MX2016001029A - Un proceso para preparar óxido de propileno. - Google Patents
Un proceso para preparar óxido de propileno.Info
- Publication number
- MX2016001029A MX2016001029A MX2016001029A MX2016001029A MX2016001029A MX 2016001029 A MX2016001029 A MX 2016001029A MX 2016001029 A MX2016001029 A MX 2016001029A MX 2016001029 A MX2016001029 A MX 2016001029A MX 2016001029 A MX2016001029 A MX 2016001029A
- Authority
- MX
- Mexico
- Prior art keywords
- propylene oxide
- potassium salt
- optionally
- acetonitrile
- water
- Prior art date
Links
- GOOHAUXETOMSMM-UHFFFAOYSA-N Propylene oxide Chemical compound CC1CO1 GOOHAUXETOMSMM-UHFFFAOYSA-N 0.000 title abstract 4
- 238000004519 manufacturing process Methods 0.000 title 1
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 abstract 9
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 abstract 6
- QQONPFPTGQHPMA-UHFFFAOYSA-N Propene Chemical compound CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 abstract 6
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 abstract 5
- 229910052698 phosphorus Inorganic materials 0.000 abstract 5
- 239000011574 phosphorus Substances 0.000 abstract 5
- 238000006735 epoxidation reaction Methods 0.000 abstract 4
- XAEFZNCEHLXOMS-UHFFFAOYSA-M potassium benzoate Chemical compound [K+].[O-]C(=O)C1=CC=CC=C1 XAEFZNCEHLXOMS-UHFFFAOYSA-M 0.000 abstract 4
- 239000007788 liquid Substances 0.000 abstract 3
- 239000001294 propane Substances 0.000 abstract 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 3
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 abstract 2
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 abstract 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 abstract 1
- 229910021536 Zeolite Inorganic materials 0.000 abstract 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 238000010924 continuous production Methods 0.000 abstract 1
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 abstract 1
- 239000011591 potassium Substances 0.000 abstract 1
- 229910052700 potassium Inorganic materials 0.000 abstract 1
- 239000011541 reaction mixture Substances 0.000 abstract 1
- 229910052719 titanium Inorganic materials 0.000 abstract 1
- 239000010936 titanium Substances 0.000 abstract 1
- 239000010457 zeolite Substances 0.000 abstract 1
- 239000011701 zinc Substances 0.000 abstract 1
- 229910052725 zinc Inorganic materials 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D301/00—Preparation of oxiranes
- C07D301/02—Synthesis of the oxirane ring
- C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
- C07D301/12—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with hydrogen peroxide or inorganic peroxides or peracids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
- B01J27/14—Phosphorus; Compounds thereof
- B01J27/16—Phosphorus; Compounds thereof containing oxygen, i.e. acids, anhydrides and their derivates with N, S, B or halogens without carriers or on carriers based on C, Si, Al or Zr; also salts of Si, Al and Zr
- B01J27/18—Phosphorus; Compounds thereof containing oxygen, i.e. acids, anhydrides and their derivates with N, S, B or halogens without carriers or on carriers based on C, Si, Al or Zr; also salts of Si, Al and Zr with metals other than Al or Zr
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
- B01J27/14—Phosphorus; Compounds thereof
- B01J27/186—Phosphorus; Compounds thereof with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
- B01J27/188—Phosphorus; Compounds thereof with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium with chromium, molybdenum, tungsten or polonium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J29/00—Catalysts comprising molecular sieves
- B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
- B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
- B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
- B01J29/7038—MWW-type, e.g. MCM-22, ERB-1, ITQ-1, PSH-3 or SSZ-25
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J29/00—Catalysts comprising molecular sieves
- B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
- B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
- B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
- B01J29/7049—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65 containing rare earth elements, titanium, zirconium, hafnium, zinc, cadmium, mercury, gallium, indium, thallium, tin or lead
- B01J29/7088—MWW-type, e.g. MCM-22, ERB-1, ITQ-1, PSH-3 or SSZ-25
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J29/00—Catalysts comprising molecular sieves
