FR2320288A1 - Procede pour la preparation d'isocyanates aromatiques - Google Patents
Procede pour la preparation d'isocyanates aromatiquesInfo
- Publication number
- FR2320288A1 FR2320288A1 FR7624337A FR7624337A FR2320288A1 FR 2320288 A1 FR2320288 A1 FR 2320288A1 FR 7624337 A FR7624337 A FR 7624337A FR 7624337 A FR7624337 A FR 7624337A FR 2320288 A1 FR2320288 A1 FR 2320288A1
- Authority
- FR
- France
- Prior art keywords
- aromatic
- metal
- formula
- reduced pressure
- under reduced
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C263/00—Preparation of derivatives of isocyanic acid
- C07C263/04—Preparation of derivatives of isocyanic acid from or via carbamates or carbamoyl halides
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP50096056A JPS5219624A (en) | 1975-08-07 | 1975-08-07 | Process for preparation of isocyanates |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| FR2320288A1 true FR2320288A1 (fr) | 1977-03-04 |
| FR2320288B1 FR2320288B1 (OSRAM) | 1982-07-16 |
Family
ID=14154777
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| FR7624337A Granted FR2320288A1 (fr) | 1975-08-07 | 1976-08-09 | Procede pour la preparation d'isocyanates aromatiques |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US4081472A (OSRAM) |
| JP (1) | JPS5219624A (OSRAM) |
| BE (1) | BE844967A (OSRAM) |
| CA (1) | CA1082728A (OSRAM) |
| DE (1) | DE2635490C3 (OSRAM) |
| FR (1) | FR2320288A1 (OSRAM) |
| GB (1) | GB1513193A (OSRAM) |
| IT (1) | IT1065802B (OSRAM) |
| NL (1) | NL186572C (OSRAM) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0054817A3 (en) * | 1980-12-19 | 1982-08-18 | Bayer Ag | Process for the continuous thermal decomposition of esters of carbamic acids and use of mixtures of esters of carbamic acids and isocyanates obtained by this process for the preparation of isocyanates |
| EP0078005A1 (de) * | 1981-10-28 | 1983-05-04 | BASF Aktiengesellschaft | Verfahren zur Herstellung von Isocyanaten durch thermische Spaltung von Urethanen |
Families Citing this family (58)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5488222A (en) * | 1977-12-20 | 1979-07-13 | Mitsubishi Chem Ind Ltd | Preparation of isocyanate from carbamate |
| DE2756928A1 (de) * | 1977-12-21 | 1979-07-05 | Bayer Ag | Verfahren zur kontinuierlichen herstellung von monoisocyanaten |
| DE2904917A1 (de) * | 1979-02-09 | 1980-08-21 | Basf Ag | Verfahren zur herstellung von methylenbis-(4-phenylcarbaminsaeureester) |
| DE2917493A1 (de) * | 1979-04-30 | 1980-11-13 | Basf Ag | Verfahren zur herstellung von aliphatischen und cycloaliphatischen di- und polyurethanen |
| US4851565A (en) * | 1979-04-30 | 1989-07-25 | Basf Aktiengesellschaft | Catalyzed process for the preparation of an aliphatic, cycloaliphatic, arylaliphatic or aliphatic-cycloaliphatic di- or polyurethane |
| DE2917569A1 (de) * | 1979-04-30 | 1980-11-13 | Basf Ag | Verfahren zur herstellung von aromatischen di- und polyurethanen |
| DE2942543A1 (de) * | 1979-10-20 | 1981-05-07 | Basf Ag, 6700 Ludwigshafen | Verfahren zur herstellung von arylisocyanaten durch thermische spaltung von arylurethanen |
