MX2017015606A - Proceso para preparar 3-metilciclopentadecan-1,5-diona. - Google Patents

Proceso para preparar 3-metilciclopentadecan-1,5-diona.

Info

Publication number
MX2017015606A
MX2017015606A MX2017015606A MX2017015606A MX2017015606A MX 2017015606 A MX2017015606 A MX 2017015606A MX 2017015606 A MX2017015606 A MX 2017015606A MX 2017015606 A MX2017015606 A MX 2017015606A MX 2017015606 A MX2017015606 A MX 2017015606A
Authority
MX
Mexico
Prior art keywords
methylcyclopentadecane
dione
formula
preparing
oxidation
Prior art date
Application number
MX2017015606A
Other languages
English (en)
Inventor
Bru Roig Miriam
Ruedenauer Stefan
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Publication of MX2017015606A publication Critical patent/MX2017015606A/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/28—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation of CHx-moieties
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
    • C01B15/01—Hydrogen peroxide
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
    • C07C49/385—Saturated compounds containing a keto group being part of a ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/18—Systems containing only non-condensed rings with a ring being at least seven-membered

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

La presente invención se refiere a un proceso para producir 3-metilciclopentadecan-1,5-diona de la Fórmula (I), que comprende la oxidación de 14-metilbiciclo[10.3.0]pentadecen[1(12)] de la Fórmula (II) con un agente oxidante, en donde la oxidación se lleva a cabo usando una mezcla de ácido fórmico con H2O2 como único agente oxidante en presencia de agua y en donde la cantidad de H2O2 es al menos 1,1 mol de H2O2 por mol del compuesto de la Fórmula (II). (ver Fórmulas).
MX2017015606A 2015-06-03 2016-06-02 Proceso para preparar 3-metilciclopentadecan-1,5-diona. MX2017015606A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP15170490 2015-06-03
PCT/EP2016/062434 WO2016193330A1 (en) 2015-06-03 2016-06-02 Process for preparing 3-methylcyclopentadecane-1,5-dione

Publications (1)

Publication Number Publication Date
MX2017015606A true MX2017015606A (es) 2018-04-24

Family

ID=53385503

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2017015606A MX2017015606A (es) 2015-06-03 2016-06-02 Proceso para preparar 3-metilciclopentadecan-1,5-diona.

Country Status (7)

Country Link
US (1) US10053409B2 (es)
EP (1) EP3303278B1 (es)
JP (1) JP6789989B6 (es)
CN (1) CN107709283B (es)
ES (1) ES2806203T3 (es)
MX (1) MX2017015606A (es)
WO (1) WO2016193330A1 (es)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3170828A1 (de) * 2015-11-23 2017-05-24 Basf Se Verfahren zur herstellung von verbindungen mit 16-oxabicyclo[10.3.1]pentadecengerüst und deren folgeprodukten
WO2017140909A1 (de) 2016-02-19 2017-08-24 Basf Se Enzymatische zyklisierung von homofarnesylsäure
CN109195959B (zh) 2016-05-31 2023-08-18 巴斯夫欧洲公司 四氢吡喃基低碳烷基酯和其使用烯酮化合物的制备
BR112018077067B1 (pt) 2016-07-15 2022-05-31 Basf Se Processo para preparar um composto
JP2023151194A (ja) * 2022-03-31 2023-10-16 花王株式会社 環状ジケトン化合物の製造方法
JP2023151195A (ja) * 2022-03-31 2023-10-16 花王株式会社 環状ジケトン化合物の製造方法

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CH519454A (de) 1966-02-08 1972-02-29 Firmenich & Cie Verfahren zur Herstellung von makrocyclischen Verbindungen
CH513791A (de) * 1966-12-08 1971-10-15 Firmenich & Cie Verfahren zur Herstellung von makrocyclischen Verbindungen
CH482637A (de) * 1966-11-01 1969-12-15 Eschenmoser Albert Dr Prof Verfahren zur Herstellung von Acetylenverbindungen
CH503680A (de) 1966-12-08 1971-02-28 Firmenich & Cie Verfahren zur Herstellung von makrocyclischen Ketonen
GB1232010A (es) 1967-09-04 1971-05-19
DE2916418A1 (de) 1979-04-23 1980-11-06 Basf Ag Verfahren zur herstellung von 14- methyl-bicyclo- eckige klammer auf 10.3.0. eckige klammer zu -pentadecen- eckige klammer auf 1(12) eckige klammer zu und neue zwischenprodukte dieses verfahrens
CN100494148C (zh) * 2006-09-15 2009-06-03 济南宏济堂制药有限责任公司 4-甲基环十五烷酮及应用
EP2625158B1 (de) * 2010-10-07 2014-08-13 Basf Se Verfahren zur herstellung von ketonen, insbesondere makrocyclischer ketone
CN102786398A (zh) * 2012-08-30 2012-11-21 新乡医学院 一种经济环保的高纯度麝香酮规模化生产工艺
US10087129B2 (en) * 2014-12-26 2018-10-02 Kao Corporation Method for producing cyclic diketone compound
JP6853189B2 (ja) 2015-05-20 2021-03-31 ビーエイエスエフ・ソシエタス・エウロパエアＢａｓｆ Ｓｅ 大環状ジケトンを調製する方法

Also Published As

Publication number Publication date
EP3303278B1 (en) 2020-04-22
EP3303278A1 (en) 2018-04-11
CN107709283B (zh) 2021-02-02
JP6789989B2 (ja) 2020-11-25
JP2018516271A (ja) 2018-06-21
WO2016193330A1 (en) 2016-12-08
US10053409B2 (en) 2018-08-21
US20180179136A1 (en) 2018-06-28
CN107709283A (zh) 2018-02-16
ES2806203T3 (es) 2021-02-16
JP6789989B6 (ja) 2020-12-16

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