- B01J29/89—Silicates, aluminosilicates or borosilicates of titanium, zirconium or hafnium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J35/00—Catalysts, in general, characterised by their form or physical properties
- B01J35/19—Catalysts containing parts with different compositions
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J35/00—Catalysts, in general, characterised by their form or physical properties
- B01J35/30—Catalysts, in general, characterised by their form or physical properties characterised by their physical properties
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J35/00—Catalysts, in general, characterised by their form or physical properties
- B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
- B01J35/61—Surface area
- B01J35/615—100-500 m2/g
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/02—Impregnation, coating or precipitation
- B01J37/0201—Impregnation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/08—Heat treatment
- B01J37/10—Heat treatment in the presence of water, e.g. steam
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D301/00—Preparation of oxiranes
- C07D301/32—Separation; Purification
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D301/00—Preparation of oxiranes
- C07D301/36—Use of additives, e.g. for stabilisation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
- C07D303/02—Compounds containing oxirane rings
- C07D303/04—Compounds containing oxirane rings containing only hydrogen and carbon atoms in addition to the ring oxygen atoms
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
- B01J2229/10—After treatment, characterised by the effect to be obtained
- B01J2229/18—After treatment, characterised by the effect to be obtained to introduce other elements into or onto the molecular sieve itself
- B01J2229/186—After treatment, characterised by the effect to be obtained to introduce other elements into or onto the molecular sieve itself not in framework positions
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Crystallography & Structural Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Epoxy Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Catalysts (AREA)
Abstract
Un proceso continuo para la preparación de óxido de propileno, que comprende (i) proporcionar una corriente de suministro líquido que comprende propeno, peróxido de hidrógeno, acetonitrilo, agua, opcionalmente propano, y al menos una sal de potasio disuelta de un oxiácido fosfórico disuelta en la que la relación molar de potasio respecto al fósforo en la al menos una sal de potasio de un oxiácido fosfórico está dentro del intervalo de 0,6 a 1,4; (ii) pasar la corriente de suministro líquida provista en (i) a un reactor de epoxidación que comprende un catalizador que comprende una zeolita de titanio de estructura tipo MWW que incluye zinc, y someter la corriente de suministro líquida a condiciones de reacción de epoxidación en el reactor de epoxidación, para obtener una mezcla de reacción que comprende óxido de propileno, acetonitrilo, agua, al menos una sal de potasio de un oxiácido fosfórico, disuelta opcionalmente propeno, y opcionalmente propano; (iii) remover una corriente de efluentes desde el reactor de epoxidación, comprendiendo la corriente de efluentes óxido de propileno, acetonitrilo, agua, al menos una porción de la al menos una sal de potasio de un disuelta de un oxiácido fosfórico disuelta, opcionalmente propeno, y opcionalmente propano.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP13177906 | 2013-07-24 | ||
PCT/EP2014/065244 WO2015010991A1 (en) | 2013-07-24 | 2014-07-16 | A process for preparing propylene oxide |
Publications (1)
Publication Number | Publication Date |
---|---|
MX2016001029A true MX2016001029A (es) | 2016-09-08 |
Family
ID=48832826
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
MX2016001029A MX2016001029A (es) | 2013-07-24 | 2014-07-16 | Un proceso para preparar óxido de propileno. |
Country Status (13)
Country | Link |
---|---|
US (1) | US9725428B2 (es) |
EP (1) | EP3024579B1 (es) |
KR (1) | KR102266683B1 (es) |
CN (1) | CN105764609B (es) |
BR (1) | BR112016001529B1 (es) |
ES (1) | ES2730990T3 (es) |
HU (1) | HUE045051T2 (es) |
MX (1) | MX2016001029A (es) |
PL (1) | PL3024579T3 (es) |
RU (1) | RU2678844C2 (es) |
SG (2) | SG10201804981TA (es) |
WO (1) | WO2015010991A1 (es) |
ZA (1) | ZA201601117B (es) |
Families Citing this family (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2015010990A1 (en) * | 2013-07-24 | 2015-01-29 | Basf Se | A process for preparing propylene oxide |
