MX2015010048A - Proceso para preparar material zeolitico que contiene boro que tiene la estructura marco mww. - Google Patents

Proceso para preparar material zeolitico que contiene boro que tiene la estructura marco mww.

Info

Publication number
MX2015010048A
MX2015010048A MX2015010048A MX2015010048A MX2015010048A MX 2015010048 A MX2015010048 A MX 2015010048A MX 2015010048 A MX2015010048 A MX 2015010048A MX 2015010048 A MX2015010048 A MX 2015010048A MX 2015010048 A MX2015010048 A MX 2015010048A
Authority
MX
Mexico
Prior art keywords
bmww
preparing
mother liquor
framework structure
zeolitic material
Prior art date
Application number
MX2015010048A
Other languages
English (en)
Inventor
Robert Bayer
Ulrich Müller
Hans-Jürgen Lützel
Georg Uhl
Andrei-Nicolae Parvulescu
Regina Vogelsang
Robert Schlosser
Franky Ruslim
Pawel Czajka
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Publication of MX2015010048A publication Critical patent/MX2015010048A/es

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B37/00—Compounds having molecular sieve properties but not having base-exchange properties
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/06—Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis
    • C01B39/12—Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis the replacing atoms being at least boron atoms
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7038—MWW-type, e.g. MCM-22, ERB-1, ITQ-1, PSH-3 or SSZ-25
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7049—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65 containing rare earth elements, titanium, zirconium, hafnium, zinc, cadmium, mercury, gallium, indium, thallium, tin or lead
    • B01J29/7088—MWW-type, e.g. MCM-22, ERB-1, ITQ-1, PSH-3 or SSZ-25
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/86—Borosilicates; Aluminoborosilicates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/89—Silicates, aluminosilicates or borosilicates of titanium, zirconium or hafnium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/30—Catalysts, in general, characterised by their form or physical properties characterised by their physical properties
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/40—Catalysts, in general, characterised by their form or physical properties characterised by dimensions, e.g. grain size
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B01J37/0027—Powdering
    • B01J37/0045—Drying a slurry, e.g. spray drying
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/009—Preparation by separation, e.g. by filtration, decantation, screening
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/04—Mixing
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/06—Washing
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • B01J37/10—Heat treatment in the presence of water, e.g. steam
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B37/00—Compounds having molecular sieve properties but not having base-exchange properties
    • C01B37/007—Borosilicates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/06—Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis
    • C01B39/08—Preparation of isomorphous zeolites characterised by measures to replace the aluminium or silicon atoms in the lattice framework by atoms of other elements, i.e. by direct or secondary synthesis the aluminium atoms being wholly replaced
    • C01B39/085—Group IVB- metallosilicates
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
    • C01B39/48—Other types characterised by their X-ray diffraction pattern and their defined composition using at least one organic template directing agent
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/12—Surface area
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/90—Other properties not specified above

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Inorganic Chemistry (AREA)
  • Thermal Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Catalysts (AREA)

Abstract

Un proceso para preparar material zeolítico que contiene boro sin aluminio que comprende la estructura marco MWW (BMWW), que comprende (a) sintetizar hidrotérmicamente el BMWW de una mezcla de síntesis que contiene agua, una fuente de silicio, una fuente de boro y un compuesto de plantilla MWW obteniendo el BMWW en su licor madre, donde el licor madre tiene un pH de más de 9; (b) ajustar el pH del licor madre, obtenido en (a) y que contiene el BMWW, hasta un valor en el rango de 6 a 9; (c) separar el BMWW del licor madre con pH ajustado obtenido en (b) por filtración en un dispositivo de filtración.
MX2015010048A 2013-02-05 2014-02-05 Proceso para preparar material zeolitico que contiene boro que tiene la estructura marco mww. MX2015010048A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP13154025 2013-02-05
PCT/EP2014/052203 WO2014122150A1 (en) 2013-02-05 2014-02-05 Process for preparing a boron containing zeolitic material having mww framework structure

Publications (1)

Publication Number Publication Date
MX2015010048A true MX2015010048A (es) 2016-03-04

Family

ID=47664192

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2015010048A MX2015010048A (es) 2013-02-05 2014-02-05 Proceso para preparar material zeolitico que contiene boro que tiene la estructura marco mww.

