MX2011011599A - Procedimiento para preparar un polvo que comprende uno o mas derivados de acido glicino-n, n-diacetico y/o uno o mas derivados de acido glutamino-n, n-diacetico y polvo de sal de trisodio de acido metilglicino-n, n-diacetico. - Google Patents
Procedimiento para preparar un polvo que comprende uno o mas derivados de acido glicino-n, n-diacetico y/o uno o mas derivados de acido glutamino-n, n-diacetico y polvo de sal de trisodio de acido metilglicino-n, n-diacetico.Info
- Publication number
- MX2011011599A MX2011011599A MX2011011599A MX2011011599A MX2011011599A MX 2011011599 A MX2011011599 A MX 2011011599A MX 2011011599 A MX2011011599 A MX 2011011599A MX 2011011599 A MX2011011599 A MX 2011011599A MX 2011011599 A MX2011011599 A MX 2011011599A
- Authority
- MX
- Mexico
- Prior art keywords
- diacetic acid
- derivatives
- powder
- glutamine
- glycine
- Prior art date
Links
- 239000000843 powder Substances 0.000 title abstract 3
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- HRXKRNGNAMMEHJ-UHFFFAOYSA-K trisodium citrate Chemical compound [Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O HRXKRNGNAMMEHJ-UHFFFAOYSA-K 0.000 title 1
- 239000007864 aqueous solution Substances 0.000 abstract 3
- 239000013078 crystal Substances 0.000 abstract 3
- 239000002002 slurry Substances 0.000 abstract 3
- 238000000034 method Methods 0.000 abstract 2
- MGFYIUFZLHCRTH-UHFFFAOYSA-N nitrilotriacetic acid Chemical class OC(=O)CN(CC(O)=O)CC(O)=O MGFYIUFZLHCRTH-UHFFFAOYSA-N 0.000 abstract 2
- 239000010409 thin film Substances 0.000 abstract 2
- 239000007787 solid Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C227/38—Separation; Purification; Stabilisation; Use of additives
- C07C227/40—Separation; Purification
- C07C227/42—Crystallisation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C229/00—Compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C229/02—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton
- C07C229/04—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated
- C07C229/24—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having more than one carboxyl group bound to the carbon skeleton, e.g. aspartic acid
-
- H—ELECTRICITY
- H02—GENERATION; CONVERSION OR DISTRIBUTION OF ELECTRIC POWER
- H02S—GENERATION OF ELECTRIC POWER BY CONVERSION OF INFRARED RADIATION, VISIBLE LIGHT OR ULTRAVIOLET LIGHT, e.g. USING PHOTOVOLTAIC [PV] MODULES
- H02S10/00—PV power plants; Combinations of PV energy systems with other systems for the generation of electric power
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
- C07B2200/00—Indexing scheme relating to specific properties of organic compounds
- C07B2200/13—Crystalline forms, e.g. polymorphs
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E10/00—Energy generation through renewable energy sources
- Y02E10/50—Photovoltaic [PV] energy
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
