MX347947B - Metodo y sistema para preparar cloruro de hidrogeno de alta pureza. - Google Patents

Metodo y sistema para preparar cloruro de hidrogeno de alta pureza.

Info

Publication number
MX347947B
MX347947B MX2013009832A MX2013009832A MX347947B MX 347947 B MX347947 B MX 347947B MX 2013009832 A MX2013009832 A MX 2013009832A MX 2013009832 A MX2013009832 A MX 2013009832A MX 347947 B MX347947 B MX 347947B
Authority
MX
Mexico
Prior art keywords
hydrogen chloride
hydrogen
purity
preparing high
chlorine
Prior art date
Application number
MX2013009832A
Other languages
English (en)
Other versions
MX2013009832A (es
Inventor
Kun Lee Jae
Yong Lee Bum
Original Assignee
Hong-In Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from KR1020110103784A external-priority patent/KR20130039249A/ko
Priority claimed from KR1020110126071A external-priority patent/KR101203490B1/ko
Application filed by Hong-In Chemical Co Ltd filed Critical Hong-In Chemical Co Ltd
Publication of MX2013009832A publication Critical patent/MX2013009832A/es
Publication of MX347947B publication Critical patent/MX347947B/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B7/00—Halogens; Halogen acids
    • C01B7/01—Chlorine; Hydrogen chloride
    • C01B7/012—Preparation of hydrogen chloride from the elements
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B7/00—Halogens; Halogen acids
    • C01B7/01—Chlorine; Hydrogen chloride
    • C01B7/07—Purification ; Separation
    • C01B7/0706—Purification ; Separation of hydrogen chloride
    • C01B7/0712—Purification ; Separation of hydrogen chloride by distillation
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B7/00—Halogens; Halogen acids
    • C01B7/01—Chlorine; Hydrogen chloride
    • C01B7/07—Purification ; Separation
    • C01B7/0743—Purification ; Separation of gaseous or dissolved chlorine
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/26—Drying gases or vapours
    • B01D53/261—Drying gases or vapours by adsorption
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/80—Compositional purity

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Separation By Low-Temperature Treatments (AREA)
  • Hydrogen, Water And Hydrids (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

La presente invención proporciona un método para producir cloruro de hidrógeno de alta pureza, que comprende las etapas de: purificar cada uno de hidrógeno crudo y cloro crudo como materias primas a una pureza de 99.999% o superior; hacer reaccionar una cantidad molar en exceso del hidrógeno purificado con el cloro purificado a una temperatura que varía de 1,200 °C a 1,400 °C para sintetizar cloruro de hidrógeno; convertir el cloruro de hidrógeno a un estado líquido por compresión; y purificar el cloruro de hidrógeno y separar el hidrógeno sin reaccionar por destilación fraccionada. La invención también proporciona un sistema para llevar a cabo el método. De acuerdo con el método y sistema, puede proporcionarse un proceso de producción ambientalmente favorable, el cual puede producir fácilmente una gran cantidad de cloruro de hidrógeno que tiene una pureza de 3 N (99.9%) - 6 N (99.9999%) en una forma rentable, y hace posible que el consumo de energía se reduzca significativamente.
MX2013009832A 2011-10-11 2012-03-09 Metodo y sistema para preparar cloruro de hidrogeno de alta pureza. MX347947B (es)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
KR1020110103784A KR20130039249A (ko) 2011-10-11 2011-10-11 고순도 염화수소 제조방법 및 제조 시스템
KR1020110126071A KR101203490B1 (ko) 2011-11-29 2011-11-29 고순도 염화수소 제조방법 및 제조 시스템
PCT/KR2012/001760 WO2013054989A1 (ko) 2011-10-11 2012-03-09 고순도 염화수소 제조 방법 및 제조 시스템

Publications (2)

Publication Number Publication Date
MX2013009832A MX2013009832A (es) 2013-10-03
MX347947B true MX347947B (es) 2017-05-19

Family

ID=48082022

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2013009832A MX347947B (es) 2011-10-11 2012-03-09 Metodo y sistema para preparar cloruro de hidrogeno de alta pureza.

Country Status (13)

