KR920017945A - 전자산업용 과산화수소 정제방법 - Google Patents
전자산업용 과산화수소 정제방법 Download PDFInfo
- Publication number
- KR920017945A KR920017945A KR1019920002555A KR920002555A KR920017945A KR 920017945 A KR920017945 A KR 920017945A KR 1019920002555 A KR1019920002555 A KR 1019920002555A KR 920002555 A KR920002555 A KR 920002555A KR 920017945 A KR920017945 A KR 920017945A
- Authority
- KR
- South Korea
- Prior art keywords
- hydrogen peroxide
- purifying
- purifying hydrogen
- distillation
- purification method
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
- C01B15/01—Hydrogen peroxide
- C01B15/013—Separation; Purification; Concentration
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
Abstract
내용 없음
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
Claims (6)
- 증류방법으로 미리 정제한 과산화수소에다 적은 양의 킬레이트화합물을 첨가하고 비이온교환 수지 흡착제와 접촉시키는 것을 특징으로 하는 반도체 기술에 사용할 수 있도록 아주 적은 양의 무기와 유기 불순물, 또는 무기나 유기 불순물을 함유하고 있는 과산화수소의 순도를 더 높이는 과산화수소 정제방법.
- 제1항에 있어서, 보로시리케이트 유리관에 증류로 미리 정제한 과산화수소를 넣는 것을 특징으로 하는 과산화수소 정제방법.
- 제1항에 있어서, 킬레이트 화합물을을 5에서 20㎎/ℓ가 되게 과산화수소에다 넣는 것을 특징으로 하는 과산화수소 정제방법.
- 제1항에 있어서, 수지 흡착제로는 스틸렌과 디비닐벤질을 기초로 하는 공중합물을 사용하는 것을 특징으로 하는 과산화수소 정제방법.
- 제4항에 있어서, 무게비로 88-92%의 스틸렌과 8-12%의 디비닐벤질을 기초로 한 공중합체를 사용하는 것을 특징으로 하는 과산화수소 정제방법.
- 상기 전 청구한 중 어느 한 항에 있어서, 수지 흡착제를 충진한 관을 통해서 과산화수소를 유입시키는 것을 특징으로 하는 과산화수소 정제방법.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DEP4107244.8 | 1991-03-07 | ||
DE4107244A DE4107244A1 (de) | 1991-03-07 | 1991-03-07 | Verfahren zur reinigung von wasserstoffperoxid fuer die mikroelektronik |
Publications (2)
Publication Number | Publication Date |
---|---|
KR920017945A true KR920017945A (ko) | 1992-10-21 |
KR100198481B1 KR100198481B1 (ko) | 1999-06-15 |
Family
ID=6426653
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019920002555A KR100198481B1 (ko) | 1991-03-07 | 1992-02-20 | 전자산업용 과산화수소 정제방법 |
Country Status (7)
Country | Link |
---|---|
US (1) | US5232680A (ko) |
EP (1) | EP0502466B1 (ko) |
JP (1) | JPH04325406A (ko) |
KR (1) | KR100198481B1 (ko) |
AT (1) | ATE128950T1 (ko) |
CA (1) | CA2062435C (ko) |
DE (2) | DE4107244A1 (ko) |
Families Citing this family (23)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE4240370C1 (de) * | 1992-12-01 | 1994-05-11 | Degussa | Verfahren zur Verringerung des Kohlenstoffgehalts wäßriger Wasserstoffperoxidlösungen |
DE69406187T2 (de) * | 1993-05-28 | 1998-02-12 | Mitsubishi Gas Chemical Co | Verfahren zur Reinigung von Wasserstoffperoxyd |
US5614165A (en) * | 1993-05-28 | 1997-03-25 | Mitsubishi Gas Chemical Co., Inc. | Process for purification of hydrogen peroxide |
TW305821B (ko) * | 1993-09-13 | 1997-05-21 | Mitsubishi Gas Chemical Co | |
US5670028A (en) * | 1994-11-22 | 1997-09-23 | Ube Industries, Ltd. | Process for preparing high purity hydrogen peroxide aqueous solution |
FI97538C (fi) * | 1995-02-15 | 1997-01-10 | Kemira Chemicals Oy | Menetelmä vetyperoksidin oleellisesti puhtaan vesiliuoksen valmistamiseksi |
JP3715371B2 (ja) * | 1996-04-08 | 2005-11-09 | 三菱化学株式会社 | 過酸化水素水の精製方法 |
JP3874036B2 (ja) * | 1996-10-09 | 2007-01-31 | 三菱瓦斯化学株式会社 | 精製過酸化水素水溶液の製造方法 |
FR2763932B1 (fr) | 1997-05-27 | 1999-07-30 | Chemoxal Sa | Procede de preparation d'une solution ultra-pure de peroxyde par echange ionique dans des lits a rapports h/d definis |
FR2763930B1 (fr) * | 1997-05-27 | 1999-07-30 | Chemoxal Sa | Procede de preparation d'une solution ultra-pure de peroxyde d'hydrogene par echange ionique sequence : anionique- cationique-anionique-cationique |
DE19926725A1 (de) * | 1999-06-11 | 2000-12-14 | Basf Ag | Verfahren zur Umsetzung organischer Verbindungen mit Wasserstoffperoxid |
