EA200701338A1 - Способ разложения циклогексилгидропероксида - Google Patents

Способ разложения циклогексилгидропероксида

Info

Publication number
EA200701338A1
EA200701338A1 EA200701338A EA200701338A EA200701338A1 EA 200701338 A1 EA200701338 A1 EA 200701338A1 EA 200701338 A EA200701338 A EA 200701338A EA 200701338 A EA200701338 A EA 200701338A EA 200701338 A1 EA200701338 A1 EA 200701338A1
Authority
EA
Eurasian Patent Office
Prior art keywords
cyclohexanone
cyclogexilhydroperoxide
decomposition
cyclohexylhydroperoxide
organic
Prior art date
Application number
EA200701338A
Other languages
English (en)
Other versions
EA011556B1 (ru
Inventor
Имре Тот
Original Assignee
ДСМ АйПи АССЕТС Б.В.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by ДСМ АйПи АССЕТС Б.В. filed Critical ДСМ АйПи АССЕТС Б.В.
Publication of EA200701338A1 publication Critical patent/EA200701338A1/ru
Publication of EA011556B1 publication Critical patent/EA011556B1/ru

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/48—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by oxidation reactions with formation of hydroxy groups
    • C07C29/50—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by oxidation reactions with formation of hydroxy groups with molecular oxygen only
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/51—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition
    • C07C45/53—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition of hydroperoxides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
    • C07C49/385—Saturated compounds containing a keto group being part of a ring
    • C07C49/403—Saturated compounds containing a keto group being part of a ring of a six-membered ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Steroid Compounds (AREA)

Abstract

Настоящее изобретение относится к способу разложения циклогексилгидропероксида с образованием циклогексанона, включающему смешивание исходного органического раствора, содержащего циклогексилгидропероксид, с раствором водного основания в отсутствие катализатора на основе переходных металлов, которое приводит к образованию смеси, включающей (i) водную фазу и (ii) органическую фазу, содержащую циклогексанон и циклогексанол.
EA200701338A 2004-12-22 2005-12-16 Способ разложения циклогексилгидропероксида EA011556B1 (ru)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP04078490 2004-12-22
PCT/EP2005/013822 WO2006066904A1 (en) 2004-12-22 2005-12-16 Process for decomposing cyclohexylhdroperoxide

Publications (2)

Publication Number Publication Date
EA200701338A1 true EA200701338A1 (ru) 2007-12-28
EA011556B1 EA011556B1 (ru) 2009-04-28

Family

ID=34928767

Family Applications (1)

Application Number Title Priority Date Filing Date
EA200701338A EA011556B1 (ru) 2004-12-22 2005-12-16 Способ разложения циклогексилгидропероксида

Country Status (16)

Country Link
US (1) US7956221B2 (ru)
EP (1) EP1828090B1 (ru)
JP (1) JP2008524298A (ru)
KR (1) KR20070094930A (ru)
CN (1) CN101087747B (ru)
AT (1) ATE486054T1 (ru)
BR (1) BRPI0519246A2 (ru)
DE (1) DE602005024436D1 (ru)
EA (1) EA011556B1 (ru)
ES (1) ES2353806T3 (ru)
MX (1) MX2007007748A (ru)
MY (1) MY144731A (ru)
PL (1) PL1828090T3 (ru)
TW (1) TW200628435A (ru)
UA (1) UA95898C2 (ru)
WO (1) WO2006066904A1 (ru)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104557497A (zh) * 2013-10-09 2015-04-29 中国石油化工股份有限公司 一种提高环己基过氧化氢分解酮醇比的方法
US10099985B2 (en) * 2014-10-31 2018-10-16 Ube Industries, Ltd. Method for producing ketone and/or alcohol, and system thereof
US10752549B2 (en) * 2015-02-27 2020-08-25 Gcp Applied Technologies Inc. Modifying cementitious compositions using ketone alcohol oil waste
CN107778133B (zh) * 2016-08-25 2021-05-07 中国石油化工股份有限公司 一种制备环己醇和环己酮的方法

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB716820A (en) 1951-04-19 1954-10-13 Du Pont Preparation of oxidized cyclohexane
JPS49108047A (ru) * 1973-02-20 1974-10-14
US4163027A (en) 1976-11-06 1979-07-31 Basf Aktiengesellschaft Working-up of reaction mixtures containing cyclohexanol and cyclohexanone
DE2650892C3 (de) * 1976-11-06 1980-05-29 Basf Ag, 6700 Ludwigshafen Verfahren zur Aufarbeitung von Cyclohexanol und Cyclohexanon enthaltenden Reaktionsgemischen
NL7802125A (nl) * 1978-02-25 1979-08-28 Stamicarbon Werkwijze voor het bereiden van cycloalkanolen en cycloalkanonen.
NL8201695A (nl) 1982-04-23 1983-11-16 Stamicarbon Werkwijze voor de bereiding van cyclohexanol en cyclohexanon.
JP2500977B2 (ja) 1992-03-24 1996-05-29 三菱化学株式会社 シクロヘキサノンの製造方法
NL9201269A (nl) * 1992-07-15 1994-02-01 Dsm Nv Werkwijze voor de bereiding van cyclohexylhydroperoxide.
US5824819A (en) * 1996-12-18 1998-10-20 Twenty-First Century Research Corporation Methods of preparing an intermediate oxidation product from a hydrocarbon by utilizing an activated initiator
US5892122A (en) * 1997-08-25 1999-04-06 E. I. Du Pont De Nemours And Company Method for making cyclohexanol and cyclohexanone

Also Published As

Publication number Publication date
US7956221B2 (en) 2011-06-07
WO2006066904A1 (en) 2006-06-29
CN101087747B (zh) 2011-06-08
DE602005024436D1 (de) 2010-12-09
EP1828090A1 (en) 2007-09-05
MX2007007748A (es) 2007-08-22
MY144731A (en) 2011-10-31
BRPI0519246A2 (pt) 2009-01-06
ES2353806T3 (es) 2011-03-07
ATE486054T1 (de) 2010-11-15
KR20070094930A (ko) 2007-09-27
EP1828090B1 (en) 2010-10-27
TW200628435A (en) 2006-08-16
JP2008524298A (ja) 2008-07-10
CN101087747A (zh) 2007-12-12
PL1828090T3 (pl) 2011-04-29
US20100137645A1 (en) 2010-06-03
UA95898C2 (ru) 2011-09-26
EA011556B1 (ru) 2009-04-28

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Legal Events

Date Code Title Description
MM4A Lapse of a eurasian patent due to non-payment of renewal fees within the time limit in the following designated state(s)

Designated state(s): AM AZ KZ KG MD TJ TM

MM4A Lapse of a eurasian patent due to non-payment of renewal fees within the time limit in the following designated state(s)

Designated state(s): BY

MM4A Lapse of a eurasian patent due to non-payment of renewal fees within the time limit in the following designated state(s)

Designated state(s): RU