | 1975-08-07 | 1975-08-07 | Process for preparation of isocyanates |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| NL7608745A NL7608745A (nl) | 1977-02-09 |
| NL186572B NL186572B (nl) | 1990-08-01 |
| NL186572C true NL186572C (nl) | 1991-01-02 |
Family
ID=14154777
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NLAANVRAGE7608745,A NL186572C (nl) | 1975-08-07 | 1976-08-06 | Werkwijze ter bereiding van aromatische isocyanaten. |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US4081472A (OSRAM) |
| JP (1) | JPS5219624A (OSRAM) |
| BE (1) | BE844967A (OSRAM) |
| CA (1) | CA1082728A (OSRAM) |
| DE (1) | DE2635490C3 (OSRAM) |
| FR (1) | FR2320288A1 (OSRAM) |
| GB (1) | GB1513193A (OSRAM) |
| IT (1) | IT1065802B (OSRAM) |
| NL (1) | NL186572C (OSRAM) |
Families Citing this family (60)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5488222A (en) * | 1977-12-20 | 1979-07-13 | Mitsubishi Chem Ind Ltd | Preparation of isocyanate from carbamate |
| DE2756928A1 (de) * | 1977-12-21 | 1979-07-05 | Bayer Ag | Verfahren zur kontinuierlichen herstellung von monoisocyanaten |
| DE2904917A1 (de) * | 1979-02-09 | 1980-08-21 | Basf Ag | Verfahren zur herstellung von methylenbis-(4-phenylcarbaminsaeureester) |
| DE2917569A1 (de) * | 1979-04-30 | 1980-11-13 | Basf Ag | Verfahren zur herstellung von aromatischen di- und polyurethanen |
| DE2917493A1 (de) * | 1979-04-30 | 1980-11-13 | Basf Ag | Verfahren zur herstellung von aliphatischen und cycloaliphatischen di- und polyurethanen |
| US4851565A (en) * | 1979-04-30 | 1989-07-25 | Basf Aktiengesellschaft | Catalyzed process for the preparation of an aliphatic, cycloaliphatic, arylaliphatic or aliphatic-cycloaliphatic di- or polyurethane |
| DE2942503A1 (de) * | 1979-10-20 | 1981-05-07 | Basf Ag, 6700 Ludwigshafen | Verfahren zur herstellung von aromatischen di- und/oder polyisocyanaten |
| DE2942543A1 (de) * | 1979-10-20 | 1981-05-07 | Basf Ag, 6700 Ludwigshafen | Verfahren zur herstellung von arylisocyanaten durch thermische spaltung von arylurethanen |
| JPS5679657A (en) * | 1979-12-04 | 1981-06-30 | Mitsui Toatsu Chem Inc | Novel preparation of polyisocyanate |
| US4321402A (en) * | 1980-08-18 | 1982-03-23 | Exxon Research & Engineering Co. | Carbamate process |
| US4294774A (en) * | 1980-11-14 | 1981-10-13 | The Dow Chemical Company | Preparation of organic isocyanates |
| DE3047898A1 (de) * | 1980-12-19 | 1982-07-15 | Bayer Ag, 5090 Leverkusen | Verfahren zur kontinuierlichen thermischen spaltung von carbamidsaeureestern und die verwendung von hierbei anfallenden isocyanate und carbamidsaeureester aufweisenden gemischen zur herstellung von isocyanaten |
| JPS57158746A (en) * | 1981-03-25 | 1982-09-30 | Asahi Chem Ind Co Ltd | Preparation of isocyanate |
| JPS57158748A (en) * | 1981-03-26 | 1982-09-30 | Asahi Chem Ind Co Ltd | Preparation of isocyanate |
| JPS57158747A (en) * | 1981-03-26 | 1982-09-30 | Asahi Chem Ind Co Ltd | Preparation of isocyanate |
| US4487713A (en) * | 1981-06-26 | 1984-12-11 | Exxon Research & Engineering Co. | Production of isocyanates from esters of aromatic carbamic acids (urethanes) |
| DE3142627A1 (de) * | 1981-10-28 | 1983-05-05 | Basf Ag, 6700 Ludwigshafen | Verfahren zur herstellung von isocyanaten durch thermische spaltung von urethanen |
| DE3215591A1 (de) * | 1982-04-27 | 1983-10-27 | Bayer Ag, 5090 Leverkusen | Verfahren zur kontinuierlichen thermischen spaltung von carbamidsaeureestern |
| DE3339300A1 (de) * | 1983-10-29 | 1985-05-09 | Basf Ag, 6700 Ludwigshafen | Verfahren zur herstellung von isocyanaten durch thermische spaltung von urethanen |
| US5773643A (en) * | 1987-01-13 | 1998-06-30 | Daicel Chemical Industries, Ltd. | Process for preparation of isocyanate compounds |
