ES2723477T3 - Procedimiento para producir compuesto de dicetona cíclica - Google Patents

Procedimiento para producir compuesto de dicetona cíclica Download PDF

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Publication number
ES2723477T3
ES2723477T3 ES15873042T ES15873042T ES2723477T3 ES 2723477 T3 ES2723477 T3 ES 2723477T3 ES 15873042 T ES15873042 T ES 15873042T ES 15873042 T ES15873042 T ES 15873042T ES 2723477 T3 ES2723477 T3 ES 2723477T3
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bond
denotes
formula
binds
compound represented
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ES15873042T
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Kenji Tanino
Daichi SAKODA
Shu Sakamoto
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Kao Corp
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Kao Corp
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
    • C07C45/64—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by introduction of functional groups containing oxygen only in singly bound form
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/28—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation of CHx-moieties
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • B01J31/0234—Nitrogen-, phosphorus-, arsenic- or antimony-containing compounds
    • B01J31/0235—Nitrogen containing compounds
    • B01J31/0239—Quaternary ammonium compounds
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
    • C01B15/01—Hydrogen peroxide
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G41/00—Compounds of tungsten
    • C01G41/02—Oxides; Hydroxides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B61/00—Other general methods
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/56—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds from heterocyclic compounds
    • C07C45/57—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds from heterocyclic compounds with oxygen as the only heteroatom
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
    • C07C45/65—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by splitting-off hydrogen atoms or functional groups; by hydrogenolysis of functional groups
    • C07C45/66—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by splitting-off hydrogen atoms or functional groups; by hydrogenolysis of functional groups by dehydration
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
    • C07C49/385—Saturated compounds containing a keto group being part of a ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
    • C07C49/587—Unsaturated compounds containing a keto groups being part of a ring

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

Un procedimiento para producir un compuesto representado por la fórmula general (I), comprendiendo el procedimiento una etapa de someter un compuesto representado por la fórmula general (II) a escisión oxidativa usando peróxido de hidrógeno en presencia de un catalizador de ácido, que es un ácido de Bronsted que tiene un pKa en agua de no más de 2,0, o en presencia de un compuesto de ácido túngstico para obtener el compuesto representado por la fórmula general (I): **(Ver fórmula)** en el que la fórmula -A1- (en donde el enlace frontal denota un enlace que se une con un átomo de carbono C1 mientras que el enlace posterior denota un enlace que se une con un átomo de carbono C2) es un grupo alquileno que tiene de 2 a 6 átomos de carbono que puede haberse sustituido y que puede incluir además un enlace éter, un enlace éster, un grupo amino secundario, un grupo tioéter, o estos, y la fórmula -A2- (en donde el enlace frontal denota un enlace que se une con un átomo de carbono C1 mientras que el enlace posterior denota un enlace que se une con un átomo de carbono C2) es un grupo alquileno que tiene de 4 a 10 átomos de carbono que puede haberse sustituido y que puede incluir además un enlace éter, un enlace éster, un grupo amino secundario, un grupo tioéter, o estos
ES15873042T 2014-12-26 2015-12-22 Procedimiento para producir compuesto de dicetona cíclica Active ES2723477T3 (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2014266684 2014-12-26
PCT/JP2015/085772 WO2016104474A1 (ja) 2014-12-26 2015-12-22 環状ジケトン化合物の製造方法

Publications (1)

Publication Number Publication Date
ES2723477T3 true ES2723477T3 (es) 2019-08-28

Family

ID=56150492

Family Applications (1)

Application Number Title Priority Date Filing Date
ES15873042T Active ES2723477T3 (es) 2014-12-26 2015-12-22 Procedimiento para producir compuesto de dicetona cíclica

Country Status (6)

