KR970705346A - 히드록시시트르산 농축물 및 그것의 제조방법(hydroxycitric acid concentrate and method of making) - Google Patents

히드록시시트르산 농축물 및 그것의 제조방법(hydroxycitric acid concentrate and method of making) Download PDF

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KR970705346A
KR970705346A KR1019970701179A KR19970701179A KR970705346A KR 970705346 A KR970705346 A KR 970705346A KR 1019970701179 A KR1019970701179 A KR 1019970701179A KR 19970701179 A KR19970701179 A KR 19970701179A KR 970705346 A KR970705346 A KR 970705346A
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hydroxycitric acid
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스코트 알렉산더 모페트
아쇼크 쿠마르 밴다리
뱅가바술라 라빈드라나스
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스코트 알렉산더 모페트
르네상스 허브즈 인코포레이티드
바이탈 말리아 사이언티픽 리서치 파운데이션
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    • A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/70—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
    • A23L2/78—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter by ion-exchange
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/10—Natural spices, flavouring agents or condiments; Extracts thereof
    • A23L27/12—Natural spices, flavouring agents or condiments; Extracts thereof from fruit, e.g. essential oils
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/82—Acid flavourants
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
    • A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
    • A23L3/3454—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
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    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
    • A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
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    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
    • Y02A40/90—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in food processing or handling, e.g. food conservation

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Abstract

본 발명은 23 내지 54중량%의 유리 히드록시시트르산, 6 내지 20중량%의 히드록시시트르산의 락톤, 0.001 내지 8중량%의 시트르산, 및 32 내지 70중량%의 물로 이루어지며, 상기 유리 히드록시시트르산, 히드록시시트르산의 락톤 및 시트르산은 물레 용해된 총 용질 중량의 94 내지 99%를 구성하는, Garcinia 껍질에서 제조된 하이드록시시트르산 농축물과, Garcinia에서 상기 농축물을 제조하는 방법 및 하이드로시시트르산을 함유하는 식품에 관한 것이다.

Description

히드록시시트르산 농축물 및 그것의 제조방법(HTDROXYCITRIC ACID CONCENTRATE AND METHOD OF MAKING)
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (27)