| DE2942503A1 (de) * | 1979-10-20 | 1981-05-07 | Basf Ag, 6700 Ludwigshafen | Verfahren zur herstellung von aromatischen di- und/oder polyisocyanaten |
| JPS5679657A (en) * | 1979-12-04 | 1981-06-30 | Mitsui Toatsu Chem Inc | Novel preparation of polyisocyanate |
| US4321402A (en) * | 1980-08-18 | 1982-03-23 | Exxon Research & Engineering Co. | Carbamate process |
| US4294774A (en) * | 1980-11-14 | 1981-10-13 | The Dow Chemical Company | Preparation of organic isocyanates |
| JPS57158746A (en) * | 1981-03-25 | 1982-09-30 | Asahi Chem Ind Co Ltd | Preparation of isocyanate |
| JPS57158748A (en) * | 1981-03-26 | 1982-09-30 | Asahi Chem Ind Co Ltd | Preparation of isocyanate |
| JPS57158747A (en) * | 1981-03-26 | 1982-09-30 | Asahi Chem Ind Co Ltd | Preparation of isocyanate |
| US4487713A (en) * | 1981-06-26 | 1984-12-11 | Exxon Research & Engineering Co. | Production of isocyanates from esters of aromatic carbamic acids (urethanes) |
| DE3215591A1 (de) * | 1982-04-27 | 1983-10-27 | Bayer Ag, 5090 Leverkusen | Verfahren zur kontinuierlichen thermischen spaltung von carbamidsaeureestern |
| DE3339300A1 (de) * | 1983-10-29 | 1985-05-09 | Basf Ag, 6700 Ludwigshafen | Verfahren zur herstellung von isocyanaten durch thermische spaltung von urethanen |
| US5914428A (en) * | 1987-01-13 | 1999-06-22 | Daicel Chemical Industries, Ltd. | Process for preparation of isocyanate compounds |
| US5773643A (en) * | 1987-01-13 | 1998-06-30 | Daicel Chemical Industries, Ltd. | Process for preparation of isocyanate compounds |
| JPS63211256A (ja) * | 1988-02-12 | 1988-09-02 | Asahi Chem Ind Co Ltd | イソシアナート類の製造方法 |
| DE3915181A1 (de) * | 1989-05-10 | 1990-11-15 | Bayer Ag | Verfahren zur herstellung von polyisocyanaten |
| US5220069A (en) * | 1990-09-20 | 1993-06-15 | Union Carbide Chemicals & Plastics Technology Corporation | Processes for the preparation of carbamates |
| JPH04221356A (ja) * | 1990-12-20 | 1992-08-11 | Mitsubishi Gas Chem Co Inc | キシリレンジイソシアネートの製造方法 |
| DE4124671A1 (de) * | 1991-07-25 | 1993-01-28 | Basf Ag | Reaktor und verfahren zur thermischen spaltung von carbamidsaeureestern |
| DE4137428A1 (de) * | 1991-11-14 | 1993-05-19 | Bayer Ag | Verfahren zur herstellung von polyisocyanaten |
| DE4141402A1 (de) * | 1991-12-16 | 1993-06-17 | Bayer Ag | Verfahren zur herstellung von hochreinen aromatischen di- und/oder polyurethanen |
| US5233010A (en) * | 1992-10-15 | 1993-08-03 | Monsanto Company | Process for preparing isocyanate and carbamate ester products |
| JP3083039B2 (ja) * | 1994-03-18 | 2000-09-04 | 三菱瓦斯化学株式会社 | イソシアネート類の製造方法 |
| EP0680994A1 (en) * | 1994-05-02 | 1995-11-08 | Nippon Paint Co., Ltd. | Re-Crosslinkable composition and method for recycling using the same |
| GB0017968D0 (en) * | 2000-07-22 | 2000-09-13 | Epichem Ltd | An improved process and apparatus for the isolation of pure,or substantially pure,organometallic compounds |
| DE10215778A1 (de) | 2002-04-10 | 2003-12-18 | Basf Ag | Reaktor zur thermischen Spaltung von mono- und polyfunktionellen Carbamidsäureestern |
| DE10338511A1 (de) * | 2003-08-22 | 2005-03-17 | Degussa Ag | Mehrstufiges Verfahren zur kontinuierlichen Herstellung von cycloaliphatischen Diisocyanaten |
