MX347947B - Metodo y sistema para preparar cloruro de hidrogeno de alta pureza. - Google Patents
Metodo y sistema para preparar cloruro de hidrogeno de alta pureza.Info
- Publication number
- MX347947B MX347947B MX2013009832A MX2013009832A MX347947B MX 347947 B MX347947 B MX 347947B MX 2013009832 A MX2013009832 A MX 2013009832A MX 2013009832 A MX2013009832 A MX 2013009832A MX 347947 B MX347947 B MX 347947B
- Authority
- MX
- Mexico
- Prior art keywords
- hydrogen chloride
- hydrogen
- purity
- preparing high
- chlorine
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B7/00—Halogens; Halogen acids
- C01B7/01—Chlorine; Hydrogen chloride
- C01B7/012—Preparation of hydrogen chloride from the elements
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B7/00—Halogens; Halogen acids
- C01B7/01—Chlorine; Hydrogen chloride
- C01B7/07—Purification ; Separation
- C01B7/0706—Purification ; Separation of hydrogen chloride
- C01B7/0712—Purification ; Separation of hydrogen chloride by distillation
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B7/00—Halogens; Halogen acids
- C01B7/01—Chlorine; Hydrogen chloride
- C01B7/07—Purification ; Separation
- C01B7/0743—Purification ; Separation of gaseous or dissolved chlorine
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/26—Drying gases or vapours
- B01D53/261—Drying gases or vapours by adsorption
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/80—Compositional purity
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Separation By Low-Temperature Treatments (AREA)
- Hydrogen, Water And Hydrids (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
La presente invención proporciona un método para producir cloruro de hidrógeno de alta pureza, que comprende las etapas de: purificar cada uno de hidrógeno crudo y cloro crudo como materias primas a una pureza de 99.999% o superior; hacer reaccionar una cantidad molar en exceso del hidrógeno purificado con el cloro purificado a una temperatura que varía de 1,200 °C a 1,400 °C para sintetizar cloruro de hidrógeno; convertir el cloruro de hidrógeno a un estado líquido por compresión; y purificar el cloruro de hidrógeno y separar el hidrógeno sin reaccionar por destilación fraccionada. La invención también proporciona un sistema para llevar a cabo el método. De acuerdo con el método y sistema, puede proporcionarse un proceso de producción ambientalmente favorable, el cual puede producir fácilmente una gran cantidad de cloruro de hidrógeno que tiene una pureza de 3 N (99.9%) - 6 N (99.9999%) en una forma rentable, y hace posible que el consumo de energía se reduzca significativamente.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
KR1020110103784A KR20130039249A (ko) | 2011-10-11 | 2011-10-11 | 고순도 염화수소 제조방법 및 제조 시스템 |
KR1020110126071A KR101203490B1 (ko) | 2011-11-29 | 2011-11-29 | 고순도 염화수소 제조방법 및 제조 시스템 |
PCT/KR2012/001760 WO2013054989A1 (ko) | 2011-10-11 | 2012-03-09 | 고순도 염화수소 제조 방법 및 제조 시스템 |
Publications (2)
Publication Number | Publication Date |
---|---|
MX2013009832A MX2013009832A (es) | 2013-10-03 |
MX347947B true MX347947B (es) | 2017-05-19 |
Family
ID=48082022
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
