MY118128A - The preparation of 1, 6-hexanediol and caprolactone - Google Patents

The preparation of 1, 6-hexanediol and caprolactone

Info

Publication number
MY118128A
MY118128A MYPI97000759A MYPI9700759A MY118128A MY 118128 A MY118128 A MY 118128A MY PI97000759 A MYPI97000759 A MY PI97000759A MY PI9700759 A MYPI9700759 A MY PI9700759A MY 118128 A MY118128 A MY 118128A
Authority
MY
Malaysia
Prior art keywords
ester
caprolactone
hydroxycaproic
hexanediol
fraction
Prior art date
Application number
MYPI97000759A
Other languages
English (en)
Inventor
Boris Breitscheidel
Frank Stein
Harald Rust
Karl Gerhard Baur
Rolf Fischer
Rolf Pinkos
Original Assignee
Basf Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from DE1996107954 external-priority patent/DE19607954A1/de
Priority claimed from DE1996147349 external-priority patent/DE19647349A1/de
Application filed by Basf Ag filed Critical Basf Ag
Publication of MY118128A publication Critical patent/MY118128A/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D315/00—Heterocyclic compounds containing rings having one oxygen atom as the only ring hetero atom according to more than one of groups C07D303/00 - C07D313/00
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
    • C07C29/136—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH
    • C07C29/147—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of carboxylic acids or derivatives thereof
    • C07C29/149—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group of >C=O containing groups, e.g. —COOH of carboxylic acids or derivatives thereof with hydrogen or hydrogen-containing gases
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/88—Separation; Purification; Use of additives, e.g. for stabilisation by treatment giving rise to a chemical modification of at least one compound
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C31/18—Polyhydroxylic acyclic alcohols
    • C07C31/20—Dihydroxylic alcohols
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/31—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting
    • C07C51/313—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting with molecular oxygen
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D313/00—Heterocyclic compounds containing rings of more than six members having one oxygen atom as the only ring hetero atom
    • C07D313/02—Seven-membered rings
    • C07D313/04—Seven-membered rings not condensed with other rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Polyesters Or Polycarbonates (AREA)
  • Pyrane Compounds (AREA)
MYPI97000759A 1996-03-01 1997-02-27 The preparation of 1, 6-hexanediol and caprolactone MY118128A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE1996107954 DE19607954A1 (de) 1996-03-01 1996-03-01 Verfahren zur Herstellung von 1,6-Hexandiol und Caprolacton
DE1996147349 DE19647349A1 (de) 1996-11-15 1996-11-15 Verfahren zur Herstellung von 1,6-Hexandiol und Caprolacton

Publications (1)

Publication Number Publication Date
MY118128A true MY118128A (en) 2004-09-30

Family

ID=26023397

Family Applications (1)

Application Number Title Priority Date Filing Date
MYPI97000759A MY118128A (en) 1996-03-01 1997-02-27 The preparation of 1, 6-hexanediol and caprolactone

Country Status (13)

Country Link
US (1) US5981769A (enExample)
EP (1) EP0883591B1 (enExample)
JP (1) JP4107396B2 (enExample)
KR (1) KR100468182B1 (enExample)
CN (1) CN1089742C (enExample)
AT (1) ATE192730T1 (enExample)
CA (1) CA2248004C (enExample)
DE (1) DE59701646D1 (enExample)
ES (1) ES2147435T3 (enExample)
GR (1) GR3033955T3 (enExample)
MY (1) MY118128A (enExample)
PT (1) PT883591E (enExample)
WO (1) WO1997031883A1 (enExample)