| DE10338508A1 (de) * | 2003-08-22 | 2005-03-17 | Degussa Ag | Mehrstufiges Verfahren zur kontinuierlichen Herstellung von cycloaliphatischen Diisocyanaten |
| DE10338509A1 (de) * | 2003-08-22 | 2005-03-17 | Degussa Ag | Mehrstufiges Verfahren zur kontinuierlichen Herstellung von cycloaliphatischen Diisocyanaten |
| DE102004022626A1 (de) * | 2004-05-07 | 2005-12-15 | Degussa Ag | Mehrstufiges Verfahren zur kontinuierlichen Herstellung von cycloaliphatischen Diisocyanaten |
| DE102004026451A1 (de) * | 2004-05-29 | 2005-12-15 | Degussa Ag | Mehrstufiges Verfahren zur kontinuierlichen Herstellung von cycloaliphatischen Diisocyanaten |
| DE102004036499A1 (de) * | 2004-07-28 | 2006-03-23 | Degussa Ag | Mehrstufiges Verfahren zur kontinuierlichen Herstellung von cycloaliphatischen Diisocyanaten |
| US7700250B2 (en) * | 2006-08-30 | 2010-04-20 | Xerox Corporation | Titanyl phthalocyanine photoconductors |
| TWI361179B (en) * | 2006-11-17 | 2012-04-01 | Asahi Kasei Chemicals Corp | A process for producing isocyanates |
| TW200844080A (en) | 2007-01-11 | 2008-11-16 | Asahi Kasei Chemicals Corp | Process for producing isocyanate |
| CN101652344B (zh) | 2007-03-30 | 2014-06-04 | 旭化成化学株式会社 | 使用含有氨基甲酸酯和芳香族羟基化合物的组合物制造异氰酸酯的方法、以及氨基甲酸酯输送用和储藏用组合物 |
| JP5313164B2 (ja) | 2007-11-19 | 2013-10-09 | 旭化成ケミカルズ株式会社 | イソシアネートおよび芳香族ヒドロキシ化合物の製造方法 |
| US8895774B2 (en) * | 2008-05-15 | 2014-11-25 | Asahi Kasei Chemicals Corporation | Process for producing isocyanates using diaryl carbonate |
| KR20130127550A (ko) | 2008-05-15 | 2013-11-22 | 아사히 가세이 케미칼즈 가부시키가이샤 | 이소시아네이트의 제조 방법 |
| DE102008002002A1 (de) | 2008-05-27 | 2009-12-03 | Evonik Degussa Gmbh | Chlor armes mehrstufiges Verfahren zur Herstellung von cycloaliphatischen Diisocyanaten |
| US9150502B2 (en) | 2009-03-26 | 2015-10-06 | Mitsui Chemicals, Inc. | Urethane compound and method for producing the same, and isocyanate and method for producing the same |
| KR101332485B1 (ko) | 2009-08-21 | 2013-11-26 | 아사히 가세이 케미칼즈 가부시키가이샤 | N-치환 카르밤산 에스테르의 제조 방법 및 상기 n-치환 카르밤산 에스테르를 사용하는 이소시아네이트의 제조 방법 |
| JP5643517B2 (ja) * | 2010-02-04 | 2014-12-17 | 三井化学株式会社 | 触媒処理方法 |
| CN101792403B (zh) * | 2010-03-22 | 2013-02-13 | 哈尔滨理工大学 | 微波辅助合成4,4’-二苯甲烷二异氰酸酯的方法 |
| WO2011161029A1 (de) * | 2010-06-22 | 2011-12-29 | Basf Se | Heterogen katalysierte carbamatspaltung zur synthese von isocyanaten an festen lewis-säuren |
| EP2679575B1 (en) | 2011-02-21 | 2019-04-10 | Asahi Kasei Kabushiki Kaisha | Process for producing carbonyl compounds |
| CN102896103B (zh) * | 2011-07-25 | 2014-12-03 | 中国石油天然气股份有限公司 | 一种清洗氨基甲酸酯热分解反应器结焦的方法 |
| KR101348229B1 (ko) | 2011-12-14 | 2014-01-08 | 경희대학교 산학협력단 | 지방족 디이소시아네이트의 제조방법 |
| WO2018212206A1 (ja) | 2017-05-15 | 2018-11-22 | 旭化成株式会社 | イソシアネートの製造方法 |
| EP3450424A1 (de) * | 2017-09-04 | 2019-03-06 | Covestro Deutschland AG | Verfahren zur herstellung von isocyanaten |
| CN110467546B (zh) * | 2018-05-10 | 2021-03-19 | 中国科学院过程工程研究所 | 一种制备间苯二亚甲基二异氰酸酯的方法 |
| CN110423208A (zh) * | 2019-08-15 | 2019-11-08 | 中国科学院过程工程研究所 | 一种二苯甲烷二异氰酸酯的制备方法 |
| WO2025013551A1 (ja) * | 2023-07-07 | 2025-01-16 | 国立研究開発法人産業技術総合研究所 | イソシアネートの製造方法 |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2409712A (en) * | 1944-02-03 | 1946-10-22 | Du Pont | Chemical process and products |