MX2013009832A MX347947B (es) | 2011-10-11 | 2012-03-09 | Metodo y sistema para preparar cloruro de hidrogeno de alta pureza. |
Country Status (13)
Country | Link |
---|---|
US (2) | US20130259796A1 (es) |
EP (1) | EP2617678B1 (es) |
JP (1) | JP5756180B2 (es) |
CN (2) | CN103221336A (es) |
AU (1) | AU2012321629B2 (es) |
CA (1) | CA2828446C (es) |
IL (1) | IL228118A (es) |
MX (1) | MX347947B (es) |
MY (1) | MY156181A (es) |
RU (1) | RU2592794C2 (es) |
SG (1) | SG192925A1 (es) |
TW (1) | TWI520906B (es) |
WO (1) | WO2013054989A1 (es) |
Families Citing this family (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP3336057B1 (en) * | 2015-08-10 | 2019-04-10 | Showa Denko K.K. | Method for producing hydrogen chloride |
US20180354789A1 (en) * | 2015-08-10 | 2018-12-13 | Showa Denko K.K. | Method for producing hydrogen chloride |
CN105502294B (zh) * | 2015-12-28 | 2018-11-20 | 青岛科技大学 | 一种电子级高纯氯化氢高压制备方法 |
CN105502295B (zh) * | 2015-12-31 | 2018-11-02 | 上海正帆科技股份有限公司 | 一种电子级氯化氢的提纯方法 |
CN107311184A (zh) * | 2016-04-26 | 2017-11-03 | 内蒙古盾安光伏科技有限公司 | 一种提高冷氢化生产三氯氢硅转化率的生产工艺 |
CN108545700B (zh) * | 2018-04-23 | 2020-03-17 | 大连中鼎化学有限公司 | 一种超纯氯化氢的制备装置及方法 |
CN109336052A (zh) * | 2018-11-23 | 2019-02-15 | 宜宾天原集团股份有限公司 | 用于生产氯化氢的微反应系统及基于该系统的氯化氢生产方法 |
CN110054155A (zh) * | 2019-06-05 | 2019-07-26 | 唐山三友氯碱有限责任公司 | 低水分含量氯化氢合成方法及合成系统 |
CN110255501A (zh) * | 2019-07-11 | 2019-09-20 | 金宏气体电子材料(淮安)有限责任公司 | 一种电子级高纯氯化氢制备方法 |
CN112578745B (zh) * | 2020-09-28 | 2022-01-14 | 山东鲁泰化学有限公司 | 一种氯化氢合成反应过程的智能化控制方法 |
CN117619272B (zh) * | 2023-12-01 | 2024-09-06 | 浙江瑞亨电子材料有限公司 | 一种高纯氯化氢的制备设备以及生产工艺 |
Family Cites Families (24)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2077310A (en) * | 1936-02-01 | 1937-04-13 | Pennsylvania Salt Mfg Co | Process of purifying chlorine |
US2444256A (en) * | 1946-07-19 | 1948-06-29 | Shell Dev | Method for manufacturing hydrogen chloride |
US2664342A (en) * | 1950-11-20 | 1953-12-29 | Shell Dev | Hydrogen halide production |
US3077082A (en) * | 1958-09-04 | 1963-02-12 | Hooker Chemical Corp | Liquefaction of hydrogen chloride |
NL129282C (es) * | 1963-10-21 | |||
US4247532A (en) * | 1979-08-13 | 1981-01-27 | Shell Oil Company | Purification of electrolytically-produced chlorine |
DE3816783A1 (de) * | 1988-05-17 | 1989-11-30 | Wacker Chemie Gmbh | Verfahren zur reinigung von rohem, gasfoermigem chlorwasserstoff |
JP3570732B2 (ja) * | 1991-05-28 | 2004-09-29 | 三井化学株式会社 | 塩素ガスの濃縮方法および装置 |
US5296017A (en) * | 1991-05-28 | 1994-03-22 | Mitsui Toatsu Chemicals, Inc. | Method and apparatus for concentrating chlorine gas |
JP2775364B2 (ja) * | 1991-10-17 | 1998-07-16 | 鶴見曹達株式会社 | 塩酸の合成装置 |
JP2923454B2 (ja) * | 1995-10-03 | 1999-07-26 | 大同ほくさん株式会社 | 水素精製方法およびこれに用いる装置 |
DE19536976A1 (de) * | 1995-10-04 | 1997-04-10 | Basf Ag | Verfahren zur selektiven Abtrennung und Wiedergewinnung von Chlor aus Gasgemischen |
US6340382B1 (en) * | 1999-08-13 | 2002-01-22 | Mohamed Safdar Allie Baksh | Pressure swing adsorption process for the production of hydrogen |
US6896865B2 (en) * | 2000-04-28 | 2005-05-24 | Tosoh Corporation | Method for recovering hydrogen chloride from chlorine based waste and use of recovered hydrogen chloride |