La invención se refiere a un procedimiento para preparar un polvo que comprende uno o más derivados de ácido glicino-N,N-diacético y/o uno o más derivados de ácido glutamino-N,N-diacético que tiene un grado de cristalinidad de = 30%, que procede de una solución acuosa que comprende los uno o más derivados de ácido glicino-N,N-diacético y/o los uno o más derivados de ácido glutamino-N,N-diacético, en un intervalo de concentración que varía de 20 a 60% en peso, con base en el peso total de la solución acuosa, en donde la solución acuosa, en un primer paso de procedimiento, es concentrada en un evaporador con elementos internos giratorios que están dispuestos a una distancia de la pared interna del evaporador de < 1% del diámetro del evaporador para dar una pasta acuosa de cristal que tiene una concentración de sólidos en el intervalo de 60 a 85% en peso, con base en el peso total de la pasta acuosa de cristal, y en donde la pasta acuosa de cristal, en un segundo paso de procedimiento, se deja madurar en un contenedor de pasta y después en un secador de contacto de película delgada, y en donde el tiempo de residencia total en el contenedor de pasta y en el secador de contacto de película delgada es =15 minutos.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP09160718 | 2009-05-20 | ||
| US25390809P | 2009-10-22 | 2009-10-22 | |
| PCT/EP2010/056856 WO2010133618A1 (de) | 2009-05-20 | 2010-05-19 | Verfahren zur herstellung eines pulvers enthaltend eines oder mehrere derivate der glycin-n,n-diessigsäure und/oder eines oder mehrere derivate der glutamin-n,n-diessigsäure und methylglycin-n,n-diessigsäure-trinatriumsalzpulver |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| MX2011011599A true MX2011011599A (es) | 2011-11-18 |
Family
ID=43125759
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| MX2011011599A MX2011011599A (es) | 2009-05-20 | 2010-05-19 | Procedimiento para preparar un polvo que comprende uno o mas derivados de acido glicino-n, n-diacetico y/o uno o mas derivados de acido glutamino-n, n-diacetico y polvo de sal de trisodio de acido metilglicino-n, n-diacetico. |
Country Status (12)
| Country | Link |
|---|---|
| US (2) | US8628684B2 (es) |
| EP (1) | EP2432759B9 (es) |
| JP (1) | JP5745507B2 (es) |
| KR (1) | KR20120023116A (es) |
| BR (1) | BRPI1010933A2 (es) |
| CA (1) | CA2762507C (es) |
| DK (1) | DK2432759T3 (es) |
| ES (1) | ES2396957T3 (es) |
| MX (1) | MX2011011599A (es) |
| PL (1) | PL2432759T3 (es) |
| SG (1) | SG175760A1 (es) |
| WO (1) | WO2010133618A1 (es) |
Families Citing this family (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102009038951A1 (de) * | 2009-08-26 | 2011-03-03 | Inprotec Ag | Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität |
| MX2013012811A (es) | 2011-05-03 | 2014-02-10 | Basf Se | Procedimiento para preparar una sal trialcalinometalica cristalina de l-mgda. |
| US9227915B2 (en) * | 2011-05-03 | 2016-01-05 | Basf Se | Process for the preparation of a crystalline L-MGDA trialkali metal salt |
| GB2491619B (en) * | 2011-06-09 | 2014-10-01 | Pq Silicas Bv | Builder granules and process for their preparation |
| US9815773B2 (en) | 2012-12-14 | 2017-11-14 | Akzo Nobel Chemicals International B.V. | Crystalline particles of glutamic acid N,N-diacetic acid |
| US9738594B2 (en) | 2012-12-14 | 2017-08-22 | Akzo Nobel Chemicals International B.V. | Crystalline particles of salts of glutamic acid N,N-diacetic acid |
| CN106458851B (zh) * | 2014-05-13 | 2019-01-11 | 阿克苏诺贝尔化学品国际有限公司 | 将螯合剂结晶的方法 |
| US10975334B2 (en) | 2015-12-11 | 2021-04-13 | Basf Se | Process for manufacturing granules |
| CA3006791A1 (en) * | 2015-12-17 | 2017-06-22 | Basf Se | Process for making a crystalline alkali metal salt of a complexing agent, and crystalline complexing agent |