| DE1022222B (de) * | 1953-01-23 | 1958-01-09 | Rohm & Haas | Verfahren zur Herstellung von 1,8-Diisocyan-p-menthan |
| US3477933A (en) * | 1966-06-06 | 1969-11-11 | Stauffer Chemical Co | Process for preparing n-monosubstituted carbamic acid esters |
| FR2017496A1 (OSRAM) * | 1968-09-06 | 1970-05-22 | American Cyanamid Co | |
| FR2228056A1 (OSRAM) * | 1973-05-04 | 1974-11-29 | Atlantic Richfield Co | |
| US3919279A (en) * | 1974-06-26 | 1975-11-11 | Atlantic Richfield Co | Catalytic production of isocyanates from esters of carbamic acids |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3962302A (en) * | 1974-03-08 | 1976-06-08 | Atlantic Richfield Company | Production of isocyanates from esters of carbamic acids (urethanes) |
-
1975
- 1975-08-07 JP JP50096056A patent/JPS5219624A/ja active Granted
-
1976
- 1976-08-05 GB GB32628/76A patent/GB1513193A/en not_active Expired
- 1976-08-05 CA CA258,489A patent/CA1082728A/en not_active Expired
- 1976-08-05 US US05/711,823 patent/US4081472A/en not_active Expired - Lifetime
- 1976-08-06 IT IT26138/76A patent/IT1065802B/it active
- 1976-08-06 BE BE169625A patent/BE844967A/xx not_active IP Right Cessation
- 1976-08-06 NL NLAANVRAGE7608745,A patent/NL186572C/xx not_active IP Right Cessation
- 1976-08-06 DE DE2635490A patent/DE2635490C3/de not_active Expired
- 1976-08-09 FR FR7624337A patent/FR2320288A1/fr active Granted
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2409712A (en) * | 1944-02-03 | 1946-10-22 | Du Pont | Chemical process and products |
| DE1022222B (de) * | 1953-01-23 | 1958-01-09 | Rohm & Haas | Verfahren zur Herstellung von 1,8-Diisocyan-p-menthan |
| US3477933A (en) * | 1966-06-06 | 1969-11-11 | Stauffer Chemical Co | Process for preparing n-monosubstituted carbamic acid esters |
| FR2017496A1 (OSRAM) * | 1968-09-06 | 1970-05-22 | American Cyanamid Co | |
| FR2228056A1 (OSRAM) * | 1973-05-04 | 1974-11-29 | Atlantic Richfield Co | |
| US3919279A (en) * | 1974-06-26 | 1975-11-11 | Atlantic Richfield Co | Catalytic production of isocyanates from esters of carbamic acids |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0054817A3 (en) * | 1980-12-19 | 1982-08-18 | Bayer Ag | Process for the continuous thermal decomposition of esters of carbamic acids and use of mixtures of esters of carbamic acids and isocyanates obtained by this process for the preparation of isocyanates |
| EP0078005A1 (de) * | 1981-10-28 | 1983-05-04 | BASF Aktiengesellschaft | Verfahren zur Herstellung von Isocyanaten durch thermische Spaltung von Urethanen |
Also Published As
| Publication number | Publication date |
|---|---|
| CA1082728A (en) | 1980-07-29 |
| IT1065802B (it) | 1985-03-04 |
| JPS5219624A (en) | 1977-02-15 |
| NL7608745A (nl) | 1977-02-09 |
| JPS5745736B2 (OSRAM) | 1982-09-29 |
| DE2635490B2 (de) | 1980-10-16 |
| DE2635490A1 (de) | 1977-02-24 |
| NL186572B (nl) | 1990-08-01 |
| NL186572C (nl) | 1991-01-02 |
| GB1513193A (en) | 1978-06-07 |
| US4081472A (en) | 1978-03-28 |
| FR2320288B1 (OSRAM) | 1982-07-16 |
| BE844967A (fr) | 1977-02-07 |
| DE2635490C3 (de) | 1981-09-17 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| ST | Notification of lapse |