US20040038803A1 (en) * | 2002-02-19 | 2004-02-26 | Derong Zhou | Adsorbent for removing water vapor during corrosive gas purification and method for preparing the adsorbent |
JP2003292304A (ja) * | 2002-03-29 | 2003-10-15 | Sumitomo Chem Co Ltd | 純塩素ガスの製造方法 |
RU2217371C1 (ru) * | 2002-04-24 | 2003-11-27 | Открытое акционерное общество "Химпром" | Способ получения хлористого водорода |
JP4507510B2 (ja) * | 2003-05-21 | 2010-07-21 | 三菱化学株式会社 | 高純度の塩化水素、及びその製造方法 |
JP5219372B2 (ja) * | 2004-09-29 | 2013-06-26 | 昭和電工株式会社 | 高純度液化塩素の製造方法 |
CN101395088B (zh) * | 2006-02-03 | 2012-04-04 | Grt公司 | 轻气体与卤素的分离方法 |
US20070261437A1 (en) * | 2006-05-12 | 2007-11-15 | Boonstra Eric F | Enhanced process for the purification of anhydrous hydrogen chloride gas |
RU2325321C2 (ru) * | 2006-05-15 | 2008-05-27 | Открытое акционерное общество "Каустик" (ОАО "Каустик") | Способ осушки газообразного хлора |
US20070269690A1 (en) * | 2006-05-22 | 2007-11-22 | Doshi Kishore J | Control system, process and apparatus for hydrogen production from reforming |
CN101948094A (zh) * | 2010-10-18 | 2011-01-19 | 天津市泰亨气体有限公司 | 一种高纯氯化氢的合成技术 |
-
2012
- 2012-02-09 MY MYPI2013003145A patent/MY156181A/en unknown
- 2012-03-09 US US13/825,089 patent/US20130259796A1/en not_active Abandoned
- 2012-03-09 WO PCT/KR2012/001760 patent/WO2013054989A1/ko active Application Filing
- 2012-03-09 CA CA2828446A patent/CA2828446C/en active Active
- 2012-03-09 JP JP2013538671A patent/JP5756180B2/ja active Active
- 2012-03-09 CN CN2012800029460A patent/CN103221336A/zh active Pending
- 2012-03-09 EP EP12830913.5A patent/EP2617678B1/en active Active
- 2012-03-09 SG SG2013064027A patent/SG192925A1/en unknown
- 2012-03-09 MX MX2013009832A patent/MX347947B/es active IP Right Grant
- 2012-03-09 CN CN201610965803.XA patent/CN107021456A/zh active Pending
- 2012-03-09 AU AU2012321629A patent/AU2012321629B2/en active Active
- 2012-03-09 RU RU2013146601/05A patent/RU2592794C2/ru active
- 2012-03-28 TW TW101110774A patent/TWI520906B/zh active
-
2013
- 2013-08-26 IL IL228118A patent/IL228118A/en active IP Right Grant
-
2021
- 2021-07-06 US US17/368,795 patent/US20210331919A1/en not_active Abandoned
Also Published As
Publication number | Publication date |
---|---|
CN107021456A (zh) | 2017-08-08 |
EP2617678B1 (en) | 2019-07-31 |
RU2592794C2 (ru) | 2016-07-27 |
EP2617678A1 (en) | 2013-07-24 |
US20210331919A1 (en) | 2021-10-28 |
JP5756180B2 (ja) | 2015-07-29 |
IL228118A0 (en) | 2013-09-30 |
MX2013009832A (es) | 2013-10-03 |
JP2013545704A (ja) | 2013-12-26 |
TW201315682A (zh) | 2013-04-16 |
CA2828446C (en) | 2019-05-07 |
SG192925A1 (en) | 2013-09-30 |
RU2013146601A (ru) | 2015-11-20 |
AU2012321629A1 (en) | 2013-09-05 |
MY156181A (en) | 2016-01-15 |
US20130259796A1 (en) | 2013-10-03 |
CN103221336A (zh) | 2013-07-24 |
EP2617678A4 (en) | 2014-03-05 |
IL228118A (en) | 2015-11-30 |
TWI520906B (zh) | 2016-02-11 |
CA2828446A1 (en) | 2013-04-18 |
AU2012321629B2 (en) | 2014-10-16 |
WO2013054989A1 (ko) | 2013-04-18 |
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Legal Events
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FG | Grant or registration |