| BR112019017127A2 (pt) | 2017-02-24 | 2020-04-14 | Basf Se | processo para produção de sal de metal alcalino de diacetato de metilglicina sólido, partículas sólidas de sal de metal alcalino de diacetato de metilglici-na, e, uso de partículas sólidas |
| CN110869345B (zh) * | 2017-07-07 | 2021-04-30 | 诺力昂化学品国际有限公司 | 甲基甘氨酸-n,n-二乙酸钠化合物，其制备方法及其用途 |
| CN110891930B (zh) * | 2017-07-07 | 2021-09-03 | 诺力昂化学品国际有限公司 | 制备氨基酸二乙酸的固体组合物的方法 |
| CN113382980A (zh) | 2018-12-21 | 2021-09-10 | 诺力昂化学品国际有限公司 | 甲基甘氨酸n,n-二乙酸的易碎相组合物 |
| US20230391713A1 (en) | 2020-06-19 | 2023-12-07 | Nouryon Chemicals International B.V. | Process to prepare a co granule of methylglycine n,n diacetic acid salts employing a crumbly phase composition of methylglycine n,n diacetic acid salts |
| CN116323551A (zh) * | 2020-12-17 | 2023-06-23 | 巴斯夫欧洲公司 | 制备氨基羧酸盐络合剂的固体碱金属盐的方法 |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3932316A (en) | 1974-11-13 | 1976-01-13 | The Procter & Gamble Company | Free flowing detergent compositions containing benzoate salts |
| DE3829829A1 (de) * | 1988-09-02 | 1990-03-22 | Basf Ag | Verfahren zur herstellung des trinatriumsalzes von isoserin-n,n-diessigsaeure |
| JP3035837B2 (ja) * | 1991-06-06 | 2000-04-24 | 株式会社林原生物化学研究所 | 粉末糖質とその製造方法並びに用途 |
| DE4319935A1 (de) | 1993-06-16 | 1994-12-22 | Basf Ag | Verwendung von Glycin-N,N-diessigsäure-Derivaten als Komplexbildner für Erdalkali- und Schwermetallionen |
| DE19546533C2 (de) * | 1995-12-13 | 2000-04-27 | Degussa | Verfahren zur Herstellung von N-Acetyl-D,L-alpha-aminocarbonsäuren |
| DE19649681A1 (de) * | 1996-11-29 | 1998-06-04 | Basf Ag | Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität |
| EP2185280A1 (de) | 2007-08-24 | 2010-05-19 | Basf Se | Katalysator sowie verfahren zu seiner herstellung und verwendung |
-
2010
- 2010-05-19 WO PCT/EP2010/056856 patent/WO2010133618A1/de active Application Filing
- 2010-05-19 EP EP10723028.6A patent/EP2432759B9/de active Active
- 2010-05-19 JP JP2012511271A patent/JP5745507B2/ja active Active
- 2010-05-19 PL PL10723028T patent/PL2432759T3/pl unknown
- 2010-05-19 ES ES10723028T patent/ES2396957T3/es active Active
- 2010-05-19 CA CA2762507A patent/CA2762507C/en active Active
- 2010-05-19 US US13/318,513 patent/US8628684B2/en active Active
- 2010-05-19 SG SG2011077179A patent/SG175760A1/en unknown
- 2010-05-19 DK DK10723028.6T patent/DK2432759T3/da active
- 2010-05-19 KR KR1020117030485A patent/KR20120023116A/ko not_active Application Discontinuation
- 2010-05-19 BR BRPI1010933A patent/BRPI1010933A2/pt not_active IP Right Cessation
- 2010-05-19 MX MX2011011599A patent/MX2011011599A/es active IP Right Grant
-
2013
- 2013-11-26 US US14/090,285 patent/US20140155646A1/en not_active Abandoned
Also Published As
| Publication number | Publication date |
|---|---|
| SG175760A1 (en) | 2011-12-29 |
| JP5745507B2 (ja) | 2015-07-08 |
| US20140155646A1 (en) | 2014-06-05 |
| US8628684B2 (en) | 2014-01-14 |
| WO2010133618A1 (de) | 2010-11-25 |
| EP2432759A1 (de) | 2012-03-28 |
| JP2012527426A (ja) | 2012-11-08 |
| PL2432759T3 (pl) | 2013-05-31 |
| EP2432759B9 (de) | 2014-04-16 |
| CA2762507C (en) | 2018-08-21 |
| US20120046491A1 (en) | 2012-02-23 |
| KR20120023116A (ko) | 2012-03-12 |
| BRPI1010933A2 (pt) | 2016-04-05 |
| CA2762507A1 (en) | 2010-11-25 |
| EP2432759B1 (de) | 2012-12-12 |
| ES2396957T3 (es) | 2013-03-01 |
| DK2432759T3 (da) | 2013-03-04 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG | Grant or registration |