Families Citing this family (43)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19757554A1 (de) 1997-12-23 1999-06-24 Basf Ag Verfahren zur Herstellung von 1,6-Hexandiol
DE19826614A1 (de) * 1998-05-29 1999-12-02 Basf Ag Verfahren zur Herstellung von Hexandiol-1,6
WO2000006528A1 (en) * 1998-07-30 2000-02-10 Sumitomo Chemical Company, Limited Process for producing adipic acid
ATE318803T1 (de) * 2000-08-24 2006-03-15 Union Carbide Chem Plastic Verfahren zur herstellung von laktonen
DE10100552A1 (de) * 2001-01-09 2002-07-11 Basf Ag Verfahren und Vorrichtung zur destillativen Aufarbeitung von 1,6-Hexandiol, 1,5-Pentandiol ung Caprolacton
DE10128249A1 (de) * 2001-06-11 2002-12-12 Basf Ag Verfahren zur Entfernung von Ameisensäure aus wässrigen Lösungen
DE10242882A1 (de) * 2002-09-16 2004-03-25 Basf Ag Verfahren zur Herstellung von 1,6-Hexandiol
BR0315969B1 (pt) * 2002-11-01 2013-03-19 processo para preparaÇço de 1,3-propanodiol.
US7794960B2 (en) * 2004-06-04 2010-09-14 Glaxosmithkline Llc Predictive biomarkers in cancer therapy
DE102004033557A1 (de) 2004-07-09 2006-02-16 Basf Ag Verfahren zur Herstellung von 1,6-Hexandiol in einer Reinheit von über 99,5%
DE102004054047A1 (de) 2004-11-05 2006-05-11 Basf Ag Verfahren zur Herstellung von 1,6-Hexandiol
DE602005019546D1 (de) * 2005-06-03 2010-04-08 Univ Twente Verzweigte Polymere, ein makromonomer, Verfahren zu deren Herstellungen und deren Verwendungen
US8304585B2 (en) * 2006-01-13 2012-11-06 Ube Industries, Ltd. Production process of 1,6-hexanediol
JP2010529159A (ja) * 2007-06-14 2010-08-26 ビーエーエスエフ ソシエタス・ヨーロピア ε−カプロラクトンの製造法
EP2217587B1 (de) * 2007-11-05 2015-09-23 Basf Se Verfahren zur herstellung von e-caprolacton
CA2708174A1 (en) 2007-12-21 2009-07-02 Basf Se Process for preparing e-caprolactone
CA2714574A1 (en) 2008-02-15 2009-08-20 Basf Se Process for preparing 6-hydroxycaproic esters
KR100922998B1 (ko) * 2008-03-06 2009-10-22 한국화학연구원 모노카르복실산 또는 그의 유도체로부터 일가 알콜의 제조방법
US8828903B2 (en) * 2008-11-10 2014-09-09 Basf Corporation Copper catalyst for dehydrogenation application
ES2395225T3 (es) * 2008-12-05 2013-02-11 Basf Se Método para preparar 1,6-hexandiol
BRPI0916168A2 (pt) * 2008-12-18 2015-11-03 Invista Tech Sarl "composição, agente de cura, lama de perfuração, removedor de tinta, extrator fotorresistente, removedor de grafite, limpador, método para dissolver uma resina, método para endurecer um substrato friável, poliéster e solvente"
WO2010079187A1 (de) 2009-01-12 2010-07-15 Basf Se Verfahren zur herstellung von polymethylolen
CN102388010B (zh) * 2009-04-07 2015-04-08 巴斯夫欧洲公司 生产1,6-己二醇和己内酯的方法
CA2755696A1 (en) * 2009-04-07 2010-10-14 Basf Se Method for producing 1,6-hexanediol
TWI490034B (zh) 2009-11-17 2015-07-01 Basf Se 製備具有增強氫化活性之經承載氫化觸媒之方法
WO2011159551A1 (en) 2010-06-16 2011-12-22 Bioamber S.A.S. Processes for the production of hydrogenated products and derivatives thereof
WO2011159562A1 (en) 2010-06-16 2011-12-22 Bioamber S.A.S. Processes for the production of hydrogenated products and derivatives thereof
EP2404889A1 (de) * 2010-07-06 2012-01-11 LANXESS Deutschland GmbH Verfahren zur Herstellung von Alpha, Omega-Diolen
WO2012038848A1 (en) * 2010-09-08 2012-03-29 Basf Se PROCESS FOR PREPARING ε- EPSILON-CAPROLACTONE AND 1,6- HEXANEDIOL
US20120059174A1 (en) * 2010-09-08 2012-03-08 Basf Se Process for preparing epsilon-caprolactone and 1,6-hexanediol
US8889922B2 (en) 2011-12-30 2014-11-18 E I Du Pont De Nemours And Company Process for preparing 1, 6-hexanediol
US8981130B2 (en) 2011-12-30 2015-03-17 E I Du Pont De Nemours And Company Process for the production of hexanediols
US8884036B2 (en) 2011-12-30 2014-11-11 E I Du Pont De Nemours And Company Production of hydroxymethylfurfural from levoglucosenone
US8865940B2 (en) 2011-12-30 2014-10-21 E I Du Pont De Nemours And Company Process for preparing 1,6-hexanediol
US8889912B2 (en) 2011-12-30 2014-11-18 E I Du Pont De Nemours And Company Process for preparing 1,6-hexanediol
JP2015508401A (ja) 2011-12-30 2015-03-19 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニーＥ．Ｉ．Ｄｕ Ｐｏｎｔ Ｄｅ Ｎｅｍｏｕｒｓ Ａｎｄ Ｃｏｍｐａｎｙ イソソルビドからのテトラヒドロフラン−２，５−ジメタノールの生成
CN102603447B (zh) * 2012-02-13 2014-09-03 湖南大学 一种制备有机内酯的方法
CN102603446B (zh) * 2012-02-13 2014-08-06 湖南大学 一种以碳材料催化氧化有机酮制备有机内酯的方法
US9018423B2 (en) 2012-04-27 2015-04-28 E I Du Pont De Nemours And Company Production of alpha, omega-diols
US8846984B2 (en) 2012-04-27 2014-09-30 E I Du Pont De Nemours And Company Production of α,ω-diols
US8859826B2 (en) 2012-04-27 2014-10-14 E I Du Pont De Nemours And Company Production of alpha, omega-diols
US11208394B2 (en) 2018-09-17 2021-12-28 Regents Of The University Of Minnesota Chemical process to manufacture branched-caprolactone
GB202109710D0 (en) 2021-07-05 2021-08-18 Johnson Matthey Davy Technologies Ltd Separation process for the production of C5 or C6 alkanediol