FR2800366B1 (fr) * | 1999-10-27 | 2002-05-24 | Air Liquide | Procede de purification de solutions aqueuses de peroxyde d'hydrogene |
DE10026363A1 (de) * | 2000-05-27 | 2001-11-29 | Merck Patent Gmbh | Verfahren zur Aufreinigung von Wasserstoffperoxidlösungen |
US7722847B2 (en) * | 2002-09-30 | 2010-05-25 | Evonik Degussa Gmbh | Aqueous hydrogen peroxide solutions and method of making same |
EP1403219A1 (en) † | 2002-09-30 | 2004-03-31 | Degussa AG | Novel aqueous hydrogen peroxide solutions |
EP1762252A1 (en) * | 2005-09-12 | 2007-03-14 | SOLVAY (Société Anonyme) | Aqueous solution suitable for the chemical sterilization of packaging materials, process for its preparation and its use |
US8899556B2 (en) * | 2007-11-15 | 2014-12-02 | Lawrence Livermore National Security, Llc. | Systems and methods for generation of hydrogen peroxide vapor |
CN102706981B (zh) * | 2012-06-20 | 2014-09-10 | 湘潭大学 | 一种用正相高效液相吸附色谱分析蒽醌法生产双氧水工作液的定量分析方法 |
EP2857351A1 (en) * | 2013-10-02 | 2015-04-08 | Solvay SA | Process for manufacturing a purified aqueous hydrogen peroxide solution |
KR102421905B1 (ko) * | 2013-10-02 | 2022-07-18 | 솔베이(소시에떼아노님) | 정제된 과산화수소 수용액의 제조 방법 |
CA3108081A1 (en) | 2018-08-02 | 2020-02-06 | Evonik Corporation | Process for preparing a stabilized aqueous hydrogen peroxide solution |
CN112533865A (zh) | 2018-08-02 | 2021-03-19 | 赢创有限公司 | 经聚合物稳定的过氧化氢水溶液和相关方法 |
WO2022272257A1 (en) * | 2021-06-23 | 2022-12-29 | Evonik Corporation | A process for sterilization treatment using a residue-free hydrogen peroxide |
Family Cites Families (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3297404A (en) * | 1957-07-08 | 1967-01-10 | Du Pont | Purification of hydrogen peroxide |
US3012860A (en) * | 1958-03-17 | 1961-12-12 | Shell Oil Co | Hydrogen peroxide purification |
FR1539843A (fr) * | 1967-08-01 | 1968-09-20 | Oxysynthese | Purification organique des solutions aqueuses de peroxyde d'hydrogène |
JP2570308B2 (ja) * | 1986-08-06 | 1997-01-08 | 三菱瓦斯化学株式会社 | 過酸化水素水溶液中の有機不純物を除去する方法 |
JPH01153509A (ja) * | 1987-12-11 | 1989-06-15 | Tokai Denka Kogyo Kk | 高純度過酸化水素の製造方法 |
DE3822348A1 (de) * | 1988-07-01 | 1990-01-04 | Siemens Ag | Reinigungsverfahren fuer wasserstoffperoxid |
US4999179A (en) * | 1988-12-26 | 1991-03-12 | Mitsubishi Gas Chemical Company, Inc. | Method for purifying impure aqueous hydrogen peroxide solution |
JP2643542B2 (ja) * | 1990-06-14 | 1997-08-20 | 積水化学工業株式会社 | 熱可塑性ポリウレタンの製造方法 |
-
1991
- 1991-03-07 DE DE4107244A patent/DE4107244A1/de not_active Withdrawn
-
1992
- 1992-02-20 KR KR1019920002555A patent/KR100198481B1/ko not_active IP Right Cessation
- 1992-02-26 US US07/841,536 patent/US5232680A/en not_active Expired - Fee Related
- 1992-03-02 AT AT92103595T patent/ATE128950T1/de not_active IP Right Cessation
- 1992-03-02 DE DE59203930T patent/DE59203930D1/de not_active Expired - Fee Related
- 1992-03-02 EP EP92103595A patent/EP0502466B1/de not_active Expired - Lifetime
- 1992-03-04 JP JP4046918A patent/JPH04325406A/ja active Pending
- 1992-03-06 CA CA002062435A patent/CA2062435C/en not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
CA2062435A1 (en) | 1992-09-08 |
JPH04325406A (ja) | 1992-11-13 |
EP0502466A1 (de) | 1992-09-09 |
EP0502466B1 (de) | 1995-10-11 |
ATE128950T1 (de) | 1995-10-15 |
DE59203930D1 (de) | 1995-11-16 |
US5232680A (en) | 1993-08-03 |
CA2062435C (en) | 2002-01-08 |
DE4107244A1 (de) | 1992-09-10 |
KR100198481B1 (ko) | 1999-06-15 |
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LAPS | Lapse due to unpaid annual fee |