| US5914428A (en) * | 1987-01-13 | 1999-06-22 | Daicel Chemical Industries, Ltd. | Process for preparation of isocyanate compounds |
| JPS63211256A (ja) * | 1988-02-12 | 1988-09-02 | Asahi Chem Ind Co Ltd | イソシアナート類の製造方法 |
| DE3915181A1 (de) * | 1989-05-10 | 1990-11-15 | Bayer Ag | Verfahren zur herstellung von polyisocyanaten |
| US5220069A (en) * | 1990-09-20 | 1993-06-15 | Union Carbide Chemicals & Plastics Technology Corporation | Processes for the preparation of carbamates |
| JPH04221356A (ja) * | 1990-12-20 | 1992-08-11 | Mitsubishi Gas Chem Co Inc | キシリレンジイソシアネートの製造方法 |
| DE4124671A1 (de) * | 1991-07-25 | 1993-01-28 | Basf Ag | Reaktor und verfahren zur thermischen spaltung von carbamidsaeureestern |
| DE4137428A1 (de) * | 1991-11-14 | 1993-05-19 | Bayer Ag | Verfahren zur herstellung von polyisocyanaten |
| DE4141402A1 (de) * | 1991-12-16 | 1993-06-17 | Bayer Ag | Verfahren zur herstellung von hochreinen aromatischen di- und/oder polyurethanen |
| US5233010A (en) * | 1992-10-15 | 1993-08-03 | Monsanto Company | Process for preparing isocyanate and carbamate ester products |
| JP3083039B2 (ja) * | 1994-03-18 | 2000-09-04 | 三菱瓦斯化学株式会社 | イソシアネート類の製造方法 |
| EP0680994A1 (en) * | 1994-05-02 | 1995-11-08 | Nippon Paint Co., Ltd. | Re-Crosslinkable composition and method for recycling using the same |
| GB0017968D0 (en) * | 2000-07-22 | 2000-09-13 | Epichem Ltd | An improved process and apparatus for the isolation of pure,or substantially pure,organometallic compounds |
| DE10215778A1 (de) | 2002-04-10 | 2003-12-18 | Basf Ag | Reaktor zur thermischen Spaltung von mono- und polyfunktionellen Carbamidsäureestern |
| DE10338509A1 (de) * | 2003-08-22 | 2005-03-17 | Degussa Ag | Mehrstufiges Verfahren zur kontinuierlichen Herstellung von cycloaliphatischen Diisocyanaten |
| DE10338508A1 (de) * | 2003-08-22 | 2005-03-17 | Degussa Ag | Mehrstufiges Verfahren zur kontinuierlichen Herstellung von cycloaliphatischen Diisocyanaten |
| DE10338511A1 (de) * | 2003-08-22 | 2005-03-17 | Degussa Ag | Mehrstufiges Verfahren zur kontinuierlichen Herstellung von cycloaliphatischen Diisocyanaten |
| DE102004022626A1 (de) * | 2004-05-07 | 2005-12-15 | Degussa Ag | Mehrstufiges Verfahren zur kontinuierlichen Herstellung von cycloaliphatischen Diisocyanaten |
| DE102004026451A1 (de) * | 2004-05-29 | 2005-12-15 | Degussa Ag | Mehrstufiges Verfahren zur kontinuierlichen Herstellung von cycloaliphatischen Diisocyanaten |
| DE102004036499A1 (de) * | 2004-07-28 | 2006-03-23 | Degussa Ag | Mehrstufiges Verfahren zur kontinuierlichen Herstellung von cycloaliphatischen Diisocyanaten |
| US7700250B2 (en) * | 2006-08-30 | 2010-04-20 | Xerox Corporation | Titanyl phthalocyanine photoconductors |
| JP4859255B2 (ja) * | 2006-11-17 | 2012-01-25 | 旭化成ケミカルズ株式会社 | イソシアネートの製造方法 |
| TW200844080A (en) | 2007-01-11 | 2008-11-16 | Asahi Kasei Chemicals Corp | Process for producing isocyanate |
| EP2147909B1 (en) | 2007-03-30 | 2016-12-14 | Asahi Kasei Kabushiki Kaisha | Method for production of isocyanate using composition comprising carbamic acid ester and aromatic hydroxy compound, and composition for transport or storage of carbamic acid ester |
| EP2213658B1 (en) | 2007-11-19 | 2015-09-09 | Asahi Kasei Chemicals Corporation | Method for production of isocyanate and aromatic hydroxy compound |
| EP2275405B1 (en) | 2008-05-15 | 2019-04-24 | Asahi Kasei Kabushiki Kaisha | Process for producing isocyanate using diaryl carbonate |
| WO2009139062A1 (ja) | 2008-05-15 | 2009-11-19 | 旭化成ケミカルズ株式会社 | イソシアネートの製造方法 |
| DE102008002002A1 (de) | 2008-05-27 | 2009-12-03 | Evonik Degussa Gmbh | Chlor armes mehrstufiges Verfahren zur Herstellung von cycloaliphatischen Diisocyanaten |
| WO2010110142A1 (ja) | 2009-03-26 | 2010-09-30 | 三井化学株式会社 | ウレタン化合物およびその製造方法、および、イソシアネートおよびその製造方法 |