Country Link
US (2) US20130259796A1 (es)
EP (1) EP2617678B1 (es)
JP (1) JP5756180B2 (es)
CN (2) CN103221336A (es)
AU (1) AU2012321629B2 (es)
CA (1) CA2828446C (es)
IL (1) IL228118A (es)
MX (1) MX347947B (es)
MY (1) MY156181A (es)
RU (1) RU2592794C2 (es)
SG (1) SG192925A1 (es)
TW (1) TWI520906B (es)
WO (1) WO2013054989A1 (es)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
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EP3336057B1 (en) * 2015-08-10 2019-04-10 Showa Denko K.K. Method for producing hydrogen chloride
US20180354789A1 (en) * 2015-08-10 2018-12-13 Showa Denko K.K. Method for producing hydrogen chloride
CN105502294B (zh) * 2015-12-28 2018-11-20 青岛科技大学 一种电子级高纯氯化氢高压制备方法
CN105502295B (zh) * 2015-12-31 2018-11-02 上海正帆科技股份有限公司 一种电子级氯化氢的提纯方法
CN107311184A (zh) * 2016-04-26 2017-11-03 内蒙古盾安光伏科技有限公司 一种提高冷氢化生产三氯氢硅转化率的生产工艺
CN108545700B (zh) * 2018-04-23 2020-03-17 大连中鼎化学有限公司 一种超纯氯化氢的制备装置及方法
CN109336052A (zh) * 2018-11-23 2019-02-15 宜宾天原集团股份有限公司 用于生产氯化氢的微反应系统及基于该系统的氯化氢生产方法
CN110054155A (zh) * 2019-06-05 2019-07-26 唐山三友氯碱有限责任公司 低水分含量氯化氢合成方法及合成系统
CN110255501A (zh) * 2019-07-11 2019-09-20 金宏气体电子材料（淮安）有限责任公司 一种电子级高纯氯化氢制备方法
CN112578745B (zh) * 2020-09-28 2022-01-14 山东鲁泰化学有限公司 一种氯化氢合成反应过程的智能化控制方法
CN117619272B (zh) * 2023-12-01 2024-09-06 浙江瑞亨电子材料有限公司 一种高纯氯化氢的制备设备以及生产工艺

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US2077310A (en) * 1936-02-01 1937-04-13 Pennsylvania Salt Mfg Co Process of purifying chlorine
US2444256A (en) * 1946-07-19 1948-06-29 Shell Dev Method for manufacturing hydrogen chloride
US2664342A (en) * 1950-11-20 1953-12-29 Shell Dev Hydrogen halide production
US3077082A (en) * 1958-09-04 1963-02-12 Hooker Chemical Corp Liquefaction of hydrogen chloride
NL129282C (es) * 1963-10-21
US4247532A (en) * 1979-08-13 1981-01-27 Shell Oil Company Purification of electrolytically-produced chlorine
DE3816783A1 (de) * 1988-05-17 1989-11-30 Wacker Chemie Gmbh Verfahren zur reinigung von rohem, gasfoermigem chlorwasserstoff
JP3570732B2 (ja) * 1991-05-28 2004-09-29 三井化学株式会社 塩素ガスの濃縮方法および装置
US5296017A (en) * 1991-05-28 1994-03-22 Mitsui Toatsu Chemicals, Inc. Method and apparatus for concentrating chlorine gas
JP2775364B2 (ja) * 1991-10-17 1998-07-16 鶴見曹達株式会社 塩酸の合成装置
JP2923454B2 (ja) * 1995-10-03 1999-07-26 大同ほくさん株式会社 水素精製方法およびこれに用いる装置
DE19536976A1 (de) * 1995-10-04 1997-04-10 Basf Ag Verfahren zur selektiven Abtrennung und Wiedergewinnung von Chlor aus Gasgemischen
US6340382B1 (en) * 1999-08-13 2002-01-22 Mohamed Safdar Allie Baksh Pressure swing adsorption process for the production of hydrogen
US6896865B2 (en) * 2000-04-28 2005-05-24 Tosoh Corporation Method for recovering hydrogen chloride from chlorine based waste and use of recovered hydrogen chloride
US20040038803A1 (en) * 2002-02-19 2004-02-26 Derong Zhou Adsorbent for removing water vapor during corrosive gas purification and method for preparing the adsorbent
JP2003292304A (ja) * 2002-03-29 2003-10-15 Sumitomo Chem Co Ltd 純塩素ガスの製造方法
RU2217371C1 (ru) * 2002-04-24 2003-11-27 Открытое акционерное общество "Химпром" Способ получения хлористого водорода
JP4507510B2 (ja) * 2003-05-21 2010-07-21 三菱化学株式会社 高純度の塩化水素、及びその製造方法
JP5219372B2 (ja) * 2004-09-29 2013-06-26 昭和電工株式会社 高純度液化塩素の製造方法
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Also Published As

Publication number Publication date
CN107021456A (zh) 2017-08-08
EP2617678B1 (en) 2019-07-31
RU2592794C2 (ru) 2016-07-27
EP2617678A1 (en) 2013-07-24
US20210331919A1 (en) 2021-10-28
JP5756180B2 (ja) 2015-07-29
IL228118A0 (en) 2013-09-30
MX2013009832A (es) 2013-10-03
JP2013545704A (ja) 2013-12-26
TW201315682A (zh) 2013-04-16
CA2828446C (en) 2019-05-07
SG192925A1 (en) 2013-09-30
RU2013146601A (ru) 2015-11-20
AU2012321629A1 (en) 2013-09-05
MY156181A (en) 2016-01-15
US20130259796A1 (en) 2013-10-03
CN103221336A (zh) 2013-07-24
EP2617678A4 (en) 2014-03-05
IL228118A (en) 2015-11-30
TWI520906B (zh) 2016-02-11
CA2828446A1 (en) 2013-04-18
AU2012321629B2 (en) 2014-10-16
WO2013054989A1 (ko) 2013-04-18

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