Country Link
US (1) US10087129B2 (es)
EP (1) EP3199514B1 (es)
JP (1) JP6691769B2 (es)
CN (1) CN107001214B (es)
ES (1) ES2723477T3 (es)
WO (1) WO2016104474A1 (es)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP6789989B6 (ja) * 2015-06-03 2020-12-16 ビーエイエスエフ・ソシエタス・エウロパエアＢａｓｆ Ｓｅ ３−メチルシクロペンタデカン−１，５−ジオンを製造するための方法
BR112018005524B1 (pt) * 2015-09-22 2021-05-25 Basf Se processo para preparar um diol e processo para preparar um odorizante macrocíclico
EP3170828A1 (de) * 2015-11-23 2017-05-24 Basf Se Verfahren zur herstellung von verbindungen mit 16-oxabicyclo[10.3.1]pentadecengerüst und deren folgeprodukten
MX2019000664A (es) * 2016-07-15 2019-05-20 Basf Se Preparacion de 14-metil-16-oxabiciclo[10.3.1]pentadecenos de 3-metil-1,5 ciclopentadecanediona.
CN108033879B (zh) * 2017-10-26 2021-02-02 万华化学集团股份有限公司 一种制备手性麝香酮的方法
CN111051314B (zh) * 2017-11-01 2023-10-27 弗门尼舍有限公司 制备双环烯醇醚的方法
EP3862356B1 (en) * 2018-09-28 2024-04-03 Kao Corporation Method for producing cyclic enol ether compound
US11753417B2 (en) * 2019-01-17 2023-09-12 International Flavors & Fragrances Inc. Synthesis of 14-methyl-16-oxabicyclo[10.3.1]hexadec-12-ene
US11685705B2 (en) 2019-03-18 2023-06-27 Kao Corporation Method for producing α-allylated cycloalkanone
EP3870587A1 (en) * 2019-04-15 2021-09-01 Firmenich SA Process for preparing bicyclic enolether
GB202011259D0 (en) * 2020-07-21 2020-09-02 Givaudan Sa Method for the production of musk fragrance ingredient
JP2023151194A (ja) * 2022-03-31 2023-10-16 花王株式会社 環状ジケトン化合物の製造方法
JP2023151195A (ja) * 2022-03-31 2023-10-16 花王株式会社 環状ジケトン化合物の製造方法

Family Cites Families (17)

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CH476775A (de) 1966-02-08 1969-08-15 Geigy Ag J R Verfahren zum Schützen von oxydationsempfindlichem organischem Material
CH513791A (de) 1966-12-08 1971-10-15 Firmenich & Cie Verfahren zur Herstellung von makrocyclischen Verbindungen
CH503680A (de) 1966-12-08 1971-02-28 Firmenich & Cie Verfahren zur Herstellung von makrocyclischen Ketonen
JP2000159693A (ja) * 1998-12-01 2000-06-13 Noguchi Inst 有機不飽和化合物の酸化方法
IL144815A (en) 2000-08-11 2005-07-25 Sumitomo Chemical Co Process for producing carbonyl or hydroxy compound
JP2002201147A (ja) 2000-11-06 2002-07-16 Sumitomo Chem Co Ltd 有機化合物の酸化方法
JP4000825B2 (ja) 2000-11-06 2007-10-31 住友化学株式会社 β−ヒドロキシヒドロペルオキシド類およびケトン類の製造法とその触媒
JP4066679B2 (ja) 2002-03-12 2008-03-26 住友化学株式会社 アラルキルケトン類の製造方法とその触媒
CN1313428C (zh) 2002-07-25 2007-05-02 独立行政法人产业技术综合研究所 制备羧酸的方法
JP3772209B2 (ja) 2002-07-25 2006-05-10 独立行政法人産業技術総合研究所 カルボン酸の製造法
JP3772210B2 (ja) 2002-07-25 2006-05-10 独立行政法人産業技術総合研究所 カルボン酸の製造方法
BRPI0609296A2 (pt) 2005-05-02 2010-03-23 Novartis Ag uso de derivados de pirimidilaminobenzamida para o tratamento de mastocitose sistÊmica
JP4036242B2 (ja) 2007-02-15 2008-01-23 宇部興産株式会社 二塩基酸の製造方法。
JP5124498B2 (ja) * 2009-01-30 2013-01-23 株式会社日立ハイテクノロジーズ 自動分析装置
JP5448036B2 (ja) 2009-02-18 2014-03-19 トヨタ自動車株式会社 カルボン酸の製造方法
CN102241589B (zh) * 2011-04-19 2013-07-10 湖南科瑞生物科技有限公司 A-失碳-3，5-开裂-雄甾-5-酮-3，17β-二酸的合成方法
CN102786398A (zh) 2012-08-30 2012-11-21 新乡医学院 一种经济环保的高纯度麝香酮规模化生产工艺

Also Published As

Publication number Publication date
US10087129B2 (en) 2018-10-02
EP3199514B1 (en) 2019-02-27
JP6691769B2 (ja) 2020-05-13
EP3199514A1 (en) 2017-08-02
WO2016104474A1 (ja) 2016-06-30
EP3199514A4 (en) 2018-03-07
CN107001214A (zh) 2017-08-01
JP2016124867A (ja) 2016-07-11
CN107001214B (zh) 2021-03-23
US20170362153A1 (en) 2017-12-21

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