EP3206756B1 (de) | 2014-10-14 | 2018-09-19 | Basf Se | Verwendung von hexadeca-8,15-dienal als aromachemikalie |
WO2016128917A1 (en) | 2015-02-12 | 2016-08-18 | Basf Se | Process for the preparation of a dealuminated zeolitic material having the bea framework structure |
EP3292099B1 (en) | 2015-05-04 | 2020-07-22 | Basf Se | Process for the preparation of melonal |
WO2017009462A1 (en) | 2015-07-15 | 2017-01-19 | Basf Se | Process for preparing an arylpropene |
WO2017009458A1 (en) | 2015-07-15 | 2017-01-19 | Basf Se | Process for preparing an arylpropene |
CN108137523B (zh) | 2015-07-22 | 2022-07-26 | 巴斯夫欧洲公司 | 制备呋喃-2,5-二甲酸的方法 |
WO2018011280A1 (en) * | 2016-07-13 | 2018-01-18 | Basf Se | A process for preparing ethene oxide |
RU2766954C2 (ru) * | 2017-04-24 | 2022-03-16 | Басф Се | Извлечение пропена посредством очистки в скруббере со смесью растворитель/вода |
CN108191794B (zh) * | 2017-12-29 | 2020-02-11 | 中触媒新材料股份有限公司 | 一种丙烯环氧化反应方法 |
CN112209356B (zh) * | 2020-09-28 | 2021-12-14 | 浙江工业大学 | 一种类p2o5结构材料及其制备方法和应用 |
ES2938316T3 (es) | 2020-10-21 | 2023-04-10 | Evonik Operations Gmbh | Un método para aumentar la producción de óxido de propileno de un procedimiento integrado para fabricar óxido de propileno y propilenglicol |
Family Cites Families (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE3936854A1 (de) | 1989-11-06 | 1991-05-08 | Basf Ag | Verfahren zur herstellung von methylformiat |
US6114551A (en) | 1999-10-04 | 2000-09-05 | Mobil Oil Corporation | Olefin epoxidation catalysts |
EP1122249A1 (fr) | 2000-02-02 | 2001-08-08 | SOLVAY (Société Anonyme) | Procédé de fabrication d'un oxiranne |
DE10044787A1 (de) | 2000-09-11 | 2002-04-04 | Basf Ag | Verfahren zur Herstellung eines Epoxides |
DE10320635A1 (de) * | 2003-05-08 | 2004-11-18 | Basf Ag | Verfahren zur Herstellung von Propylenoxid |
US7273826B2 (en) * | 2005-07-26 | 2007-09-25 | Lyondell Chemical Technology, L.P. | Epoxidation catalyst |
EP2173731B1 (en) * | 2007-07-10 | 2011-10-26 | Sumitomo Chemical Company, Limited | Method for producing propylene oxide |
MX2012000556A (es) | 2009-07-16 | 2012-04-11 | Basf Se | Metodo para la separacion de acetonitrilo a partir de agua. |
US8124798B2 (en) * | 2009-12-17 | 2012-02-28 | Lyondell Chemical Technology, Lp | Direct epoxidation catalyst and process |
US8124555B2 (en) * | 2010-02-01 | 2012-02-28 | Lyondell Chemical Technology L.P. | Process for making titanium-MWW zeolite |
JP2012116758A (ja) * | 2010-11-29 | 2012-06-21 | Sumitomo Chemical Co Ltd | オレフィンオキサイドの製造方法 |
US8785670B2 (en) * | 2010-12-07 | 2014-07-22 | Basf Se | Process for the production of propylene oxide |
JP2012236177A (ja) * | 2011-05-13 | 2012-12-06 | Sumitomo Chemical Co Ltd | チタノシリケート含有触媒の製造方法 |
-
2014
- 2014-07-16 PL PL14739188T patent/PL3024579T3/pl unknown
- 2014-07-16 SG SG10201804981TA patent/SG10201804981TA/en unknown
- 2014-07-16 HU HUE14739188A patent/HUE045051T2/hu unknown
- 2014-07-16 ES ES14739188T patent/ES2730990T3/es active Active
- 2014-07-16 EP EP14739188.2A patent/EP3024579B1/en active Active
- 2014-07-16 SG SG11201600530YA patent/SG11201600530YA/en unknown
- 2014-07-16 US US14/907,998 patent/US9725428B2/en active Active
- 2014-07-16 WO PCT/EP2014/065244 patent/WO2015010991A1/en active Application Filing
- 2014-07-16 CN CN201480052389.2A patent/CN105764609B/zh active Active
- 2014-07-16 MX MX2016001029A patent/MX2016001029A/es active IP Right Grant
- 2014-07-16 BR BR112016001529-0A patent/BR112016001529B1/pt active IP Right Grant
- 2014-07-16 RU RU2016105805A patent/RU2678844C2/ru active
- 2014-07-16 KR KR1020167004190A patent/KR102266683B1/ko active IP Right Grant
-
2016
- 2016-02-18 ZA ZA2016/01117A patent/ZA201601117B/en unknown
Also Published As
Publication number | Publication date |
---|---|
US9725428B2 (en) | 2017-08-08 |
ES2730990T3 (es) | 2019-11-13 |
SG10201804981TA (en) | 2018-07-30 |
EP3024579A1 (en) | 2016-06-01 |
RU2016105805A3 (es) | 2018-04-28 |
EP3024579B1 (en) | 2019-03-13 |
WO2015010991A1 (en) | 2015-01-29 |
KR102266683B1 (ko) | 2021-06-21 |
SG11201600530YA (en) | 2016-02-26 |
RU2678844C2 (ru) | 2019-02-04 |
BR112016001529B1 (pt) | 2020-10-06 |
CN105764609B (zh) | 2018-02-23 |
CN105764609A (zh) | 2016-07-13 |
KR20160051746A (ko) | 2016-05-11 |
HUE045051T2 (hu) | 2019-12-30 |
ZA201601117B (en) | 2019-07-31 |
RU2016105805A (ru) | 2017-08-29 |
PL3024579T3 (pl) | 2019-09-30 |
BR112016001529A2 (pt) | 2019-12-17 |
US20160176834A1 (en) | 2016-06-23 |
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