Country Status (15)

Country Link
US (2) US10046974B2 (es)
EP (1) EP2953897B1 (es)
JP (1) JP6418611B2 (es)
KR (1) KR102231920B1 (es)
CN (1) CN105073639B (es)
BR (1) BR112015017780A2 (es)
ES (1) ES2894074T3 (es)
HU (1) HUE055878T2 (es)
MX (1) MX2015010048A (es)
MY (1) MY182015A (es)
PL (1) PL2953897T3 (es)
RU (1) RU2651150C2 (es)
SG (2) SG10201705893SA (es)
WO (1) WO2014122150A1 (es)
ZA (1) ZA201506432B (es)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2953897B1 (en) * 2013-02-05 2021-07-21 Basf Se Process for preparing a boron containing zeolitic material having mww framework structure
MX2017003132A (es) * 2014-09-09 2017-06-14 Basf Se Un proceso para la preparacion de un material zeolitico de mww que comprende boro y titanio.
US10122153B2 (en) * 2016-08-29 2018-11-06 International Business Machines Corporation Resonant cavity strained group III-V photodetector and LED on silicon substrate and method to fabricate same
ES2907869T3 (es) * 2016-09-06 2022-04-26 Basf Se Síntesis térmica de sólidos de una zeolita que contiene boro con una estructura de entramado MWW.
JP6939171B2 (ja) * 2017-07-19 2021-09-22 東ソー株式会社 触媒及び触媒を用いた窒素酸化物還元の方法
CN112705252B (zh) * 2019-10-24 2023-04-07 中国石油化工股份有限公司 一种液相烷基化催化剂及其制备方法和应用以及苯与乙烯进行液相烷基化反应的方法

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2815346B1 (fr) * 2000-10-13 2004-02-20 Servier Lab Nouveaux composes aminotriazolones, leur procede de preparation et les compositions pharmaceutiques qui les contiennent
US7258611B2 (en) * 2002-02-28 2007-08-21 Igt Gaming device having free game bonus with a changing multiplier
JP4241068B2 (ja) 2002-03-07 2009-03-18 昭和電工株式会社 Ｍｗｗ型ゼオライト物質の製造方法
US7323154B2 (en) 2002-03-07 2008-01-29 Showa Denko K.K. Titanosilicate, process for its production, and its use in producing oxidized compound
JP4270901B2 (ja) 2002-03-07 2009-06-03 昭和電工株式会社 チタノシリケート、その製造方法およびチタノシリケートを用いた酸化化合物の製造方法
DE10232406A1 (de) * 2002-07-17 2004-01-29 Basf Ag Verfahren zur Herstellung eines zeolithhaltigen Feststoffes
HUE061093T2 (hu) * 2004-12-28 2023-05-28 Neste Oyj Eljárás katalitikus anyagok elõállítására
US20060182681A1 (en) 2004-12-28 2006-08-17 Fortum Oyj Catalytic materials and method for the preparation thereof
US7211239B2 (en) 2005-04-22 2007-05-01 Basf Aktiengesellschaft Process for preparing a nanosized zeolitic material
CN103771440B (zh) 2008-05-21 2015-12-30 巴斯夫欧洲公司 直接合成具有CHA结构的含Cu沸石的方法
WO2011158219A1 (en) * 2010-06-18 2011-12-22 Basf Se Alkali-free synthesis of zeolitic materials of lev-type structure
EP2953897B1 (en) * 2013-02-05 2021-07-21 Basf Se Process for preparing a boron containing zeolitic material having mww framework structure

Also Published As

Publication number Publication date
HUE055878T2 (hu) 2021-12-28
ZA201506432B (en) 2022-08-31
SG10201705893SA (en) 2017-08-30
MY182015A (en) 2021-01-18
RU2651150C2 (ru) 2018-04-18
JP2016506903A (ja) 2016-03-07
US20160002058A1 (en) 2016-01-07
BR112015017780A2 (pt) 2017-07-11
ES2894074T3 (es) 2022-02-11
US10442697B2 (en) 2019-10-15
JP6418611B2 (ja) 2018-11-07
CN105073639A (zh) 2015-11-18
EP2953897A1 (en) 2015-12-16
PL2953897T3 (pl) 2022-01-03
WO2014122150A1 (en) 2014-08-14
EP2953897B1 (en) 2021-07-21
CN105073639B (zh) 2018-05-22
KR102231920B1 (ko) 2021-03-25
US10046974B2 (en) 2018-08-14
KR20150116888A (ko) 2015-10-16
RU2015137734A (ru) 2017-03-14
SG11201505945UA (en) 2015-08-28
US20180362352A1 (en) 2018-12-20

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