MX2009006276A - Proceso para la preparacion de derivados de cianofenoxi-pirimidini loxi-fenil acrilato sustituido. - Google Patents

Proceso para la preparacion de derivados de cianofenoxi-pirimidini loxi-fenil acrilato sustituido.

Info

Publication number
MX2009006276A
MX2009006276A MX2009006276A MX2009006276A MX2009006276A MX 2009006276 A MX2009006276 A MX 2009006276A MX 2009006276 A MX2009006276 A MX 2009006276A MX 2009006276 A MX2009006276 A MX 2009006276A MX 2009006276 A MX2009006276 A MX 2009006276A
Authority
MX
Mexico
Prior art keywords
aromatic substrate
cynophenoxy
pyrimidiny
loxy
substituted
Prior art date
Application number
MX2009006276A
Other languages
English (en)
Inventor
David Leonov
David Ovadia
Raya Sturkovich
Original Assignee
Makhteshim Chem Works Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Makhteshim Chem Works Ltd filed Critical Makhteshim Chem Works Ltd
Publication of MX2009006276A publication Critical patent/MX2009006276A/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D239/00—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings
    • C07D239/02—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings
    • C07D239/24—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings having three or more double bonds between ring members or between ring members and non-ring members
    • C07D239/28—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings having three or more double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, directly attached to ring carbon atoms
    • C07D239/46—Two or more oxygen, sulphur or nitrogen atoms
    • C07D239/52—Two oxygen atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D239/00—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings
    • C07D239/02—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings
    • C07D239/24—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings having three or more double bonds between ring members or between ring members and non-ring members
    • C07D239/28—Heterocyclic compounds containing 1,3-diazine or hydrogenated 1,3-diazine rings not condensed with other rings having three or more double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, directly attached to ring carbon atoms
    • C07D239/46—Two or more oxygen, sulphur or nitrogen atoms
    • C07D239/52—Two oxygen atoms
    • C07D239/54—Two oxygen atoms as doubly bound oxygen atoms or as unsubstituted hydroxy radicals

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Pyridine Compounds (AREA)

Abstract

La presente invención proporciona un proceso para hacer reaccionar un derivado de fenol y un sustrato aromático bajo condiciones de formación de fenolato, que comprende las siguientes etapas: a) hacer reaccionar un derivado de fenol con una base en un solvente orgánico polar para obtener una sal de fenolato, en donde el agua se retira de la mezcla de reacción durante la reacción, b) agregar el sustrato aromático a la mezcla de reacción obtenida en la etapa (a), c) calentar la mezcla de reacción de la etapa (b) a una temperatura en el rango de 80º a 130ºC, preferentemente de 90-100ºC durante 2 a 7 horas para obtener un sustrato aromático de fenoxi sustituido, d) retirar el solvente de la mezcla de la etapa (c) y aislar y purificar adicionalmente el sustrato aromático de fenoxi sustituido. Opcionalmente, el retiro del agua durante la etapa (a) se realiza junto con el retiro parcial del solvente orgánico.
MX2009006276A 2006-12-17 2007-12-16 Proceso para la preparacion de derivados de cianofenoxi-pirimidini loxi-fenil acrilato sustituido. MX2009006276A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
IL180134A IL180134A0 (en) 2006-12-17 2006-12-17 Process for the preparation of substituted cyanophenoxy-pyrimidinyloxy -phenyl acrylate derivatives
PCT/IL2007/001551 WO2008075341A1 (en) 2006-12-17 2007-12-16 Process for the preparation of substituted cynophenoxy-pyrimidinyloxy-phenyl acrylate derivatives

Publications (1)

Publication Number Publication Date
MX2009006276A true MX2009006276A (es) 2009-06-23

Family

ID=39323004

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2009006276A MX2009006276A (es) 2006-12-17 2007-12-16 Proceso para la preparacion de derivados de cianofenoxi-pirimidini loxi-fenil acrilato sustituido.