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1618143C3 (de) * 1967-04-27 1975-08-21 Basf Ag, 6700 Ludwigshafen Verfahren zur Gewinnung von epsilon-Hydroxycapronsäurelacton und von Alkandicarbonsäuren
DE2060548C3 (de) * 1970-12-09 1979-10-11 Basf Ag, 6700 Ludwigshafen Verfahren zur Herstellung von sehr reinem 1,6-Hexandiol durch Kristallisation
DE2321101C2 (de) * 1973-04-26 1982-07-22 Basf Ag, 6700 Ludwigshafen Verfahren zur Herstellung im wesentlichen trägerfreier Kobaltkatalysatoren
US3933930A (en) * 1975-03-06 1976-01-20 Celanese Corporation Hexanediol from cyclohexane
DE2819593C2 (de) * 1978-05-05 1986-12-11 Basf Ag, 6700 Ludwigshafen Verfahren zur rückstandsfreien Herstellung von α,ω-Diolen
DE3823213A1 (de) * 1988-07-08 1990-01-11 Basf Ag Verfahren zur herstellung von caprolacton
ES2131707T3 (es) * 1993-10-08 1999-08-01 Ube Industries Procedimiento para la obtencion de un compuesto diolico.
DE69408813T2 (de) * 1993-12-28 1998-08-06 Ube Industries Verfahren zur Herstellung von Diol-Verbindungen

Also Published As

Publication number Publication date
JP2000506134A (ja) 2000-05-23
PT883591E (pt) 2000-10-31
CA2248004A1 (en) 1997-09-04
GR3033955T3 (en) 2000-11-30
KR100468182B1 (ko) 2005-03-16
CN1211969A (zh) 1999-03-24
CN1089742C (zh) 2002-08-28
DE59701646D1 (de) 2000-06-15
EP0883591A1 (de) 1998-12-16
JP4107396B2 (ja) 2008-06-25
ES2147435T3 (es) 2000-09-01
ATE192730T1 (de) 2000-05-15
EP0883591B1 (de) 2000-05-10
WO1997031883A1 (de) 1997-09-04
CA2248004C (en) 2006-04-11
KR19990087422A (ko) 1999-12-27
US5981769A (en) 1999-11-09

Similar Documents

Publication Publication Date Title
MY118128A (en) The preparation of 1, 6-hexanediol and caprolactone
MY117553A (en) Process for preparing 1, 6 hexane diol with a level of purity over 99%
JPH09509941A (ja) シクロヘキシルアジペートおよびアジピン酸の製造方法
DE69412044D1 (de) Verfahren zur Herstellung von Hydroxyverbindungen durch Hydrierung von sauerstoffenthaltenden Verbindungen
MY116778A (en) Preparation of 1, 6-hexanediol and 6-hydroxycaproic acid and esters thereof
MY124268A (en) Process for preparing esters of carboxylic acids
ATE481375T1 (de) Verfahren zur herstellung von hexandiol - 1,6
US4146741A (en) Conversion of furan to 1,4-butanediol and tetrahydrofuran
EP1049657B1 (en) Process for the preparation of butane-1,4-diol, gamma-butyrolactone and tetrahydrofuran
JP4001861B2 (ja) 水溶液からのギ酸の除去方法
US5844111A (en) Method for purifying an inert gas while preparing lower alkyl esters
JP3059695B2 (ja) シクロヘキサン酸化生成物の洗浄水から二酸を製造する方法
CA2329040A1 (en) Method for producing hexanediol
CA2291445A1 (en) Improved process for recovering hydrogen in producing pure terephthalic acid
JP2003055303A (ja) カプロラクタム製造工程で発生するアルカリ性廃液より炭素原子数４〜６のジカルボン酸のエステル類を製造する方法
CA2247991A1 (en) Process for preparing 1,6 hexane diol with a level of purity over 99 %
US5321155A (en) Process for the production of cyclohexyladipates and adipic acid
US3078316A (en) Production of menthol
US3981931A (en) Diols by transesterification using magnesia catalysts
AU6264600A (en) Method for producing hexanediol
RU2013115238A (ru) СПОСОБ ПОЛУЧЕНИЯ ε-КАПРОЛАКТОНА И 1,6-ГЕКСАНДИОЛА
US3991099A (en) Process for the preparation of mixture consisting predominantly of .epsilon.α-formylvaleric acid and the esters of these acids
US8217191B2 (en) Process for integrated co-production of hydrogen peroxide and epoxidized esters
JPH02111735A (ja) １，４−ブタンジオールの製造方法
JPS5742684A (en) Preparation of epsilon-caprolactone