MX2007008981A - Procedimiento para preparar ciclohexanona y ciclohexanol. - Google Patents

Procedimiento para preparar ciclohexanona y ciclohexanol.

Info

Publication number
MX2007008981A
MX2007008981A MX2007008981A MX2007008981A MX2007008981A MX 2007008981 A MX2007008981 A MX 2007008981A MX 2007008981 A MX2007008981 A MX 2007008981A MX 2007008981 A MX2007008981 A MX 2007008981A MX 2007008981 A MX2007008981 A MX 2007008981A
Authority
MX
Mexico
Prior art keywords
mixture
cyclohexanol
phase
organic
degree
Prior art date
Application number
MX2007008981A
Other languages
English (en)
Inventor
Larry Walker Wyatt
Original Assignee
Dsm Ip Assets Bv
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=36092208&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=MX2007008981(A) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Dsm Ip Assets Bv filed Critical Dsm Ip Assets Bv
Publication of MX2007008981A publication Critical patent/MX2007008981A/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
    • C07C49/385—Saturated compounds containing a keto group being part of a ring
    • C07C49/403—Saturated compounds containing a keto group being part of a ring of a six-membered ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/32—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen
    • C07C45/33—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/51—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition
    • C07C45/53—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition of hydroperoxides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

La presente invencion se refiere a un procedimiento para preparar ciclohexanona y ciclohexanol, comprendiendo dicho procedimiento (a) neutralizar acidos y/o dioxido de carbono presentes en una disolucion organica que comprende ademas hidroperoxido de ciclohexilo mezclando la disolucion organica con una primera disolucion acuosa basica a una temperatura de desde 50 hasta 80 degree C para formar una primera mezcla que comprende una primera fase acuosa con un pH de desde 8.5 hasta 13 y una primera fase organica, (b) separar la primera fase acuosa de la primera mezcla dando como resultado una mezcla restante que comprende la primera fase organica, (c) descomponer el hidroperoxido de ciclohexilo presente en dicha mezcla restante mezclando dicha mezcla restante con una segunda disolucion acuosa basica a una temperatura de desde 60 hasta 110 degree C para formar una segunda mezcla que comprende una segunda fase acuosa y una segunda fase organica que comprende ciclohexanona y ciclohexanol, (d) separar la segunda fase acuosa de la segunda fase organica a una temperatura superior a 80 degree C.
MX2007008981A 2005-01-25 2006-01-17 Procedimiento para preparar ciclohexanona y ciclohexanol. MX2007008981A (es)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP05075184 2005-01-25
EP05075185 2005-01-25
PCT/EP2006/001003 WO2006079562A1 (en) 2005-01-25 2006-01-17 Process for preparing cyclohexanone and cyclohexanol

Publications (1)

Publication Number Publication Date
MX2007008981A true MX2007008981A (es) 2007-09-21

Family

ID=36092208

Family Applications (2)

Application Number Title Priority Date Filing Date
MX2007008983A MX2007008983A (es) 2005-01-25 2006-01-17 Procedimiento para preparar ciclohexanona y ciclohexanol.
MX2007008981A MX2007008981A (es) 2005-01-25 2006-01-17 Procedimiento para preparar ciclohexanona y ciclohexanol.

Family Applications Before (1)

Application Number Title Priority Date Filing Date
MX2007008983A MX2007008983A (es) 2005-01-25 2006-01-17 Procedimiento para preparar ciclohexanona y ciclohexanol.

Country Status (15)

Country Link
US (2) US7642384B2 (es)
EP (2) EP1841720B1 (es)
JP (2) JP2008528537A (es)
KR (2) KR101310409B1 (es)
CN (2) CN101107209B (es)
AT (1) ATE426586T1 (es)
BR (2) BRPI0607224A2 (es)
DE (1) DE602006005898D1 (es)
EA (2) EA014018B1 (es)
ES (1) ES2684413T3 (es)
MX (2) MX2007008983A (es)
MY (2) MY144617A (es)
PL (1) PL1841721T3 (es)
TW (2) TWI365868B (es)
WO (2) WO2006079562A1 (es)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
MX2007008983A (es) * 2005-01-25 2007-09-21 Dsm Ip Assets Bv Procedimiento para preparar ciclohexanona y ciclohexanol.
US7491856B2 (en) 2007-06-27 2009-02-17 H R D Corporation Method of making alkylene glycols
US8304584B2 (en) 2007-06-27 2012-11-06 H R D Corporation Method of making alkylene glycols
US7592493B2 (en) * 2007-06-27 2009-09-22 H R D Corporation High shear process for cyclohexanol production
TW200944497A (en) * 2008-04-17 2009-11-01 China Petrochemical Dev Corp System and method for producing naphthenone
RU2458903C1 (ru) * 2010-12-23 2012-08-20 Открытое акционерное общество "Щекиноазот" Способ получения циклогексанона и циклогексанола и установка для его осуществления
CN102627525B (zh) * 2012-03-31 2013-12-25 肖藻生 一种环己烷氧化制备环己醇和环己酮的生产工艺
CN104557497A (zh) * 2013-10-09 2015-04-29 中国石油化工股份有限公司 一种提高环己基过氧化氢分解酮醇比的方法
CN105646141A (zh) * 2014-11-11 2016-06-08 中国科学院大连化学物理研究所 一种碱液循环用无过环己烷氧化液脱酸的方法
EP3388409A4 (en) * 2015-12-07 2019-07-24 UBE Industries, Ltd. METHOD FOR PRODUCING KETONE AND / OR ALCOHOL AND SYSTEM THEREFOR
CN107778133B (zh) * 2016-08-25 2021-05-07 中国石油化工股份有限公司 一种制备环己醇和环己酮的方法
CN107778132B (zh) * 2016-08-25 2021-02-05 中国石油化工股份有限公司 一种基于多层导流筒鼓泡反应器制备环己醇和环己酮的方法
CN107778131B (zh) * 2016-08-25 2021-02-05 中国石油化工股份有限公司 一种基于多层双环流导流筒鼓泡反应器制备环己醇和环己酮的方法
CN109180444B (zh) * 2018-09-05 2021-07-16 上海交通大学 使用二氧化碳加速氢化芳香化合物合成环己酮的方法