| EP3153500B1 (en) | 2009-08-21 | 2019-03-06 | Asahi Kasei Kabushiki Kaisha | Method for producing isocyanate using n-substituted carbamic acid ester, and composition for transferring and storing n-substituted carbamic acid ester containing n-substituted carbamic acid ester and aromatic hydroxy compound |
| JP5643517B2 (ja) * | 2010-02-04 | 2014-12-17 | 三井化学株式会社 | 触媒処理方法 |
| CN101792403B (zh) * | 2010-03-22 | 2013-02-13 | 哈尔滨理工大学 | 微波辅助合成4,4’-二苯甲烷二异氰酸酯的方法 |
| JP2013540101A (ja) * | 2010-06-22 | 2013-10-31 | ビーエーエスエフ ソシエタス・ヨーロピア | イソシアネートの合成のための固体ルイス酸上での不均一系触媒によるカルバメートの解離 |
| JP5760077B2 (ja) | 2011-02-21 | 2015-08-05 | 旭化成ケミカルズ株式会社 | カルボニル化合物の製造方法 |
| CN102896103B (zh) * | 2011-07-25 | 2014-12-03 | 中国石油天然气股份有限公司 | 一种清洗氨基甲酸酯热分解反应器结焦的方法 |
| KR101348229B1 (ko) | 2011-12-14 | 2014-01-08 | 경희대학교 산학협력단 | 지방족 디이소시아네이트의 제조방법 |
| TW201900606A (zh) | 2017-05-15 | 2019-01-01 | 日商旭化成股份有限公司 | 異氰酸酯的製造方法 |
| EP3450424A1 (de) * | 2017-09-04 | 2019-03-06 | Covestro Deutschland AG | Verfahren zur herstellung von isocyanaten |
| CN110467546B (zh) * | 2018-05-10 | 2021-03-19 | 中国科学院过程工程研究所 | 一种制备间苯二亚甲基二异氰酸酯的方法 |
| CN110423208A (zh) * | 2019-08-15 | 2019-11-08 | 中国科学院过程工程研究所 | 一种二苯甲烷二异氰酸酯的制备方法 |
| WO2025013551A1 (ja) * | 2023-07-07 | 2025-01-16 | 国立研究開発法人産業技術総合研究所 | イソシアネートの製造方法 |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2409712A (en) * | 1944-02-03 | 1946-10-22 | Du Pont | Chemical process and products |
| DE1022222B (de) * | 1953-01-23 | 1958-01-09 | Rohm & Haas | Verfahren zur Herstellung von 1,8-Diisocyan-p-menthan |
| US3477933A (en) * | 1966-06-06 | 1969-11-11 | Stauffer Chemical Co | Process for preparing n-monosubstituted carbamic acid esters |
| US3734941A (en) * | 1968-09-06 | 1973-05-22 | American Cyanamid Co | Process for converting urethanes to isocyanates |
| CA1023379A (en) * | 1973-05-04 | 1977-12-27 | Atlantic Richfield Company | Production of isocyanates from esters of carbamic acids (urethanes) |
| US3962302A (en) * | 1974-03-08 | 1976-06-08 | Atlantic Richfield Company | Production of isocyanates from esters of carbamic acids (urethanes) |
| US3919279A (en) * | 1974-06-26 | 1975-11-11 | Atlantic Richfield Co | Catalytic production of isocyanates from esters of carbamic acids |
-
1975
- 1975-08-07 JP JP50096056A patent/JPS5219624A/ja active Granted
-
1976
- 1976-08-05 GB GB32628/76A patent/GB1513193A/en not_active Expired
- 1976-08-05 CA CA258,489A patent/CA1082728A/en not_active Expired
- 1976-08-05 US US05/711,823 patent/US4081472A/en not_active Expired - Lifetime
- 1976-08-06 IT IT26138/76A patent/IT1065802B/it active
- 1976-08-06 NL NLAANVRAGE7608745,A patent/NL186572C/xx not_active IP Right Cessation
- 1976-08-06 BE BE169625A patent/BE844967A/xx not_active IP Right Cessation
- 1976-08-06 DE DE2635490A patent/DE2635490C3/de not_active Expired
- 1976-08-09 FR FR7624337A patent/FR2320288A1/fr active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| GB1513193A (en) | 1978-06-07 |
| BE844967A (fr) | 1977-02-07 |
| FR2320288A1 (fr) | 1977-03-04 |
| NL186572B (nl) | 1990-08-01 |
| NL7608745A (nl) | 1977-02-09 |
| FR2320288B1 (OSRAM) | 1982-07-16 |
| DE2635490B2 (de) | 1980-10-16 |
| JPS5745736B2 (OSRAM) | 1982-09-29 |
| CA1082728A (en) | 1980-07-29 |
| DE2635490A1 (de) | 1977-02-24 |
| DE2635490C3 (de) | 1981-09-17 |
| JPS5219624A (en) | 1977-02-15 |
| IT1065802B (it) | 1985-03-04 |
| US4081472A (en) | 1978-03-28 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| BA | A request for search or an international-type search has been filed | ||
| BB | A search report has been drawn up | ||
| BC | A request for examination has been filed | ||
| A85 | Still pending on 85-01-01 | ||
| V1 | Lapsed because of non-payment of the annual fee |
Effective date: 19960301 |