Country Status (13)

Country Link
US (2) US8471013B2 (es)
EP (2) EP2102174B1 (es)
JP (1) JP2010513265A (es)
CN (2) CN107056714A (es)
BR (1) BRPI0718724B1 (es)
CA (1) CA2671414A1 (es)
CO (1) CO6210699A2 (es)
DK (1) DK2102174T3 (es)
ES (1) ES2624692T3 (es)
IL (1) IL180134A0 (es)
MX (1) MX2009006276A (es)
PL (1) PL2102174T3 (es)
WO (1) WO2008075341A1 (es)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IL181125A0 (en) * 2007-02-01 2007-07-04 Maktheshim Chemical Works Ltd Polymorphs of 3-(e)-2-{2-[6-(2-
CN102690237A (zh) * 2012-06-11 2012-09-26 江西中科合臣实业有限公司 一种合成高纯度嘧菌酯的方法
CN103265496B (zh) 2013-05-16 2015-02-25 北京颖泰嘉和生物科技有限公司 一种嘧菌酯的制备方法
TWI621614B (zh) 2013-05-28 2018-04-21 科麥農股份有限公司 4,6-雙(芳氧基)嘧啶衍生物的製備方法
CN104119282B (zh) * 2014-08-05 2016-06-29 江苏七洲绿色化工股份有限公司 一种嘧菌酯的脱色和提纯方法
CN109384728A (zh) * 2017-08-07 2019-02-26 华东理工大学 嘧菌酯通道型溶剂化物及其制备方法
TWI705961B (zh) * 2018-11-28 2020-10-01 興農股份有限公司 亞托敏的製備方法

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DE3044856A1 (de) 1980-11-28 1982-07-01 Celamerck Gmbh & Co Kg, 6507 Ingelheim Pyridinderivate
CN1005376B (zh) * 1984-12-12 1989-10-11 旭化成工业株式会社 含有5-(2-氯-4-三氟甲基苯氧基)-2-硝基-α-取代的苯乙酮和/或衍生物肟作为有效成分的除草剂以及消灭不需要的杂草的方法
EP0391451A1 (en) 1986-04-17 1990-10-10 Imperial Chemical Industries Plc Fungicides
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IL110159A0 (en) 1993-06-30 1994-10-07 Wellcome Found Diaryl compounds, their preparation and pharmaceutical compositions containing them
IN179039B (es) 1994-02-08 1997-08-09 Rallis India Ltd
ES2162074T3 (es) 1995-06-28 2001-12-16 Syngenta Ltd Procedimiento para la preparacion de 2-(6-sustituido pirid-2-iloximetil)fenilacetato.
DE19605901A1 (de) * 1996-02-17 1997-08-21 Basf Ag Verfahren zur Herstellung von 2-(2-Methylphenyl)-3-methoxyacrylsäure -methylester
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ES2305491T3 (es) 2002-09-19 2008-11-01 Eli Lilly And Company Eteres de diarilo como antagonistas de receptores de opioides.
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GB0619941D0 (en) * 2006-10-09 2006-11-15 Syngenta Ltd Chemical process
IL181125A0 (en) 2007-02-01 2007-07-04 Maktheshim Chemical Works Ltd Polymorphs of 3-(e)-2-{2-[6-(2-

Also Published As

Publication number Publication date
US20130261303A1 (en) 2013-10-03
US8471013B2 (en) 2013-06-25
WO2008075341A1 (en) 2008-06-26
CA2671414A1 (en) 2008-06-26
CN101558047B (zh) 2017-02-08
IL180134A0 (en) 2007-07-04
EP2527331A1 (en) 2012-11-28
CN101558047A (zh) 2009-10-14
EP2102174A1 (en) 2009-09-23
EP2102174B1 (en) 2017-03-08
DK2102174T3 (en) 2017-05-08
JP2010513265A (ja) 2010-04-30
US20090281316A1 (en) 2009-11-12
CN107056714A (zh) 2017-08-18
CO6210699A2 (es) 2010-10-20
BRPI0718724B1 (pt) 2021-01-12
PL2102174T3 (pl) 2017-09-29
ES2624692T3 (es) 2017-07-17
BRPI0718724A2 (pt) 2014-01-28

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