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US768292A (en) 1904-04-01 1904-08-23 George Josiph Miller Animal-trap.
NL288272A (es) 1963-01-28
DE2650892C3 (de) * 1976-11-06 1980-05-29 Basf Ag, 6700 Ludwigshafen Verfahren zur Aufarbeitung von Cyclohexanol und Cyclohexanon enthaltenden Reaktionsgemischen
NL7802125A (nl) * 1978-02-25 1979-08-28 Stamicarbon Werkwijze voor het bereiden van cycloalkanolen en cycloalkanonen.
NL8201695A (nl) 1982-04-23 1983-11-16 Stamicarbon Werkwijze voor de bereiding van cyclohexanol en cyclohexanon.
US4874901A (en) 1988-05-06 1989-10-17 Boc, Inc. Process for the production of polyfluorinated ethers
JPH0819019B2 (ja) * 1991-07-16 1996-02-28 三菱化学株式会社 シクロヘキサンの酸化反応混合物の処理法
JPH05250069A (ja) 1992-03-09 1993-09-28 Funai Electric Co Ltd トラックボール付入力装置
JP2500977B2 (ja) * 1992-03-24 1996-05-29 三菱化学株式会社 シクロヘキサノンの製造方法
BE1007904A3 (nl) * 1993-12-23 1995-11-14 Dsm Nv Werkwijze voor de bereiding van een alkanol en/of een alkanon.
BE1009662A3 (nl) * 1995-10-13 1997-06-03 Dsm Nv Werkwijze voor het ontleden van cycloalkylhydroperoxide.
JP2002128714A (ja) * 2000-10-17 2002-05-09 Sumitomo Chem Co Ltd シクロヘキサンの酸化方法
US6700022B2 (en) * 2002-06-05 2004-03-02 E. I. Du Pont De Nemours And Company High yield cyclohexyl hydroperoxide decompostition process
MX2007008983A (es) * 2005-01-25 2007-09-21 Dsm Ip Assets Bv Procedimiento para preparar ciclohexanona y ciclohexanol.

Also Published As

Publication number Publication date
BRPI0607369A2 (pt) 2009-09-01
MX2007008983A (es) 2007-09-21
KR101310409B1 (ko) 2013-09-23
ATE426586T1 (de) 2009-04-15
EA011023B1 (ru) 2008-12-30
US7619122B2 (en) 2009-11-17
JP2008528528A (ja) 2008-07-31
PL1841721T3 (pl) 2018-10-31
ES2684413T3 (es) 2018-10-02
CN101107209A (zh) 2008-01-16
CN101107210B (zh) 2010-06-16
MY144617A (en) 2011-10-14
CN101107209B (zh) 2011-01-12
EP1841720A1 (en) 2007-10-10
EP1841721B1 (en) 2018-07-25
BRPI0607224A2 (pt) 2009-08-25
EA200701581A1 (ru) 2007-12-28
KR20070097587A (ko) 2007-10-04
TWI365867B (en) 2012-06-11
KR20070110299A (ko) 2007-11-16
EP1841721A1 (en) 2007-10-10
EA200701580A1 (ru) 2007-12-28
EP1841720B1 (en) 2009-03-25
TW200637812A (en) 2006-11-01
US20090018367A1 (en) 2009-01-15
US7642384B2 (en) 2010-01-05
EA014018B1 (ru) 2010-08-30
TWI365868B (en) 2012-06-11
US20090054692A1 (en) 2009-02-26
MY145594A (en) 2012-02-29
DE602006005898D1 (de) 2009-05-07
TW200642997A (en) 2006-12-16
JP2008528537A (ja) 2008-07-31
WO2006079562A1 (en) 2006-08-03
CN101107210A (zh) 2008-01-16
WO2006079485A1 (en) 2006-08-03

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