  1. 23 내지 54중량%의 유리 히드록시시트르산, 6 내지 20중량%의 히드록시시트르산의 락톤, 0.001 내지 8중량%의 시트르산, 및 32 내지 70중량%의 물로 이루어지며, 상기 유리 히드록시시트르산, 히드록시시트트산의 락톤 및 시트르산은 물레 용해된 총 용질 중량의 94 내지 99%를 구성하는 ,Garcinia 껍질에서 제조된 하이드록시시트르산 농축물.
  2. 제1항에 있어서, 32 내지 48중량%의 유리히드록시시트르산, 10 내지 18중량%의 히드록시시트르산의 락톤, 0.001 내지 6중량%의 시트르산, 및 35 내지 55중량%의 물로 이루어지며, 상기 유리 히드록시시트르산, 히드록시시트르산의 락톤 및 시트르산은 물은 용해된 총 용질 중량의 96 내지 99%를 구성하는 , 하이드록시시트르산 농축물.
  3. 제2항에 있어서, 36 내지 48중량%의 유리히드록시시트르산, 10 내지 18중량%의 히드록시시트르산의 락톤, 0.001 내지 3중량%의 시트르산, 및 38 내지 50중량%의 물로 이루어지며, 상기 유리 히드록시시트르산, 히드록시시트르산의 락톤 및 시트르산은 물은 용해된 총 용질 중량의 98 내지 99%를 구성하는 , 하이드록시시트르산 농축물.
  4. (1) Garcinia 껍질의 무염의 물 추출물을 얻고, (2) 히드록시시트르산을 음이온 교환컬럼 상에 흡착시키기 위해 음이온 교환 컬럼에 상기 추출물을 로딩하고, (3) 상기 히드록시시트르산을 제1용액 중에 금속염으로서 방출시키기 위하여 상기 음이온 교환 칼럼으로부터 상기 히드록시시트르산을 그룹IA 금속 수산화물로 용출시키고, (4) 상기 제1용액을 양이온 교환 컬럼에 러딩시켜 히드록시시트르산을 제2용액 중에 유리산으로서 수집하는 단계로 이루어지며, 상기 추출물이 상기음이온 교환 칼럼의 100-125% 용량으로 로딩되고, 상기 제1용액이 상기 양이온 교환 칼럼의 50-90%의 용량으로 로딩되는 Garcinia껍질로부터 하이드록시시트르산을 부화(富化)시키는 방법,
  5. 제4항에 있어서, 상기 물 추출물이 상기 음이온 교환 칼럼의 105-115%의 용량으로 로딩되는 방법.
  6. 제4항에 있어서, 상기 제1용액이 상기 양이온 교환 칼럼의 50-75%의 용량으로 로딩되는 방법.
  7. 제5항에 있어서, 상기 제1용액이 상기 양이온 교환 칼럼의 60-75%의 용량으로 로딩되는 방법.
  8. 제4항에 있어서, 상기 그룹 IA 금속 수산화물이 NaOH 또는 KOH인 방법.
  9. 제4항에 있어서, 상기 무염의 물 수용액이 염에 절인 Garcinia 껍질을 제1추출하고, 물과 섞일 수 있는 유기 용매로 염을 제거하는 것에 의해 제조되는 방법.
  10. 제9항에 있어서, 상기 용매가 아세톤 또는 에틸 알코올의 방법.
  11. 제4항에 있어서, 상기 (4) 단계 후에, 제2용액의 부피를 줄여 하이드록시트르산 농축물을 만든 다음이 농축물을 식품에 첨가하는 단계를 포함하는 방법.
  12. 제11항에 있어서, 상기 식품이 음료인 방법.
  13. 제11항에 있어서, 상기 식품이 스낵 바인 방법.
  14. 0.17 내지 23중량%의 유리 히드록시시트르산, 0.08 내지 7중량%의 히드록시시트르산의 락톤 및 0.002중량% 이상의 시트르산을 포함하는 식품.
  15. 제14항에 있어서, 0.35 내지 12중량%의 유리히드록시시트르산, 0.15 내지 중량%의 히드록시시트르산의 락톤 및 0.002중량% 이상의 시트르산을 포함하는 식품.
  16. 제14항에 있어서, 0.04 내지 0.4중량%의 비타민 C를 추가로 함유하는 식품.
  17. 제15항에 있어서, 0.04 내지 0.4중량%의 비타민 C를 추가로 함유하는 식품.
  18. 제16항에 있어서, 0.04 내지 0.08중량%의 비타민 C를 추가로 함유하는 식품.
  19. 제17항에 있어서, 0.04 내지 0.08중량%의 비타민 C를 추가로 함유하는 식품.
  20. 제14항에 있어서, 0.8 내지 22중량%의 섬유를 추가로 함유하는 식품.
  21. 제15항에 있어서, 0.8 내지 22중량%의 섬유를 추가로 함유하는 식품.
  22. 제15항에 있어서, 상기 식품이 음료인 식품.
  23. 제17항에 있어서, 상기 식품이 음료인 식품.
  24. 제21항에 있어서, 상기 식품이 음료인 식품.
  25. 제15항에 있어서, 상기 식품이 스넥 바인 식품.
  26. 제17항에 있어서, 상기 식품이 스넥 바인 식품.
  27. 제21항에 있어서, 상기 식품이 스넥 바인 식품.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019970701179A 1994-08-24 1995-08-22 히드록시시트르산농축물및그것의제조방법 KR100390036B1 (ko)

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US08/295,281 US5536516A (en) 1994-08-24 1994-08-24 Hydroxycitric acid concentrate and food products prepared therefrom

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US6770782B1 (en) * 1995-05-15 2004-08-03 Sabinsa Corporation Process for the production of potassium hydroxy citric acid, and compositions containing the potassium hydroxy citric acid
AU5736096A (en) * 1995-05-15 1996-11-29 Sabinsa Corporation A new process for the production of potassium hydroxy citric acid, and compositions containing the potassium hydroxy cit ric acid
IT1276253B1 (it) 1995-12-15 1997-10-27 Sigma Tau Ind Farmaceuti Composizione farmaceutica contenente l-carnitina o alcanoil l-carnitine per la prevenzione ed il trattamento di stati morbosi
ES2106689B1 (es) * 1996-04-18 1998-05-16 Cabo Soler Jose Nueva formulacion a base de acido hidroxicitrico (sales y derivados) y sus aplicaciones cosmeticas y farmaceuticas por via topica percutanea.
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KR100390036B1 (ko) 2003-10-30
CA2198376C (en) 2011-01-04
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CA2198376A1 (en) 1996-02-29
EP0782399A1 (en) 1997-07-09
WO1996005741A1 (en) 1996-02-29
BR9508766A (pt) 1997-11-11
CN1082354C (zh) 2002-04-10
US5656314A (en) 1997-08-12
US5536516A (en) 1996-07-16
EP0782399A4 (en) 1998-06-03
JP4083216B2 (ja) 2008-04-30
AU3412995A (en) 1996-03-14
DE69523614D1 (de) 2001-12-06
TW338710B (en) 1998-08-21
EP0782399B1 (en) 2001-10-31
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