MX2011011732A - Metodo continuo para producir esteres de acidos carboxilicos alifaticos. - Google Patents

Metodo continuo para producir esteres de acidos carboxilicos alifaticos.

Info

Publication number
MX2011011732A
MX2011011732A MX2011011732A MX2011011732A MX2011011732A MX 2011011732 A MX2011011732 A MX 2011011732A MX 2011011732 A MX2011011732 A MX 2011011732A MX 2011011732 A MX2011011732 A MX 2011011732A MX 2011011732 A MX2011011732 A MX 2011011732A
Authority
MX
Mexico
Prior art keywords
continuous method
aliphatic carboxylic
carboxylic acids
optionally substituted
formula
Prior art date
Application number
MX2011011732A
Other languages
English (en)
Inventor
Roman Morschhaeuser
Matthias Krull
Original Assignee
Clariant Finance Bvi Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Clariant Finance Bvi Ltd filed Critical Clariant Finance Bvi Ltd
Publication of MX2011011732A publication Critical patent/MX2011011732A/es

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00Preparation of carboxylic acid esters
    • C07C67/08Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/08Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J19/12Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor employing electromagnetic waves
    • B01J19/122Incoherent waves
    • B01J19/126Microwaves
    • HELECTRICITY
    • H05ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
    • H05BELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
    • H05B6/00Heating by electric, magnetic or electromagnetic fields
    • H05B6/64Heating using microwaves
    • H05B6/70Feed lines
    • H05B6/701Feed lines using microwave applicators
    • HELECTRICITY
    • H05ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
    • H05BELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
    • H05B6/00Heating by electric, magnetic or electromagnetic fields
    • H05B6/64Heating using microwaves
    • H05B6/80Apparatus for specific applications
    • H05B6/806Apparatus for specific applications for laboratory use
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/08Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J2219/12Processes employing electromagnetic waves
    • B01J2219/1203Incoherent waves
    • B01J2219/1206Microwaves
    • B01J2219/1209Features relating to the reactor or vessel
    • B01J2219/1212Arrangements of the reactor or the reactors
    • B01J2219/1215Single reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/08Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J2219/12Processes employing electromagnetic waves
    • B01J2219/1203Incoherent waves
    • B01J2219/1206Microwaves
    • B01J2219/1209Features relating to the reactor or vessel
    • B01J2219/1221Features relating to the reactor or vessel the reactor per se
    • B01J2219/1224Form of the reactor
    • B01J2219/1227Reactors comprising tubes with open ends
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/08Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J2219/12Processes employing electromagnetic waves
    • B01J2219/1203Incoherent waves
    • B01J2219/1206Microwaves
    • B01J2219/1248Features relating to the microwave cavity
    • B01J2219/1272Materials of construction
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/08Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J2219/12Processes employing electromagnetic waves
    • B01J2219/1203Incoherent waves
    • B01J2219/1206Microwaves
    • B01J2219/1275Controlling the microwave irradiation variables
    • B01J2219/1281Frequency
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/08Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J2219/12Processes employing electromagnetic waves
    • B01J2219/1203Incoherent waves
    • B01J2219/1206Microwaves
    • B01J2219/1275Controlling the microwave irradiation variables
    • B01J2219/1284Intensity
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/08Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
    • B01J2219/12Processes employing electromagnetic waves
    • B01J2219/1203Incoherent waves
    • B01J2219/1206Microwaves
    • B01J2219/1287Features relating to the microwave source
    • B01J2219/129Arrangements thereof

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Electromagnetism (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Clinical Laboratory Science (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

La invención se refiere a un método continuo para producir ésteres de ácido carbónico alifáticos haciendo reaccionar por lo menos un ácido carboxulico alifático de la fórmula (l):R1-COOH (I), en donde R1 representa hidrógeno o un grupo hidrocarburo alifático opcionalmente sustituido con de 1 a 50 átomos de carbono, con por lo menos un alcohol de la fórmula (Il):R2-(OH)n(ll), en donde: R2representa un grupo hidrocarburo opcionalmente sustituido con de 1 a 100 átomos de carbono y n es un número entero de 1 a 10, en la presencia de por lo menos un catalizador de transesterificación en un tubo de reacción, el eje longitudinal del mismo se extiende en la dirección de propagación de las microondas de un aplicador de microondas de monomodo, bajo radiación de microondas para formar el éster.
MX2011011732A 2009-06-30 2010-06-09 Metodo continuo para producir esteres de acidos carboxilicos alifaticos. MX2011011732A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102009031053A DE102009031053A1 (de) 2009-06-30 2009-06-30 Kontinuierliches Verfahren zur Herstellung von Estern aliphatischer Carbonsäuren
PCT/EP2010/003446 WO2011000463A2 (de) 2009-06-30 2010-06-09 Kontinuierliches verfahren zur herstellung von estern aliphatischer carbonsäuren

Publications (1)

Publication Number Publication Date
MX2011011732A true MX2011011732A (es) 2011-11-29

Family

ID=43128288

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2011011732A MX2011011732A (es) 2009-06-30 2010-06-09 Metodo continuo para producir esteres de acidos carboxilicos alifaticos.

Country Status (14)

Country Link
US (1) US20120103790A1 (es)
EP (1) EP2448905B1 (es)
JP (2) JP5961552B2 (es)
KR (1) KR20120046720A (es)
CN (1) CN102741212B (es)
AU (2) AU2010268448A1 (es)
BR (1) BRPI1012744A2 (es)
CA (1) CA2766952A1 (es)
DE (1) DE102009031053A1 (es)
EA (1) EA021516B1 (es)
ES (1) ES2405687T3 (es)
MX (1) MX2011011732A (es)
MY (1) MY152089A (es)
WO (1) WO2011000463A2 (es)

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DE102008017213B4 (de) * 2008-04-04 2012-08-09 Clariant International Limited Kontinuierliches Verfahren zur Herstellung von Amiden aliphatischer Hydroxycarbonsäuren
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CN106278888B (zh) * 2016-08-10 2019-03-19 江南大学 一种乳酸基环保增塑剂的制备方法及其应用
CN109843848B (zh) * 2016-10-12 2023-02-28 巴斯夫欧洲公司 制备羟烷基羧酸酯的方法
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Also Published As

Publication number Publication date
CN102741212B (zh) 2014-12-10
JP5961552B2 (ja) 2016-08-02
EP2448905B1 (de) 2013-04-17
AU2016203660A1 (en) 2016-07-28
CA2766952A1 (en) 2011-01-06
MY152089A (en) 2014-08-15
WO2011000463A2 (de) 2011-01-06
ES2405687T3 (es) 2013-06-03
EA021516B1 (ru) 2015-07-30
JP2012531452A (ja) 2012-12-10
CN102741212A (zh) 2012-10-17
BRPI1012744A2 (pt) 2016-03-22
AU2010268448A1 (en) 2011-11-03
KR20120046720A (ko) 2012-05-10
WO2011000463A3 (de) 2011-03-31
JP2016138123A (ja) 2016-08-04
EP2448905A2 (de) 2012-05-09
EA201200069A1 (ru) 2012-05-30
DE102009031053A1 (de) 2011-01-13
US20120103790A1 (en) 2012-05-03

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